Table 2.
Position | 1 a | 2 a | 3 a | 4 b |
---|---|---|---|---|
1 | 147.1, C | 87.8, C | 88.0, C | 158.8, C |
2 | 120.1, CH | 128.2, CH | 128.3, CH | 119.4, CH |
3 | 52.0, CH | 140.4, CH | 140.8, CH | 137.8, CH |
4 | 83.4, C | 72.8, C | 73.4, C | 133.3, C |
5 | 38.5, CH2 | 36.5, CH2 | 41.0, CH2 | 195.1, C |
6 | 34.7, CH2 | 35.2, CH2 | 25.4, CH2 | 45.7, CH2 |
7 | 88.9, C | 219.3, C | 76.0, CH | 204.3, C |
8 | 91.9, C | 79.7, C | 75.8, C | 86.1, C |
9 | 29.9, CH2 | 42.0, CH2 | 39.0, CH2 | 33.3, CH2 |
10 | 24,1, CH2 | 25.9, CH2 | 25.5, CH2 | 27.2, CH2 |
11 | 65.6, CH | 150.3, CH | 149.5, CH | 143.6, CH |
12 | 60.4, C | 125.1, C | 125.5, C | 130.9, C |
13 | 33.0, CH2 | 25.0, CH2 | 25.8, CH2 | 37.1, CH2 |
14 | 25.8, CH2 | 27.5, CH2 | 27.5, CH2 | 27.6, CH2 |
15 | 34.0, CH | 38.4, CH | 38.9, CH | 36.3, CH |
16 | 21.3, CH3 | 17.4, CH3 | 17.4, CH3 | 22.4, CH3 |
17 | 23.9, CH3 | 17.1, CH3 | 17.1, CH3 | 21.7, CH3 |
18 | 26.2, CH3 | 29.3, CH3 | 30.2, CH3 | 10.9, CH3 |
19 | 25.1, CH3 | 28.5, CH3 | 24.4, CH3 | 28.9, CH3 |
20 | 173.9, C | 168.8, C | 169.5, C | 165.8, C |
a Measured in CD3OD; b Measured in CDCl3.