Table 1.
Data collection and refinement statistics for the structure of the olfactomedin (OLF) domain of mouse myocilin, PDB 6NAX.
| Data Collection | |
|---|---|
| Space group | P4 |
| Cell dimensions | |
| a, b, c (Å) | 112.0, 112.0, 44.1 |
| α, β, γ (degrees) | 90, 90, 90 |
| Resolution (Å) | 33.11 – 1.55 (1.61 – 1.55) |
| Reflections | |
| Total | 355,190 (29,541) |
| Unique | 79,283 (7,499) |
| Redundancy | 4.5 (3.9) |
| Completeness (%) | 98.5 (95.2) |
| Wilson B-factor | 11.6 |
| Rsym | 0.0671 (0.210) |
| I/Iσ | 18.0 (6.1) |
| CC1/2 | 0.996 (0.950) |
| CC* | 0.999 (0.987) |
| Refinement | |
| Resolution (Å) | 33.11 – 1.55 (1.61 – 1.55) |
| Reflections | |
| Used in refinement | 78,413 (7,499) |
| Used for R-free | 2,000 (193) |
| R-work/R-free | 0.158 (0.173) / 0.178 (0.201) |
| CC (work) / CC (free) | 0.968 (0.934) / 0.970 (0.916) |
| Molecules | |
| Protein residues | 518 |
| Ligands | 29 |
| Solvent | 623 |
| B-factor: average | 15.0 |
| Protein residues | 13.2 |
| Ligands | 26.8 |
| Solvent | 26.3 |
| RMS | |
| Bond-lengths (Å) | 0.01 |
| Bond-lengths (deg) | 0.88 |
| Ramachandran | |
| Favored (%) | 96.69 |
| Allowed (%) | 3.31 |
| Outliers (%) | 0 |
| Clashscore | 3.58 |