Table 7.
Reagents | Volume | |||
---|---|---|---|---|
HNO3 (65%) | 6.0 mL | |||
H2O2 (35%) | 2.0 mL | |||
Step | Temperature (°C) | Pressure (bar) | Time (min) | Power (%) |
1 | 160 | 40 | 5 | 90 |
2 | 200 | 40 | 15 | 90 |
3 | 50 | 40 | 10 | 0 |
4 | 50 | 40 | 0 | 0 |
5 | 50 | 50 | 0 | 0 |
Reagents | Volume | |||
---|---|---|---|---|
HNO3 (65%) | 6.0 mL | |||
H2O2 (35%) | 2.0 mL | |||
Step | Temperature (°C) | Pressure (bar) | Time (min) | Power (%) |
1 | 160 | 40 | 5 | 90 |
2 | 200 | 40 | 15 | 90 |
3 | 50 | 40 | 10 | 0 |
4 | 50 | 40 | 0 | 0 |
5 | 50 | 50 | 0 | 0 |