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(a) Synthesis of dcypf-ligated Ni(I) halides via comproportionation. (b) Solid-state structures and X-band EPR spectra taken at 77 K of dcypfNiI Cl and dcypfNiI Br. ORTEP are shown with thermal ellipsoids at 50% probability. Hydrogen atoms and solvent of crystallization have been removed for clarity. (c) Suzuki–Miyaura reaction using dcypfNiI Cl and dcypfNiI Br as precatalysts.
