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. Author manuscript; available in PMC: 2021 May 4.
Published in final edited form as: Chembiochem. 2020 Jan 21;21(9):1315–1319. doi: 10.1002/cbic.201900609

Figure 2.

Figure 2.

a) Comparison of the DNP enhancements measured in a sample containing 1 mM wildtype ubiquitin with 15 mM dispersed TOTAPOL (left) and 1 mM ubiquitin-TTz (right). Spectra were acquired at 600 MHz 1H Larmor frequency, 12 kHz MAS, 100 K. b) DNP-enhanced 2D 13C-13C CORD correlation[36] spectrum of 1 mM ubiquitin-TTz acquired at 24 kHz.