Abstract
Selective laser melting (SLM) is a powder bed fusion type metal additive manufacturing process which is being applied to manufacture highly customised and value-added parts in biomedical, defence, aerospace, and automotive industries. Aluminium alloy is one of the widely used metals in manufacturing parts in SLM in these sectors due to its light weight, high strength, and corrosion resistance properties. Parts used in such applications can be subjected to severe dynamic loadings and high temperature conditions in service. It is important to understand the mechanical response of such products produced by SLM under different loading and operating conditions. This paper presents a comprehensive review of the latest research carried out in understanding the mechanical properties of aluminium alloys processed by SLM under static, dynamic, different build orientations, and heat treatment conditions with the aim of identifying research gaps and future research directions.
Keywords: selective laser melting, aluminium alloys, mechanical properties, tensile, compression, fatigue, heat treatment, build orientation
1. Introduction
Additive manufacturing (AM), more popularly known as 3D printing (3DP), has been extensively applied for various engineering applications. When compared to conventional manufacturing, highly complex parts such as lattice structures can be produced by AM because of the layer-by-layer fabrication process [1]. In recent times, AM technologies are being sought after for providing customized solutions to problems arising due to the COVID-19 virus [2]. Several technologies are in practice for the AM of metallic parts, which include selective laser melting (SLM), electron beam melting (EBM), laser engineered net shaping (LENS), direct metal deposition (DMD), and cold spray additive manufacturing (CSAM). Each of these processes offers its own merits and limitations in terms of quality of the print-part, mechanical property, performance of the component, and the range of materials that can be fabricated. Among these AM processes, SLM is being widely accepted by industry to manufacture customized, high value-added, and complex metal components for aerospace, automotive, defence, and biomedical applications [3]. SLM is a powder-bed fusion type process that produces metal parts by selectively fusing metal powders on a platform using a laser beam. Figure 1 presents the schematic illustration of the SLM process. According to Kempen et al. [4], the fusing occurs through the melting and rapid solidification of metal powders scanned by a laser beam along a 3D print-path created by a processing software.
Figure 1.
Illustration of the SLM process [5].
Aluminium alloys, titanium alloys, steels including stainless steels and tool steels, nickel superalloys, and cobalt-chromium alloys are the most common SLM-processed metals. There is a growing need for SLM to create fully dense parts, where mechanical, thermal, and other properties are comparable to those of the wrought and/or conventionally fabricated materials. However, SLM is a very complex process and a lot of research is targeted at understanding the effects of various process parameters on mechanical properties, performance, and quality of printed parts. Some of the main process parameters affecting part quality and properties in SLM are the laser power, hatch spacing, defocus distance, powder layer thickness, scan speed, and scan strategy. Maamoun et al. [6] presented a detailed study on the influence of these processing parameters on relative density, porosity, surface roughness, and dimensional accuracy. They identified an optimal processing window using process maps to achieve desired values for each performance characteristic. Likewise, Rashid et al. [7] have reported that varying a single SLM parameter, scan strategy, can result in significantly different microstructural and mechanical properties of the printed parts. Therefore, it is very important to understand the effects of the different SLM process parameters on the part quality and properties.
Aluminium (Al) and its alloys are characterized by their light weight, high strength, corrosion resistance, and good weldability, making them suitable for a range of applications in industries such as automotive, aerospace, machinery and tooling, defence, and construction. Of the different alloy combinations, aluminium-silicon-based alloys (Al-Si), specifically AlSi10Mg, AlSi12, A356 (AlSi7Mg0.3), and A357 (AlSi7Mg0.7), have been extensively used in the SLM process owing to their fabricability.
This paper presents a comprehensive review on latest research conducted on mechanical properties of Al alloys processed by SLM. A large number of articles have been published on process optimization, anisotropy effects due to build orientation, and the improvement of SLM built part properties by heat treatment. This paper presents a classification and discussion of these published papers into various research categories to identify research directions and research gaps for different types of mechanical properties and performance under static and dynamic loading conditions.
2. 3D-Printing of Aluminium Alloys by SLM
Aluminium alloys processed by SLM are attracting attention due to their light weight, high strength to weight ratio, corrosion resistance, and good mechanical properties, and due to the unique advantages offered by SLM, such as tool-less fabrication, geometric freedom, customized design, and intricate shapes. As a result, there is an increased interest from researchers to fabricate Al-Si alloy components using SLM with desirable properties.
Even though Al-Si alloys find extensive applications in the cast form, they are difficult to process using SLM because it is a laser-based process with rapid melting and solidification. Al powders are lightweight, have poor flowability, high reflectivity, and high thermal conductivity. Moreover, Al powders have low laser absorption and are prone to oxidation and balling [8]. Montero-Sistiaga et al. [9] have stated that, besides high reflectivity, high reactivity with oxygen, and high conductivity, there are potential challenges in processing Al alloys using SLM. Despite these drawbacks, aluminium can be alloyed with other metals to overcome some of these challenges. Therefore, the two most common Al-Si alloys used in SLM systems are AlSi10Mg and AlSi12. The addition of silicon to aluminum improves its fluidity and reduces its melting temperature. The addition of magnesium to aluminum increases its strength through solid solution strengthening and also improves its strain hardening ability [10]. Although significant amount of works are published on AlSi10Mg, the research work on AlSi12 and other Al-Si alloys, including A356 and A357, is still evolving [11,12,13,14,15,16,17,18,19,20,21,22,23,24,25,26].
Table 1 presents a compilation of key published literature on the SLM of these Al alloys, which are reviewed in detail in this study, capturing the main findings of each article, considering the process conditions (build orientation, heat treatment, and process optimisation), types of mechanical properties, and type of SLM machine used. It was also noted that most of the researchers have used commercial SLM machines produced by leading SLM manufacturers, such as SLM Solutions, EOS, Concept Laser, Realizer, and Renishaw. More detailed discussion on some of these publications is presented in later sections of this review.
Table 1.
List of published literature on SLM of aluminium alloys.
| Author (Year) | Material | Process Conditions | Mechanical Properties Evaluated | Main Findings | SLM Machine | Reference |
|---|---|---|---|---|---|---|
| Aboulkhair et al. (2016) | AlSi10Mg | Laser power 200 W, layer thickness 25 µm, scan speed 550 mm/s, hatch spacing 80 µm, and scan strategy chess board. Heat treatment: Solution treated at 520 °C for 1 h, water quenched to room temperature and then aged for 6 h at 160 °C. |
Fatigue |
|
Renishaw AM250 | [27] |
| Aboulkhair et al. (2016) | AlSi10Mg | Laser power 200 W, scan speed 550 mm/s, hatch spacing 130 µm, layer thickness 25 µm, and checkerboard scan strategy. Heat treatment: T6 |
Tensile strength, compressive yield strength, nano-hardness |
|
Renishaw AM250 | [11] |
| Aboulkhair et al. (2015) | AlSi10Mg | Laser power 200 W, point distance 80 µm, exposure time 140 µs, hatch spacing 130 µm, layer thickness 25 µm and checkerboard scan strategy. | Tensile and compressive strength, nano-hardness |
|
Renishaw AM250 | [12] |
| Alghamdi and Haghshenas (2019) | AlSi10Mg | Two 400 W lasers at CalRAM Inc. were used, with default SLM 280 parameter set. Heat Treatment: T6, solutionising at 520 °C for 1 h, followed by water quench, then artificial ageing at 170 °C for 4 h. |
Nano-hardness |
|
400 W laser at CalRAM Inc. SLM 280 |
[28] |
| Amani et al. (2018) | AlSi10Mg | Laser power 250 W, scanning speed 571 mm/s, layer thickness 60 µm, and argon gas atmosphere. | Compression behaviour |
|
SLM 250 | [29] |
| Anwar & Pham (2017) | AlSi10Mg | Laser power 350 W, layer thickness 100 µm, laser speed 900 mm/s, and hatch spacing of 0.12 mm. | Tensile strength |
|
SLM Solutions 280 HL | [30] |
| Asgari et al. (2018) | AlSi10Mg | Laser power 370 W, scanning speed 1300 mm/s, hatch distance 190 µm, powder layer thickness 30 µm, build platform pre-heating temperature 200 °C. Build orientation: Vertical and Horizontal. |
Dynamic compression, Split Hopkinson pressure bar testing |
|
EOS M290 machine | [31] |
| Aversa et al. (2017) | A357 | Laser power 195 W, scan speed 1200 mm/s, layer thickness 30 µm, hatching distance 0.1 mm and stripe scanning strategy. | Tensile |
|
EOS M270 Dual Mode system | [32] |
| Awd et al. (2018) | AlSi10Mg | Process parameters not disclosed. Build orientation: 0°, 45° and 90° with respect to the build plate. |
Tensile |
|
M2 Cusing system | [33] |
| Baitimerov et al. (2018) | AlSi12 | Laser power 200 W, layer thickness 50 µm, stripe hatch scanning strategy, powder dried at 100 °C for 1 h and the oxygen inside the build chamber was maintained below 500 ppm. | Density |
|
Sinterstation® Pro DM125 SLM System | [34] |
| Bao et al. (2020) | AlSi10Mg | Laser power ranging 360 W–400 W, layer thickness 0.05 mm, laser scanning speed 1200 mm/s–1500 mm/s, scan spacing 0.13–0.16 mm. | Fatigue |
|
BLT S310 | [35] |
| Bassoli et al. (2018) | A357 | Laser power 950 W, scan speed 2000 mm/s, spot size 400 µm, hatch distance 0.2 mm, layer thickness 50 µm, nitrogen gas chamber atmosphere, preheating temperature 200 °C and skin core scan strategy. | Tensile, Fatigue |
|
X Line 2000R (Concept Laser) | [36] |
| Beretta et al. (2020) | AlSi10Mg | Laser power 350 W, hatch distance 0.13 mm, scan speed 1650 mm/s, layer thickness 50 µm, preheating of build platform up to 150 °C. Build orientation: Horizontal (0°), Inclined (45°), and Vertical (90°). |
Fatigue strength |
|
SLM 280HL v1.0 | [37] |
| Biffi et al. (2018) | AlSi10Mg | Pulsed wave laser: laser power 300 W, build platform temperature 170 °C, exposure time 120 µs, point distance 130 µm, spot size 130 µm, hatch distance 140 µm, layer thickness 25 µm and build chamber environment argon. Continuous wave laser: laser power 350 W, build platform temperature 150 °C, laser travel speed 1150 mm/s, spot size 80 µm, hatch distance 170 µm, layer thickness 50 µm and build environment argon. |
Compression |
|
Renishaw AM 250 system SLM Solutions SLM 500 system |
[38] |
| Boschetto et al. (2017) | AlSi10Mg | Laser power 370 W, scan speed 1300 mm/s, hatch spacing 190 µm, layer thickness 30 µm, laser beam diameter 100 µm, hatch rotation 67°. | Roughness |
|
EOSINT® M290 | [39] |
| Brandl et al. (2012) | AlSi10Mg | Laser power 250 W, beam diameter 0.2 mm, layer thickness 50 µm, scanning speed 500 mm/s, scan spacing 0.15 mm and argon gas shielding, with and without build plate heating, build plate heating temperature 300 °C. Build orientation: 0°, 45°, and 90°. |
Fatigue (using tensile samples), fracture analysis |
|
Trumpf TrumaForm LF130 powder-bed machine | [40] |
| Buchbinder et al. (2013) | AlSi10Mg | Laser power 195 W, layer thickness 30 µm, scanning speed 800 mm/s, hatch distance 150 µm, hatch rotation 67°, preheating temperatures 100°, 150°, 200°, and 250°. | Distortion |
|
EOSINT M 270 | [41] |
| Casati et al. (2018) | AlSi10Mg | Laser power 340 W, hatch distance 0.2 mm, scan rate 1300 mm/s, layer thickness 30 µm, platform temperature 160 °C. | Tensile |
|
EOS M290 SLM system | [42] |
| Ch et al. (2019) | AlSi10Mg | Laser power 370 W, scan speed 1300 mm/s, hatch spacing 0.19 mm, layer thickness 30 µm, preheating up to 300 °C. Build orientation: Horizontal and Vertical. |
Tensile, surface roughness, porosity, fracture morphology |
|
EOS M280 machine | [43] |
| Chen et al. (2017) | AlSi10Mg | Laser power 350 W, scan speed 1170 mm/s, layer thickness 50 µm, hatch spacing 240 µm. | Tensile |
|
SLM 250HL, SLM Solutions | [44] |
| Chou et al. (2015) | AlSi12 | Laser power 0.5–4.5 kW, travel speed 90–180 mm/min, spot size 150 µm, hatch distance 0.1 mm, layer thickness 0.1 mm. | Hardness, density |
|
In house built Pulsed-SLM facility | [45] |
| Chou et al. (2018) | A356 (AlSi7Mg0.3) | Laser power (peak) 5 kW, square pulse, hatch distance 0.1 mm, layer thickness 100 µm, bidirectional zigzag scanning pattern, argon atmosphere. | Density |
|
In house built Pulsed-SLM facility | [21] |
| Dai and Gu (2016) | AlSi10Mg composite | Laser power 180 W, scan speed 100, 200, 300, and 400 mm/s, laser energy per unit length (LEPUL) 450, 600, 900, and 1800 J/m. | Numerical simulation, thermodynamics of the molten pool |
|
In house SLM | [46] |
| Dai et al. (2018) | AlSi10Mg composite | Laser power 200 W, layer thickness 30 µm, scanning speed 100–300 mm/s, hatch spacing 60–100 µm. | Wear |
|
In house SLM | [47] |
| de Menezes et al. (2019) | A357 | Laser power 200 W, layer thickness 25 µm, hatch distance 115 µm. Isothermal aging at 160 °C for 4 h. |
Tensile |
|
Renishaw AM250 SLM system | [48] |
| Delahaye et al. (2019) | AlSi10Mg | Laser power 175 W, scan speed 195 mm/s, layer thickness 60 µm, preheating temperature 200 °C. | Nanohardness, fracture morphology, tensile |
|
MTT SLM 250 | [49] |
| Deleroisse et al. (2017) | AlSi10Mg | Laser power 250 W, scan speed 571 mm/s, layer thickness 60 µm, and argon atmosphere. Heat treatment: T6 heat treatment, annealing at 525 °C for 5 h, water quench and then artificial ageing at 165 °C for 7 h. |
Porosity, strut properties |
|
- | [50] |
| Denti (2018) | A357 | Laser power 950 W, scanning speed 2000 mm/s, hatch distance 0.2 mm, laser spot 400 µm, nitrogen chamber atmosphere, preheated at 200 °C and skin-core scan strategy. | Shear, Tensile |
|
Concept Laser X Line 2000 R | [51] |
| Ding and Wang (2017) | AlSi10Mg | Laser power 400 W, laser beam radius 67.5 µm, hatch space 130 µm, scan speed 300 mm/s. | Modelling and simulation, density, hardness |
|
- | [52] |
| Dong et al. (2018) | AlSi10Mg | Laser power 370 W, laser spot size 100 µm, hatch spacing 190 µm, scanning speed 1500 mm/s, layer thickness 30 µm, argon chamber atmosphere. | Tensile, porosity, fractography |
|
Concept X-line 1000R machine | [53] |
| Everitt et al. (2016) | AlSi10Mg | Laser power 100 W, scan speed 250 mm/s, hatch space 50 µm, argon atmosphere. | Nanohardness |
|
Realizer SLM-50 | [54] |
| Fefelov et al. (2017) | AlSi12 | - | Fracture surface morphology, tensile |
|
EOSINT M 280 device | [55] |
| Fiegl et al. (2019) | AlSi10Mg | Laser power 1000 W, layer thickness of 50 µm, volume energy 40 J/mm3, island scanning strategy and nitrogen atmosphere. | Tensile |
|
X LINE 2000R (modified) | [56] |
| Fiocchi et al. (2017) | AlSi10Mg | Laser power 300 W, spot size 130 µm, layer thickness 25 µm, hatch distance 140 µm, and argon atmosphere. | Differential scanning calorimetry, hardness |
|
Renishaw AM250 | [57] |
| Fousova et al. (2018) | AlSi10Mg | Laser power 350 W, layer thickness 50 µm, scanning speed 500 mm/s, hatch spacing 170 µm, argon atmosphere and chessboard scanning strategy. | Tensile |
|
SLM Solution 280HL machine | [58] |
| Gokuldoss Prashanth et al. (2016) | AlSi12 | Laser power 320 W, scan speed 1455 mm/s, layer thickness 50 µm, hatch spacing 110 µm and argon atmosphere. | Tensile |
|
SLM 250 HL | [18] |
| Girelli et al. (2019) | AlSi10Mg | Laser power 400 W, beam diameter 100 µm, argon atmosphere. Build orientation: Horizontal and Vertical Heat treatment: Solutionising at 540 °C for 1–9 h, followed by ageing at 160 °C for 4 h or 180 °C for 2 h. |
Impact properties, fracture morphology |
|
EOS M290 system | [59] |
| Gong et al. (2017) | AlSi10Mg | - | Tensile |
|
- | [60] |
| Hadadzadeh et al. (2018) | AlSi10Mg | Laser power 370 W, beam spot size 100 µm, scanning speed 1300 mm/s, hatch spacing 190 µm, layer thickness 30 µm, argon atmosphere. Build orientation: Horizontal and Vertical. |
Dynamic compression |
|
EOS M290 machine | [61] |
| Hadadzadeh et al. (2019) | AlSi10Mg | Laser power 370 W, scanning speed 1300 mm/s, hatch spacing 190 µm, layer thickness 30 µm, stripe scanning strategy, argon atmosphere. | Dynamic compression |
|
EOS M290 | [62] |
| Han and Jiao (2019) | AlSi10Mg | Laser power 200 W, hatch spacing 130 µm, layer thickness 25 µm, scanning speed 500 mm/s, chessboard bidirectional scanning strategy. Heat treatment: Solution-treated at 550 °C for 2 h, followed by furnace cooling. Laser surface remelting treatment: Laser power 20 W, beam diameter 32 µm, scanning speed 300 mm/s, layer thickness 0.01 mm. |
Tensile, Hardness, Roughness |
|
Renishaw AM250 | [63] |
| Hatamleh et al. (2018) | A357 | Heat treated at 170 °C for 3 h. Laser shock peening applied. |
Finite element analysis, residual stress analysis, tensile testing |
|
- | [64] |
| Hitzler et al. (2016) | AlSi10Mg | Tensile |
|
SLM 280HL machine | [65] | |
| Hitzler et al. (2017) | AlSi10Mg | Laser power 350 W, hatch spacing 0.42 mm, scan speeds 600–930 mm/s, base plate heating 200 °C. Build orientation: horizontal, inclined (45°), and vertical. |
Fracture toughness |
|
SLM 280HL machine | [66] |
| Hitzler et al. (2017) | AlSi10Mg | Laser power 350 W, hatch spacing 0.42 mm, scan speeds 600–930 mm/s, base plate heating 200 °C, nitrogen atmosphere. | Tensile, surface hardness |
|
SLM 280HL machine | [67] |
| Hitzler et al. (2018) | AlSi10Mg | Laser power 400 W, layer thickness 50 µm, nitrogen atmosphere. | Tensile, compression |
|
SLM 280HL machine | [68] |
| Hu et al. (2016) | AlSi10Mg | Laser energy input 700–1300 J/m, layer thickness 50 µm, argon atmosphere. | CFD model, thermal gradient |
|
- | [69] |
| Iturrioz et al. (2018) | AlSi10Mg | Laser power 400 W, protective atmosphere. Heat treatment: Stress-relieving (heating rate of 10 °C/min until 300 °C for 2 h), Solution-treated at 450 °C and 550 °C for 2 h, followed by water quenching, and T6 heat treatment. |
Tensile, hardness, density |
|
SLM 280HL machine | [70] |
| Jawade et al. (2020) | AlSi10Mg | Laser power 250 W, beam diameter 0.2 mm, layer thickness 50 µm, scanning speed 500 mm/s. | Tensile |
|
Renishaw AM 250 | [71] |
| Jiang et al. (2018) | AlSi10Mg composite | Laser power 370 W, scan speed ranging from 900–1900 mm/s, scan spacing 105 µm, layer thickness 30 µm, zigzag scan strategy. | Tensile, hardness, density |
|
Concept Laser M2 Cusing SLM system | [72] |
| Jing et al. (2019) | AlSi10Mg | Hatch spacing 190 µm, layer thickness 30 µm, volume energy density 26–54 Jmm−3, laser power 310–390 W, scanning speed 1300–1900 mm/s, chamber pressure 0.45 mbar. Build orientation: Horizontal and Vertical. |
Porosity, microhardness, tensile testing and fracture morphology |
|
EOS 83 M290 SLM | [73] |
| Kang et al. (2017) | AlSi12 | Laser power 400 W, scanning speed 5000 mm/s, layer thickness 50 µm and hatch distance 45 µm. | Tensile |
|
Realizer SLM 250 machine | [74] |
| Kempen et al. (2012) | AlSi10Mg | 200 W fiber laser, laser beam diameter 150 µm, scan speed 1400 mm/s, scan spacing 105 µm. Build orientation: Horizontal and Vertical. |
Tensile |
|
Modified Concept Laser M1 SLM Machine | [4] |
| Kempen et al. (2014) | AlSi10Mg | Laser power 300 W, laser spot size 80 µm, scan speed 1600 mm/s. Build orientation: XY and Z. |
Surface roughness, Metrology |
|
In-house built SLM machine | [75] |
| Kempen et al. (2015) | AlSi10Mg | 200 W fiber laser, laser beam diameter 150 µm, scan speed 1400 mm/s, scan spacing 105 µm and layer thickness 30 µm. Build orientation: Horizontal and Vertical. |
Tensile, Hardness |
|
Modified Concept Laser M1 SLM Machine | [76] |
| Kempen et al. (2011) | AlSi10Mg | 170 to 200 W fiber laser, laser beam diameter 150 µm, scan speed 200–1400 mm/s, scan spacing 105 µm and layer thickness 30 µm. Build orientation: Horizontal and Vertical. |
Density, Roughness |
|
Modified Concept Laser M1 SLM Machine | [77] |
| Kim et al. (2016) | AlSi10Mg | Laser power 200 W, scanning speed 1500 mm/s, bidirectional scanning vector. | Tensile |
|
Concept Laser M2 machine | [78] |
| Kimura and Nakamoto (2016) | A356 | Laser power 200–370 W, scan speed 400–3000 mm/s, scan spacing 0.08–0.18 mm, layer thickness of 30 µm. | Tensile, Density |
|
EOSINT M280 SLM | [20] |
| Krishnan et al. (2014) | AlSi10Mg | 200 W Yb fiber laser, layer thickness 20–40 µm, beam diameter 0.1 mm, laser power 180–195 W, scanning speed 700–900 mm/s, hatch distance 0.1–0.25 mm, nitrogen atmosphere. | Hardness, Density |
|
- | [79] |
| Li et al. (2016) | AlSi10Mg | Laser power 350 W, beam diameter 80 µm, scan speed 1140 mm/s, layer thickness 50 µm, scan spacing 170 µm, argon chamber atmosphere, substrate plate pre-heated to 100 °C. Heat treatment: T6 treatment, solution treated at 450 °C, 500 °C, and 550 °C for 2 h, water quenched, and aged at 180 °C for 12 h. |
Tensile, hardness |
|
SLM250 HL | [80] |
| Li et al. (2017) | AlSi10Mg | Build orientation: Horizontal (Y-direction) and Vertical (Z-direction), tensile testing carried out at −71 °C. | Tensile |
|
- | [81] |
| Li et al. (2015) | AlSi12 | Laser power 200 W, scanning speed 500 mm/s, layer thickness 50 µm, scan spacing 150 µm, substrate heated to 200 °C, argon atmosphere. Heat treatment: Solution treated at 500 °C for 4 h and water quenched. |
Tensile, residual stresses, FEM |
|
ReaLizer SLM-100 machine | [82] |
| Li et al. (2018) | AlSi10Mg | Laser power 200 W, hatch spacing 80 µm, laser spot diameter 80 µm, layer thickness 25 µm, exposure time 100–180 µs, point distance 60–100 µm. | Modelling and simulation |
|
Renishaw AM 400 SLM system (Renishaw PLC) | [83] |
| Li and Gu (2014) | AlSi10Mg | Laser power of 150–300 W, laser spot diameter 70 µm, scanning speed 100–400 mm/s, layer thickness 50 µm, hatch spacing 50 µm, argon atmosphere. | Modelling and simulation |
|
YLR-500-SM | [84] |
| Liu et al. (2010) | AlSi10Mg | Laser power 200 W | Tensile, hardness, density, roughness |
|
M2 Cusing from Concept Laser, Germany | [85] |
| Liu et al. (2018) | AlSi10Mg | Laser power 500 W, scan speed 1500 mm/s, layer thickness 30 µm, zigzag scan strategy, scanning angle alternated by 90° for subsequent layers. | Hardness, wear resistance, modelling and simulation |
|
BLT-S300 SLM machine | [86] |
| Liu et al. (2018) | AlSi10Mg | Laser power 160–200 W, spot size 100 µm, scanning speed 200–1000 mm/s, argon atmosphere. | Modelling and simulation |
|
IPG YLR-200 | [87] |
| Louvis et al. (2011) | AA 6061 | Laser power 50–100 W, laser spot size 80 µm, hatch spacing 0.05–0.3 mm, scan speed range 75–1000 mm/s, layer thickness 50 µm, argon atmosphere, point distance 65–85 µm | Density |
|
MCP Realizer 100 SLM machine | [8] |
| Maamoun et al. (2019) | AlSi10Mg & AA 6061 | For AA 6061: Laser power 300–370 W), scanning speed 800–1300 mm/s, hatch spacing 0.1–0.19 mm, energy density 40.5–123.3 J/mm3. For AlSi10Mg: Laser power 200–370 W), scanning speed 1000–1300 mm/s, hatch spacing 0.15–0.25 mm, energy density 27–65 J/mm3. |
Tensile, hardness |
|
- | [88] |
| Maconachie et al. (2020) | AlSi10Mg | Laser power 350 W, scanning speed 1650 mm/s, layer thickness 30 µm, hatch spacing 130 µm and beam diameter 90 µm. Build Orientation: 0°, 45° and 90°. |
Tensile, dynamic behaviour in tension (SHTB), fracture |
|
SLM500 | [89] |
| Majeed et al. (2019) | AlSi10Mg | Laser power 320 W, hatch spacing 0.08 mm, layer thickness 30 µm, scanning speed 900 mm/s, checkerboard scanning strategy, argon atmosphere. Heat Treatment: T4 treatment involving solution heat treated at 530 or 540 °C for 2 h and water quenched. T6 treatment involving solution treated at 530 °C for 2 h, water quenched and artificially aged at 155 °C for 12 h. |
Density, tensile, fracture |
|
280 HL SLM | [90] |
| Maskery et al. (2015) | AlSi10Mg | Laser power 200 W, layer thickness 25 µm, hatch spacing 130 µm, scanning speed 571 mm/s, point distance 80 µm, exposure time 140 µs, build platform temperature 180 °C, hatch rotation 67°. Heat treatment: Solution treated at 520 °C for 1 h, water quenched, and aged at 160 °C for 6 h. |
Tensile, fatigue |
|
Renishaw AM250 SLM machine | [91] |
| Mfusi et al. (2019) | AlSi10Mg | Laser power 150 W, scanning speed 1000 mm/s, hatch spacing 50 µm, and layer thickness 50 µm. Build Orientation: XY, 45°, and Z orientations. Heat treatment: Stress relief treatment at 300 °C for 2 h followed by furnace cooling. |
Tensile, fatigue crack growth, fracture toughness, density, hardness, porosity |
|
SLM Solution M280 GmbH | [92] |
| Ngnekou et al. (2017) | AlSi10Mg | Laser powers 200 W and 400 W. Build Orientation: XY and Z Heat treatment: Stress relieved at 160 °C for 1 h or 300 °C for 2 h, T6 heat treatment involving solution treated at 540 °C for 8 h, water quenched, and tempered at either 20 °C for 24 h or 160 °C for 10 h. |
Fatigue |
|
Phenix PM100 3D Systems machine EOS M290 machine |
[93] |
| Nurel et al. (2018) | AlSi10Mg | Laser power 400 W, spot diameter 80 µm, scan velocity 1000 mm/s, strip scanning strategy, hatch distance 200 µm, hatch rotation 67°, layer thickness 60 µm, argon atmosphere, build plate temperature 35 °C. Build orientation: Horizontal and Vertical Heat Treatment: T5/Stress relief treated at 300 °C for 2 h. |
Dynamic-Compression |
|
EOSINT M280 system | [94] |
| Nurel et al. (2018) | AlSi10Mg | Laser power 400 W, spot diameter 80 µm, layer thickness 30 µm. Build orientation: Horizontal and Vertical. Heat treatment: T5 at 300 °C for 2 h. |
Dynamic-Compression |
|
EOSINT M280 system | [95] |
| Ojha et al. (2018) | AlSi10Mg | Laser power 100 W, scanning speed 2000 mm/s, spot size 0.2 mm, layer thickness 80 µm. | Modelling and simulation |
|
- | [96] |
| Pei et al. (2017) | AlSi10Mg | Laser power 180 W, scanning speed 600–1600 mm/s, layer thickness 35 µm, spot size 70 µm. | Modelling and simulation |
|
SLM-150 equipment | [97] |
| Pola et al. (2019) | AlSi10Mg | - | Fatigue, porosity, surface roughness, tensile |
|
EOS M290 system | [98] |
| Ponnusamy et al. (2018) | AlSi12 | Laser power 285 W, scanning speed 1000 mm/s, hatch spacing 100 µm, layer thickness 40 µm, defocus distance −4 mm, alternative scan strategy. Build orientation: Horizontal, Inclined, Vertical |
Dynamic - Compression |
|
3D Systems ProX 200 | [99] |
| Ponnusamy et al. (2020) | AlSi12 | Laser power 285 W, scanning speed 1000 mm/s, hatch spacing 100 µm, layer thickness 40 µm, defocus distance −4 mm, alternative scan strategy, hexagon scan pattern, argon atmosphere. Build orientation: Vertical Heat treatment: Annealed at 200 °C and 400 °C for 3 hrs. |
Dynamic compression |
|
ProX 200 | [100] |
| Prashanth et al. (2014) | AlSi12 | Laser power 320 W, layer thickness 50 µm, hatch spacing 110 µm, hatch rotation 73°, scanning speed 1455–1939 mm/s, argon atmosphere. Build orientation: 30°, 45°, 60°, 75°, 90°. Heat treatment: Solution treated at 473–723 K for 6 h. |
Wear rate, corrosion properties |
|
SLM 250 HL | [16] |
| Prashanth et al. (2017) | AlSi12 | Laser power 320 W, layer thickness 50 µm, hatch spacing 110 µm, hatch rotation 73°, scanning speed 1455–1939 mm/s, argon atmosphere, scan strategies included single melt, double melt, single melt continuous, and checkerboard, base plate heating 473–673 K. Heat treatment: Solution treated at 473–723 K for 6 h. |
Tensile |
|
SLM 250 HL | [101] |
| Prashanth et al. (2014) | AlSi12 | Laser power 320 W, layer thickness 50 µm, hatch spacing 110 µm, hatch rotation 73°, scanning speed 1455–1939 mm/s, argon atmosphere. Build orientation: 30°, 45°, 60°, 75°, 90°. Heat treatment: Solution treated at 473–723 K for 6 h. |
Tensile |
|
SLM 250 HL | [17] |
| Qiu et al. (2015) | AlSi10Mg | Laser power 150–400 W, beam spot size 50 µm, scanning speed 1000–7000 mm/s. | Compression |
|
Concept Laser M2 Cusing SLM system | [102] |
| Rakesh et al. (2018) | AlSi10Mg | Laser beam diameter 80 µm, argon/nitrogen gas inert atmosphere. Build orientation: Transverse (XZ), Longitudinal (Y) |
Tensile, Impact strength |
|
EOSINT M280 machine | [103] |
| Rao et al. (2016) | A357 | Laser power 100–370 W, layer thickness 30 µm, hatch distance 0.1 mm, spot size diameter 0.1 mm, scan speed 500–5000 mm/s, substrate temperature 35–200 °C. Build orientation: Horizontal, Vertical. |
Tensile |
|
EOSINT M280 | [25] |
| Rao et al. (2017) | A357 | Laser power 100–370 W, layer thickness 30 µm, hatch distance 0.1 mm, spot size diameter 0.1 mm, scan speed 500–5000 mm/s, substrate temperature 35–200 °C. Heat treatment: Stress relieving at 300 ± 1 °C and air-cooled, solution treating at 535 ± 3 °C in salt bath from 0.25 h to 150 h followed by water quenching. |
Tensile |
|
EOSINT M280 | [24] |
| Rashid et al. (2018) | AlSi12 | Laser power 285 W, scan speed 1000–2000 mm/s, layer thickness 40 µm, hatch distance 100 µm, defocus distance –4 mm. Build orientation: Horizontal, Inclined (45°), Vertical |
Tensile, density |
|
ProX 200 | [104] |
| Rashid et al. (2017) | AlSi12 | Laser power 285 W, scan speed 1000–2000 mm/s, layer thickness 40 µm, hatch distance 100 µm, defocus distance –4 mm. Lattice structures: Circular cells, honeycomb cells, triangular cells |
Flexural |
|
ProX 200 | [105] |
| Rathod et al. (2019) | AlSi12 | Laser power 320 W, scan speed 1455 mm/s, layer thickness 50 µm, and hatch spacing 110 µm. | Wear |
|
280HL equipment | [106] |
| Raus et al. (2017) | AlSi10Mg | Laser spot size 80 µm, laser power 350 W, scan speed 1650 mm/s, layer thickness 30 µm, hatch distance 0.13 mm, stripe scanning strategy, argon atmosphere, build platform temperature 150 °C. | Tensile, hardness, impact toughness |
|
SLM 125 HL | [107] |
| Read et al. (2015) | AlSi10Mg | Laser power 100–200 W, laser track width 150 µm, layer thickness 30 µm, scan speed 700–2000 mm/s, hatch spacing 0.2–0.8 mm, island scanning strategy, island size 2–8 mm, argon atmosphere. Build orientation: Horizontal, Vertical. |
Tensile, creep resistance |
|
Concept Laser M2 Cusing SLM system | [108] |
| Rosenthal et al. (2015) | AlSi10Mg | Laser power 400 W, laser spot size 100 µm, scan velocity 1000 mm/s, strip scanning strategy, hatch rotation 67°. | Tensile, density |
|
EOSINT M280 | [109] |
| Rosenthal et al. (2018) | AlSi10Mg | Laser power 400 W, laser spot size 100 µm, scan velocity 1000 mm/s, hatch distance 200 µm, layer thickness 60 µm, argon atmosphere. Build orientation: Horizontal (X), Vertical (Z). Heat Treatment: T5 stress relief treatment at 300 °C for 2 h, modified T5 at 200 °C for 2 h. |
Impact resistance |
|
EOSINT M280 | [110] |
| Rosenthal and Stern (2016) | AlSi10Mg | Laser power 400 W, laser spot size 100 µm, scan velocity 1000 mm/s, hatch distance 200 µm, layer thickness 60 µm. Heat treatment: Treated at 100–250 °C for 2 h, treated at 200 °C for 168 h, treated at 100 °C for 336 h. |
Hardness |
|
EOSINT M280 | [111] |
| Rosenthal et al. (2014) | AlSi10Mg | Laser power 400 W, scanning speed 1000 mm/s, strip scanning strategy Build orientation: Vertical, Horizontal. Heat treatment: Stress relieving at 300 °C for 2 h. |
Tensile, hardness, fracture morphology |
|
- | [112] |
| Rosenthal et al. (2017) | AlSi10Mg | Laser power 400 W, laser spot size 100 µm, scan velocity 1000 mm/s, hatch distance 200 µm, layer thickness 60 µm, argon atmosphere, build plate temperature 35 °C, strip scanning strategy, hatch rotation 67°. Build orientation: Vertical, Horizontal. |
Tensile, fracture surface analysis |
|
EOSINT M280 | [113] |
| Samantaray et al. (2018) | AlSi10Mg | Laser power ranging 70–190 W, laser spot diameter 0.2 mm, scanning speed 100–500 mm/s, layer thickness 1 mm. | Modelling and simulation |
|
- | [114] |
| Siddique et al. (2017) | AlSi12 | Laser power 400 W, volume energy density 39.6 J/mm3, argon atmosphere. Heat treatment: Stress relieving at 240 °C for 2 h followed by oven cooling. |
Fatigue, tensile |
|
SLM 250 | [115] |
| Siddique et al. (2015) | AlSi12 | Laser power 350 W, scan speed 930 mm/s, hatch distance 0.19–0.25 mm, energy density 20–39.6 J/mm3, argon atmosphere. Heat treatment: Stress relieving at 200 °C followed by oven cooling. |
Fatigue, porosity, modelling and simulation |
|
SLM 250 HL | [116] |
| Siddique et al. (2017) | AlSi12 | Laser power 350 W, scan speed 930 mm/s, hatch spacing 0.19 mm, layer thickness 50 µm, energy density 39.6 J/mm3, scanning strategy chessboard, hatch rotation 79°, argon atmosphere, base plate temperature 200 °C. Build orientation: Vertical. Heat treatment: Stress relieving at 200 °C for 2 h. |
Fatigue, porosity, hardness, crack propagation testing |
|
SLM 250 HL | [14] |
| Siddique et al. (2015) | AlSi12 | Laser power of 400 W, energy density 20–39.6 J/mm3, chessboard scanning strategy, hatch rotation 79°, argon atmosphere, base plate temperature 200 °C. Build orientation: Vertical. Heat treatment: Stress relieving at 240 °C followed by oven cooling. |
Tensile, surface roughness, residual stress analysis, fatigue |
|
SLM 250 HL | [15] |
| Silvestri et al. (2020) | AlSi10Mg | EOS M400: Laser power 1000 W, laser spot diameter 90 µm, nitrogen atmosphere. SLM 280: Laser power 400–1000 W, laser spot diameter 80–225 µm, argon atmosphere. Renishaw AM400: Laser power 400 W, laser spot diameter 70 µm, argon atmosphere. Build orientation: 0°, 60°, 90°. |
Tensile |
|
EOS M400 SLM 280 Renishaw AM400 |
[117] |
| Subbiah et al. (2020) | AlSi10Mg | Laser power 350 W, laser spot size 0.2 mm, scanning speed 730 mm/s, hatch spacing 0.12 mm, layer thickness 30 µm, stripe scanning strategy, inert atmosphere, base plate temperature 150 °C. Heat treatment: Solution treated at 550 °C for 2 h and water quenched. |
Tensile, surface roughness, modelling and simulation |
|
SLM 280 HL | [118] |
| Sun et al. (2019) | AlSi10Mg | Laser power 400 W, laser spot size 100 µm, scanning speed 1000 mm/s, hatch spacing 0.165 mm, layer thickness 25 µm, chessboard scanning strategy, hatch rotation 67°. Heat Treatment: T2 treatment—annealed at 380 °C for 45 mins and air cooled, T6-like treatment—solution treated at 500 °C for 15 mins, quenched, and aged at 158 °C for 10 mins. |
Tensile |
|
Renishaw AM 250 | [119] |
| Suryawanshi et al. (2016) | AlSi12 | Laser power 320 W, layer thickness 50 µm, hatch spacing 110 µm, hatch rotation 73°, scanning speed (1455 mm/s for volume and 1939 mm/s for contour), argon atmosphere, single melt and checkerboard scanning strategy. Heat treatment: solution treated at 573 K for 6 h. |
Tensile, fracture toughness, fatigue crack growth |
|
SLM 250 HL | [120] |
| Takata et al. (2017) | AlSi10Mg | Laser power 380 W, layer thickness 30 µm, hatch spacing 0.1 mm, hatch rotation 67°, argon atmosphere. Build orientation: Horizontal (X/Y), Vertical (Z). Heat treatment: Annealing at 300 °C for 2 h, or solution treatment at 530 °C for 6 h and water quenched. |
Tensile |
|
EOSINT M 280 | [121] |
| Tang and Pistorius (2017) | AlSi10Mg | Laser power 370 W, scan speed 1300 mm/s, layer thickness 30 µm, laser spot diameter 100 µm, hatch spacing 0.16–0.22 mm, hatch rotation 67°. Build orientation: XY, Z. Heat treatment: Stress relieving at 573 K for 2 h. |
Tensile, fracture morphology, porosity |
|
EOS M280 | [122] |
| Tang and Pistorius (2019) | AlSi10Mg | Laser power 370 W, scan speed 1300 mm/s, laser beam diameter 0.1 mm, layer thickness 30 µm, hatch spacing 0.16–0.22 mm, and the Build orientation: XY, Z. Heat treatment: Stress relieving at 573 K for 2 h. |
Fatigue, porosity |
|
EOS M280 | [123] |
| Tradowsky et al. (2016) | AlSi10Mg | Laser power 175 W, laser spot size 60 µm, scan speed 1025 mm/s, layer thickness 30 µm, scan spacing 97.5 µm, chess scanning strategy, island size 5.6 mm, argon atmosphere. Build orientation: Horizontal, Vertical. Heat treatment: Solution treated at 520 °C for 5 h, water quenched, and aged at 160 °C for 12 h followed by air cooling. |
Tensile, porosity, modelling and simulation |
|
Concept Laser M2 cusing system | [124] |
| Trevisan et al. (2016) | A357 | Laser power 195 W, spot size 100 µm, layer thickness 30 µm, scanning speed 1200 mm/s, hatch distance 0.1 mm, hatch rotation 67°, build plate temperature 100 °C. Heat treatment: Stress relieving at 300 °C for 2 h, T6 treatment involving solution treatment at 540 °C for 8 h, water quench, and ageing at 170 °C for 3 h. |
Tensile, hardness |
|
EOSINT M270 Dual mode machine | [125] |
| Uzan et al. (2017) | AlSi10Mg | Laser power 400 W, beam diameter 100–150 µm, scanning speed 1000 mm/s, layer thickness 30 µm and 60 µm (before and after melting), hatch distance 200 µm, stripe scanning strategy, argon atmosphere, build plate temperature 35 °C. Build orientation: Z direction. Heat treatment: Stress relieved at 300 °C for 2 h. |
Fatigue, tensile, fracture toughness, hardness |
|
EOSINT M-280 | [126] |
| Vrana et al. (2016) | AlSi10Mg | Laser power 150–400 W, layer thickness 50 µm, scanning speed 1000–4000 mm/s, nitrogen atmosphere, build platform temperature 120 °C. | Impact testing |
|
SLM 280HL | [127] |
| Wang et al. (2019) | AlSi10Mg | Laser power 370 W, scan speed 1300 mm/s, hatch spacing 190 µm, layer thickness 30 µm, argon atmosphere. Build orientation: Vertical. Heat treatment: Stress relieved at 250 °C for 4 h. |
Tensile, porosity, modelling and simulation |
|
EOS M290 | [128] |
| Wang et al. (2018) | AlSi10Mg | Laser power 400 W, laser spot size 76 µm, scanning speed 1000 mm/s, hatch distance 175 µm, layer thickness 25 µm, chessboard scanning strategy, island size 5 mm, argon atmosphere. Heat treatment: T6 solution treated at 535 °C for 7–15 mins and aged at 158 °C for 10 h. |
Tensile, bending, hardness |
|
Renishaw AM 250 | [129] |
| Wang et al. (2018) | AlSi10Mg | Laser power 400 W, scanning speed 1000 mm/s, hatch spacing 175 µm, layer thickness 25 µm, chessboard scanning strategy, hatch rotation 67°. Build orientation: Parallel, Normal. Heat Treatment: T2 stress relieving treatment at 380 °C for 45 mins followed by air cooling. |
Tensile, bending, hardness |
|
Renishaw AM 250 system | [130] |
| Wang et al. (2014) | AlSi12 | Laser power 200 W, beam diameter 35 µm, scanning speed 375–2000 mm/s, hatch spacing 0.15 mm, layer thickness 50 µm, stripe scanning strategy, hatch rotation 90°, inert atmosphere. | Tensile, hardness |
|
Realizer SLM 100 | [131] |
| Wei et al. (2017) | AlSi10Mg | Laser spot size 70 µm, laser power 150–180 W, scanning speed 600–1400 mm/s, layer thickness 40 µm, hatch spacing 50–70 µm, random scanning strategy, argon atmosphere. | Tensile, fracture morphology |
|
Self-developed SLM 150 equipment | [132] |
| Wu et al. (2016) | AlSi10Mg | Laser power 175 W, scanning speed 1030 mm/s, hatch spacing 0.65 mm, island size 6 mm. | Tensile, in-situ compression testing |
|
Concept Laser M2 system | [133] |
| Yan et al. (2014) | AlSi10Mg | Laser beam diameter 100 µm, laser power of 400 W, layer thickness 30 µm, argon atmosphere. | Compression, computed tomography |
|
EOSINT M280 | [134] |
| Yang et al. (2018) | A357 | Laser power 750 W, scanning speed 1100 mm/s, hatch rotation 90°, build plate temperature 35 °C. Build orientation: Horizontal, Vertical. Heat Treatment: Directly aged at 160 °C for 8 h; Stress-relieved at 300 °C for 2 h; Stress-relieved and solution treated at 543 °C for 1–8 h, quenched and aged at 160 °C for 8 h. |
Tensile, porosity |
|
Concept Laser X-line 1000 machine | [26] |
| Zaretsky et al. (2017) | AlSi10Mg | Build orientation: XY, Z. Heat treatment: T5 stress relieving at 300 °C for 2 h. |
Dynamic and quasi-static tensile |
|
EOSINT M280 system | [135] |
| Zhang et al. (2018) | AlSi10Mg | Laser power 490 W, scanning speed 2000 mm/s, layer thickness 40 µm, hatch spacing 0.1 mm, hatch rotation 90°, argon atmosphere. Heat treatment: Stress relieved at 300 °C for 2 h; Solution treated at 530 °C for h, water quenched, and aged at 170 °C for 12 h. |
Fatigue, tensile |
|
Self-developed SLM system (LSNF-2) | [136] |
| Zhou et al. (2018) | AlSi10Mg | Laser power 400 W, scanning speed 1300 mm/s, layer thickness 30 µm, hatch spacing 0.19 mm. Heat treatment: T6 solution treated at 520 °C for 0.5–4 h, water quenched, and aged at 160 °C for 1–24 h. |
Hardness |
|
EOS M280 | [137] |
| Zhou et al. (2019) | AlSi10Mg | Laser power 300 W, scanning speed 800 mm/s, laser spot size 80 µm, hatch spacing 0.13 mm, layer thickness 30 µm, volumetric energy density 62.5 J/mm3, argon atmosphere, build plate temperature 150 °C. Heat treatment: Stress relieved at 300 °C for 2 h and water quenched; solution treated 535 °C for 1 h, water quenched, and aged at 190 °C for 10 h. |
Tensile |
|
SLM 280 HL | [138] |
It is evident from the information presented in Table 1 that there is a lot of interest in understanding the SLM processability of various aluminium alloys. Olakanmi et al. [139] reported in detail the influence of process parameters, powder properties, and laser types on the densification of aluminium alloys. Moreover, they also reported the potential issues arising during the SLM of aluminium alloys, such as metallurgical defects, porosity, and oxidation. The primary causes for these processing challenges include high reflectivity, high thermal conductivity, and poor flowability of aluminium alloy powders, which, as reported by Aversa et al. [140], can be addressed by the development of new alloys specifically designed to improve the SLM-printability of various aluminium alloys. This idea was corroborated by Sercombe and Li [141] who reported improved microstructures and enhanced mechanical properties of various aluminium metal matrix composites fabricated via SLM.
The primary research focus areas of most of the published literature on SLM of aluminium alloys can be broadly classified into four categories, viz, process parameter optimization, effects of build orientation, in-situ and post heat treatment strategies, and modelling and numerical analysis of print-part performance as listed in the overview of publications in Table 2. It is clear from this overview that AlSi10Mg alloy has received maximum attention of research papers for all four research focus areas for mechanical properties, with a large number of researchers paying attention to the effects of build orientation and heat treatment of this alloy. More research needs to be done on process optimization and effects of the build orientation and heat treatment of AlSi12 alloy and other two less popular A356 and A357 alloys processed by SLM. As reported by Rometsch et al. [142] and Zhang et al. [143], these studies aim to improve the performance of SLM-printed aluminium components via: (a) optimizing powder characteristics, (b) optimizing process parameters to obtain 100% dense parts, (c) minimizing the defects such as residual stresses, distortion, and cracking, (d) optimizing post heat treatment techniques to achieve desired mechanical properties, (e) understanding the microstructural characteristics of the print-part, and (f) anisotropic mechanical properties as a result of varying build orientation.
Table 2.
Overview of research focus areas into four categories.
| Aluminium Alloy | Process Parameter Optimisation | Build Orientation | Heat Treatment | Numerical Studies |
|---|---|---|---|---|
| AlSi10Mg | [38,73,76,77,79,80,88,108] | [10,12,31,33,37,40,41,42,43,49,50,59,61,66,68,71,73,75,81,89,93,94,95,110,113,117,122,126,135,144] | [10,11,27,28,50,57,58,59,63,65,67,70,80,90,91,92,94,95,110,111,118,119,121,124,126,129,130,136,137,138,145,146] | [29,52,69,83,84,87,96,97,114,118,128] |
| AlSi12 | [34] | [99,104,120] | [15,16,17,18,82,100,101,106,120] | - |
| A356 | - | - | [20] | - |
| A357 | - | [25,26,36,48,51] | [24,26,32,48,125] | [64] |
3. Mechanical Properties of SLM-Printed Aluminium Alloys
Characterisation of the mechanical properties of any additively manufactured part is generally very demanding. Although ASTM F3122-14 presents standard guidelines to evaluate most of the mechanical properties of 3D-printed metallic materials, there is no set standard developed for this purpose, making it difficult to benchmark and/or compare the properties of the same material printed using different AM printers with varying geometries. Therefore, extensive research has been published to characterize various types of mechanical properties of SLM processed Al alloys under static, dynamic, and heat treatment conditions. Table 3 is a compilation of the various mechanical properties investigated by researchers for four main types of SLM-printed aluminium alloys, namely AlSi10Mg, AlSi12, A356, and A357.
Table 3.
List of studies evaluating various mechanical properties of SLM-printed Aluminium alloys.
| Property | AlSi10Mg | AlSi12 | A356 | A357 |
|---|---|---|---|---|
| Microhardness | [50,52,53,58,66,68,70,73,76,77,79,86,92,107,111,112,126,129,130,137,145] | [45,131] | - | [125] |
| Nanohardness | [11,12,28,49,54] | - | - | - |
| Tensile | [4,10,11,12,30,33,42,43,44,49,53,58,63,65,67,68,70,71,72,73,76,78,80,81,85,88,89,90,92,98,103,107,109,112,113,117,118,119,121,122,124,126,128,129,130,132,136,138,144,146] | [15,17,18,55,74,101,104,115,120,131] | [20] | [24,25,26,32,36,48,51,64,125] |
| Compressive | [11,12,38,102,134] | - | - | - |
| Fatigue | [27,35,37,40,92,93,98,123,126,136,144] | [14,115,116,120] | - | [36] |
| Fracture Toughness | [40,43,49,53,59,66,73,89,90,92,112,118,122,126,132,144] | [55,120] | - | - |
| Dynamic | [61,62,89,95] | [99,100,147] | - | - |
| Creep Resistance | [108] | - | - | - |
| Impact | [103,107,110,127,135] | - | - | - |
| Wear | [47,86] | [106] | - | - |
| Flexural/Bending | [129,130] | [105] | - | - |
| Shear | - | - | - | [51] |
Table 3 shows that maximum research effort has been directed to investigate the tensile properties of SLM processed aluminium alloys. In most of these publications, effect of build orientation and heat treatment on microhardness, yield strength (YS) and ultimate tensile strength (UTS) has been studied. Many of these publications have also discussed the microstructure variation in the samples arising due to rapid heating and cooling encountered in the SLM process and relate them to the mechanical property relationships. Table 3 also reveals that some important mechanical properties such as quasi-static compression, dynamic (high strain rate), fatigue, impact, flexural and wear have received very little attention of researchers. These properties are of significance in many automotive, aerospace, and biomedical applications.
Heat treatment is one of the essential processes to achieve the desired property such as the ductility of the part produced by SLM. Ma et al. [148] have applied the heat treatment of hyper-eutectic alloy AlSi20 to investigate the mechanical properties as well as microstructure. In the heat treatment process, Si particles became coarser and the morphology changed from fibrous to plate like structure. Also, as anticipated, the changes in the microstructure during heat treatment affects the mechanical properties. A significant decrease in strength and, on the other hand, a very high increase in ductility were observed.
A detailed description of research carried out on each of the above-mentioned aluminium alloys is discussed below.
3.1. SLM-Printed AlSi10Mg
AlSi10Mg is one of the most common aluminium alloys and finds wide applications in various industries of 3D printing applications such as automotive and aerospace. The effect of build orientations in horizontal (H), inclined (I), and vertical (V) directions, and the effect of post heat treatment on the tensile mechanical properties of SLM-printed AlSi10Mg are summarized in Table 4. In most of the studies, the tensile samples built in horizontal direction on the build plate seem to provide higher tensile strength than the sample build in vertical direction. In most studies, it was observed that heat treated (HT) SLM samples display reduced tensile strength and increased ductility than the as-built (AB) SLM samples. Very few studies have been conducted to assess the effect of build orientation on heat treated SLM samples. Table 4 also presents results of some studies carried out on fatigue and fracture toughness of the SLM-built parts. Very few studies have been undertaken on flexural behaviour of the printed aluminium parts. Table 4 shows results of work carried out on the quasi-static and dynamic compression of SLM processed aluminium samples. Again, a great deal of studies are required to understand the quasi-static compression and high strain rate dynamic tensile and compressive behaviour of SLM-processed aluminium parts for different orientations and heat treatment conditions. Moreover, the mechanical performance of SLM-processed aluminium alloys operating at elevated temperatures have also not received the attention of researchers.
Table 4.
Mechanical properties of SLM-printed AlSi10Mg.
| Effect of Build Orientation: | |||||
| Build Orientation a | Hardness b | YS (MPa) | UTS (MPa) | Strain (%) | Reference |
| H, V | 109.7 (max) | 200 | 360 | 2 | [12] |
| H, I, V | - | 241.2 (H) | 379.6 (H) | 8.1 (H) | [33] |
| 239.1 (I) | 367.8 (I) | 5.7 (I) | |||
| 236.8 (V) | 351.8 (V) | 8.3 (V) | |||
| H, V | - | - | 338 (H) | - | [43] |
| - | 385 (V) | - | |||
| H, I, V | 130.6 (max) | 206.74 (0°,5°) | 366.43 (0°,5°) | - | [67] |
| 241.15 (0°, 5°) | 399.10 (0°, 5°) | - | |||
| 222.83 (0°, 85°) | 360.27 (0°, 85°) | - | |||
| 188.15 (45°, 0°) | 330.11 (45°, 0°) | - | |||
| 179.71 (45°, 5°) | 314.32 (45°, 5°) | - | |||
| 208.57 (90°, 45°) | 357.49 (90°, 45°) | - | |||
| H, V | - | - | 340 (H) | - | [81] |
| - | 350 (V) | - | |||
| H, V | 94 | 170 (H) (max) | 277 (H) (max) | - | [112] |
| 170 (V) (max) | 267 (V) (max) | - | |||
| H, V | - | 195 (H) | 338 (H) | 11.1 (H) | [113] |
| 187 (V) | 331 (V) | 11.5 (V) | |||
| H, V | - | 187 (H) | 284 (H) | - | [122] |
| 191 (V) | 274 (V) | - | |||
| H, I, V | - | - | 250 (H) | - | [68] |
| - | 190 (I) | - | |||
| - | 220 (V) | - | |||
| H, V | 127 (H) | - | 391 (H) | - | [4] |
| 86 (V) | - | 396 (V) | - | ||
| Effect of Heat Treatment: | |||||
| AB/HT c | Hardness | YS (MPa) | UTS (MPa) | Strain (%) | Reference |
| AB | - | 300 | 455 | 0.08 | [44] |
| AB | - | 224.3 | 349.5 | - | [53] |
| AB | - | - | 380 | - | [56] |
| AB | - | 265 | 375 | - | [124] |
| AB | - | - | 360 | 6 | [132] |
| AB | 1.52 GPa | 218 | 312 | 1.80 | [49] |
| AB | - | 240 | 360 | - | [78] |
| AB | 118 (Max) | 186 | 354 | - | [88] |
| AB | 2.098 GPa | 270 | 446 | 8.09 | [138] |
| AB | - | 248 (H) | 386 (H) | 8.6 (H) | [42] |
| 228 (V) | 412 (V) | 7 (V) | |||
| HT-T6 | 243 (H) | 323 (H) | 15.3 (H) | ||
| 223 (V) | 302 (V) | 16 (V) | |||
| HT-T5 | 321 (H) | 471 (H) | 8.6 (H) | ||
| 292 (V) | 493 (V) | 6 (V) | |||
| AB | 140.7 | 255 | 377 | - | [58] |
| SR | 158 | 256 | - | ||
| HT-T6 | 210 | 284 | - | ||
| AB | 123 | 200 | 400 | - | [63] |
| HT | 51 | 100 | 150 | - | |
| AB | 127 | - | 307 | - | [70] |
| HT | - | 382 (max) | - | ||
| AB | 136 | - | 396 | - | [76] |
| HT | 152 | - | 399 | - | |
| AB | 132 | - | 434 | - | [80] |
| HT | 95 | - | 168 | - | |
| AB | - | - | 434 | - | [10] |
| HT | - | 200 | - | ||
| AB | - | - | 470 | - | [92] |
| HT | - | 160 | - | ||
| HT-T2 | 53 HB (max) | 105 | 171 | - | [130] |
| HT-T6 | 100 | 239 | 333 | 4.50 | [11] |
| HT | 143.33 | - | 499 | - | [72] |
| Quasi-static and Dynamic Compressive Properties: | |||||
| QS/D d | UCS (MPa) | YS (MPa) | Strain (%) | Reference | |
| QS-C | 560 | 350 | 10 | [38] | |
| D-C | 590 | - | 0.3 | [94] | |
| D-C | 700 | - | 0.13 | [61] | |
| Fatigue and Bending Properties: | |||||
| Other tests e | Fatigue Strength/No. of cycles | Fracture Toughness (MPa.m0.5) | Reference | ||
| AF, FT | 3 × 107 | 99 (max) | [27] | ||
| RB | 5 × 107 | - | [40] | ||
| AF, FT | 3 × 107 | 94 | [91] | ||
| AF, FT | 107 at 125 MPa | 37.4 | [126] | ||
| AF, FT | 120 MPa | 27 | [136] | ||
| AF | 100 MPa (max) | - | [123] | ||
| FT (at build orientations) | - | 59.06 (0°, 5°) | [66] | ||
| - | 51.60 (0°, 5°) | ||||
| - | 58.03 (0°, 85°) | ||||
| - | 55.79 (45°, 0°) | ||||
| - | 50.76 (45°, 5°) | ||||
| - | 40.63 (90°, 45°) | ||||
Key:a—H (Horizontal), I (Inclined at 45°), V (Vertical); b—Measurements reported in HV (Vickers Hardness), unless otherwise specified differently; c—AB (As-built), SR (Stress Relief), HT (Heat-treated); d—QS (Quasi-static testing), D-T (Dynamic-Tension testing), D-C (Dynamic-Compression testing); e—AF (Axial Fatigue), RB (Rotating Bending), FT (Fracture Toughness).
According to Aboulkhair et al. [149], when the process parameters and scan strategy were optimised, it would affect the density of AlSi10Mg parts produced by SLM directly. Therefore, the porosity component was evaluated, and the part was found to be 99.8% dense. In a study by Read et al. [108], the mechanical properties of the SLM built AlSi10Mg samples were found to perform better than as-cast alloys of the same composition. The mechanical properties tested were tensile strength, creep, and the porosity. Similarly, Li et al. [80] reported that the solution treatment of as-built AlSi10Mg samples produced by SLM yielded better ductility (from 5% to 24% approximately), while the tensile strength was significantly reduced from 434 MPa to 168 MPa approximately. Li et al. [81] investigated the as-built SLM AlSi10Mg samples and tested them at −70 °C for mechanical properties. The fish-scale morphology along the build direction and oval structures on the direction perpendicular to the build direction were observed.
A study by Hitzler et al. [68] focused on the anisotropic compressive behaviour of SLM AlSi10Mg. They found that compressive Young’s modulus was significantly higher than the Young’s modulus of tensile loading as well as Young’s modulus of bulk base material. The compressive Young’s modulus found to be about 82 GPa. Furthermore, they reported that the compressive yield strength was found to be similar to tensile yield strength, however the ultimate compressive strength was obtained to be significantly higher than the tensile strength.
Wang et al. [150] studied the effect of energy density on densification behaviour and surface roughness of SLM AlSi10Mg. The densification behaviour was analysed using X-ray and CT scanning. High relative density was obtained through the point distance of 80–105 µm with an exposure time of 140–160 µs. Furthermore, energy density was stated to have a significant influence on the surface morphology. On one hand, the increased energy density could lead to a balling defect and, on the other hand, reduced energy density could cause defects, such as porosity and micro-cracks.
Everitt et al. [54] investigated the hardness through nano-indentation and found that AlSi10Mg samples produced by SLM have higher hardness than cast counterpart. Furthermore, the microstructural studies revealed that grain sizes were increased at the melt pool edges, which were associated with the homogenous distribution of Si particles throughout the sample.
A study by Leon and Aghion [151] evaluated the effect of surface roughness on SLM processed AlSi10Mg followed by stress-relief heat treatment. They focused on corrosion resistance and corrosion fatigue performance. Furthermore, the results of SLM processed AlSi10Mg samples were compared with the cast counterparts. Polishing was found to improve the corrosion fatigue life span of SLM samples, whereas the unpolished SLM samples caused an increase in surface roughness and other surface defects.
Ch et al. [43] studied the SLM AlSi10Mg alloy under two different environments namely argon and nitrogen, while building the parts in both horizontal and vertical orientations. Their microstructural findings include cellular structure showing α-Al matrix displaying Al and Si eutectic mixture. Tensile strengths were found to be 385 MPa and 338 MPa for the nitrogen and argon atmosphere respectively. Furthermore, the samples built in the horizontal orientation showed a variation of about 5% in the nitrogen environment, whereas in the vertical orientation, 7.5% variation of strength was found. Based on their findings, nitrogen was inferred to have preference over argon as the shielding gas.
Takata et al. [121] studied the microstructure and mechanical properties of SLM processed AlSi10Mg samples heat treated at temperatures 300 °C and 500 °C. They reported that, at elevated temperatures, fine Si phase precipitation occurred resulting in coarse eutectic Si particles. The as-built part was found to exhibit a tensile strength of 480 MPa. Furthermore, the tensile strength was reported to be isotropic, whereas the tensile ductility was found to be anisotropic. Even, the anisotropic property was found to disappear at a heat-treated temperature of 530 °C.
Girelli et al. [152] investigated the effect of temperature, solution treatment, and ageing on the microstructure, microhardness, and density of SLM AlSi10Mg. They also investigated the AlSi10Mg samples produced by gravity casting under the same heat treatment conditions. The as-built SLM samples were said to exhibit superior mechanical properties than gravity casted samples due to the refinement of grains and nano-sized Si particles. The as-built AlSi10Mg samples had a fine microstructure and the heat treatment was found to decrease the ultimate tensile strength but not the yield strength.
Liu et al. [85] investigated the as-built AlSi10Mg samples produced by SLM and reported the issues with respect to surface roughness and mechanical properties. Sandblasting had shown a difference of 80% in surface roughness values. Furthermore, the results of tensile tests revealed superior outcome than the die-cast counterparts. A similar behaviour was found in terms of hardness and density.
In a study by Raus et al. [107], mechanical properties namely microhardness, tensile strength and impact toughness were investigated. The results were then compared with conventional high pressure die cast A360 alloy. The results revealed that microhardness and yield strength were higher for the SLM AlSi10Mg by 42% and 31% respectively than the die cast counterparts. They used the SLM process parameters as laser power of 350 W, scanning speed of 1650 mm/s, and hatching distance of 0.13 mm to attain the part density of 99.13%.
Recently, Hadadzadeh et al. [61] studied the strain rate behaviour for AlSi10Mg alloy processed by SLM under dynamic loading in two build orientations, one horizontal and the other being vertical. The strain rate was said to increase rapidly in both the cases, while the strain rate at vertical orientation was ~1400 s−1. Both the flow stresses follow a similar trend, whereas the flow stress in the vertical orientation were stated to progress further with increase in strain.
Nurel et al. [95] have also reported the dynamic properties of SLM processed AlSi10Mg at strain rates of 7 × 102–8 × 103 s−1 using SHPB. The SLM AlSi10Mg was found to have been affected by build orientation and heat treatment. They also investigated the anisotropic nature of SLM parts using ellipticity after the SHPB tests, but they have not observed any strain rate sensitivity. The focus of this research was on the significance of the build orientation at different strain rates. No significant correlation of build orientation with respect to strain rate was found in the range of 1000–3000 s−1.
Asgari et al. [31] have also investigated the dynamic behaviour and texture of AlSi10Mg with build plate heating at 200 °C. Their findings showed that, in vertically built SLM samples, shock loading did not have an influence on texture and in horizontally built samples, transition of texture was observed (at a strain rate of 1600 s−1). The dynamic mechanical behaviour was investigated using split Hopkinson pressure bar at a strain rate ranging from 150 s−1 to 1600 s−1.
Trevisan et al. [10] reviewed the process, microstructure and mechanical properties of SLM AlSi10Mg. The focus was on mechanical properties coupled with very fine microstructure, which is primarily due to rapid melting of AlSi10Mg powder and fast solidification. The review analysed the effect of main process parameters, namely laser power, scan speed, layer thickness, and scan strategy. In addition, the effect of heat treatment on tensile as well as fatigue properties associated with the SLM AlSi10Mg samples were discussed.
3.2. SLM-Printed AlSi12
The AlSi12 alloy is increasingly gaining focus because it is a near eutectic alloy characterised by good casting ability and high specific strength. The low melting point of this alloy provides good castability due to its low density and good wear properties, AlSi12 is quite attractive for applications in automotive and aerospace industries. It can be used for cryogenic applications as it can retain its strength at low temperatures such as at high altitudes [106]. The mechanical properties of SLM-printed AlSi12 are summarized in Table 5. It is noted that SLM processed AlSi12 alloy has received less attention for mechanical characterization compared to AlSi10Mg alloy in terms of heat treatment and build orientation effects. Most of the comments mentioned earlier concerning the need for further research on different properties mentioned for the AlSi10Mg alloy also apply for SLM printed AlSi12 alloy.
Table 5.
Mechanical properties of SLM-printed AlSi12.
| Effect of Build Orientations: | |||||
| Build Orientation a | Hardness b | YS (MPa) | UTS (MPa) | Strain (%) | Reference |
| H, V | - | 270 (H) | 325 (H) | 4.4 (H) | [120] |
| 274 (V) | 296 (V) | 2.2 (V) | |||
| H, I, V | - | 227 (H) | 260 (H) | 2.0 (H) | [104] |
| 263 (I) | 367 (I) | 4.5 (I) | |||
| 224 (V) | 398 (V) | 5.0 (V) | |||
| Effect of Heat Treatment: | |||||
| AB/HT c | Hardness b | YS (MPa) | UTS (MPa) | Strain (%) | Reference |
| AB | - | 290 | 460 | - | [101] |
| AB | - | 263 | 365 | - | [104] |
| AB | - | 201 | 361 | 4 | [116] |
| AB | 115 | 224 (max) | 368 (max) | 4.8 | [131] |
| AB | - | 240 | 325 | - | [18] |
| HT | 138 | 207 | - | ||
| AB | - | 220 | 418 | 3.9 | [15] |
| HT | 218 | 372 | 3.4 | ||
| HT | - | 102 | 425 | 12 | [55] |
| Dynamic Compressive Properties: | |||||
| QS/D d | UTS (MPa) | UCS (MPa) | YS (MPa) | Strain (%) | Reference |
| D-C at RT | - | 550 | 400 | 0.18 | [99] |
| D-C at 200 °C | - | 490 | 270 | 0.18 | [147] |
| Fatigue and Fracture Toughness: | |||||
| Other tests e | Fatigue Strength/No. of cycles | Fracture Toughness (MPa.m0.5) | Reference | ||
| AF | 109 at 60.5 ± 4.7 MPa | - | [15] | ||
| FT | - | 19.7 | [120] | ||
Key:a—H (Horizontal), I (Inclined at 45°), V (Vertical); b—Measurements reported in HV (Vickers Hardness), unless otherwise specified differently; c—AB (As-built), HT (Heat-treated); d—QS (Quasi-static testing), D-C (Dynamic-Compression testing); e—AF (Axial Fatigue), FT (Fracture Toughness).
Siddique [14,115] reported that in automotive and aerospace industries, there is trend to replace cast iron with Al-Si alloys to achieve light weighting in components such as engine blocks, cylinder heads, pistons, power trains, and intake manifolds. Many of these parts are moving and operating under dynamic loading conditions with elevated temperatures. Therefore, extensive work needs to be done to understand the mechanical behaviour of Al-Si alloys processed by SLM under dynamic loading, impact, wear, and elevated temperature conditions.
Prashanth et al. [17] investigated mechanical behaviour of SLM AlSi12 and reported that the yield strength and tensile strength were 260 MPa and 380 MPa respectively. The effect of annealing on the microstructure and on the tensile properties revealed that mechanical properties could be fine-tuned, and wide range of strength and ductility could be achieved. In another study, Prashanth et al. [16] evaluated the effect of annealing on tribological and corrosion properties of SLM processed AlSi10Mg through sliding and fretting wear tests. The sliding wear showed less wear rate when compared to the cast parts. The studies revealed that wear properties and corrosion behaviours have a correlation with each other, as both are strongly associated with a change in microstructure. The change in microstructure was due to the heat treatment, as the Si particles grow, and the density decreases with increasing annealing temperature.
In another investigation, Prashanth et al. [153] carried out compression tests on both AlSi12– Titanium, Niobium, and Molybdenum (TNM) composites and AlSi12 matrix produced by SLM and studied their behaviour. The compression tests revealed that TNM composites–AlSi12 matrix had significantly better compressive strength when compared to the AlSi12 matrix. However, the TNM composites had revealed less plasticity. Prashanth et al. [101] also analysed the tensile behaviour of SLM AlSi12, where they applied the base plate heating and four different hatch styles. The samples showed similar crystallite sizes but different textures. In addition, the samples produced with base plate heating had lesser residual stress. The results reported were the yield strength ranging between 235 MPa and 290 MPa, while the ultimate tensile strength varied between 385 MPa and 460 MPa. Furthermore, the ductility varied between 2.8% to 4.5%. Since the base plate heating produced desirable results, they carried out base plate heating at three different temperatures namely 473 K, 573 K, and 673 K, which yielded the tensile ductility of 3.5%, ~3%, and 9.5% respectively.
Siddique et al. [116] used the computer tomography for investigating the fatigue performance of SLM AlSi12 samples. The samples revealed better or at least comparable yield strength or ultimate tensile strength when compared to cast parts. Surface roughness was found to affect the fatigue strength, which was improved by post processing. Furthermore, a porosity study was essential to employ the samples for high cycle applications. The computer tomography was applied to study the stress concentration due to porosity. In another study Siddique et al. [15] determined the effect of process parameters and post processing on the microstructure and mechanical properties of SLM processed AlSi12. They performed quasi-static tests and fatigue tests for mechanical characterisation. Furthermore, they observed extra-ordinary eutectic microstructure using scanning electron microscope. By changing the build rate and keeping the process in control, mechanical properties obtained were found to be better for SLM parts than cast counterparts. Moreover, Siddique et al. [14] focused on the design considerations and mechanical properties of SLM processed AlSi12 parts. From the application perspective, the parts were designed to perform in the high cycle environment. Therefore, the study was more focused on very high cycle fatigue and the corresponding crack propagation behaviour in the cyclic environment. They further investigated the base plate heating and post processing, especially stress relieving, which are critical for the fatigue loading of AlSi12 parts. The base plate heating was found to influence the fatigue crack initiation mechanisms.
Wang et al. [131] studied the effect of build chamber atmosphere on the SLM AlSi12 samples. The effect of three different atmosphere namely argon, nitrogen and helium were studied for their influence on the mechanical properties. Hardness, density, and relative density were analysed and found to have similar attributes for all the atmospheres. However, the mechanical properties of parts produced in argon and nitrogen atmospheres were found to be better than the helium atmosphere. Furthermore, the mechanical properties in SLM parts were better than those produced by conventionally made AlSi12 counterparts.
Lykov and Baitimerov [154] investigated the SLM AlSi12 to determine the process parameters to ensure the least porosity. The samples were found to have varied microstructures and the porosity was reported to be about 0.5%. The AlSi12 powders were found to have poor flowability. The surface morphology revealed that samples have an uneven surface. They recommended that to reduce the surface roughness and porosity, it was essential to use AlSi12 powder with fine fraction of about 17 µm and the scanning strategy include double pass laser scan strategy.
Mendřický and Keller [155] focused on the precision, geometry and dimensional accuracy of the AlSi12 parts produced by SLM. The part orientation was planned to minimise the internal stress. The SLM part was digitised to collect the sample data. The collected data was compared with the CAD data to evaluate for dimensional and geometrical accuracy. The deformation of the model was caused by the internal stress on the as-built AlSi12 parts.
Šafka et al. [156] analysed the build orientation and the placement of part in the SLM build substrate, which could reduce the amount of support structures required and improve the flexural strength of SLM AlSi12 parts. They observed that the least energy and therefore less heat would lead to little deformation of the printed final part.
Chou et al. [45] proposed a new approach of using pulsed SLM over the conventional SLM for AlSi12 and achieved greater control of the heat input. In the SLM AlSi12, Si refinement below 200 nm was attained. Furthermore, 95% of dense parts and the hardness of 135 HV were achieved. The part produced by pulsed SLM method yielded better hardness than the conventional cast alloy counterpart. The cooling rate and thermal gradient had an influence on solidification phase and the microstructure.
In a study by Vora et al. [13], a novel method had been discussed to produce aluminium parts with the anchorless SLM. This anchorless method is opposed to the regular method that uses anchor or support for the SLM parts. Furthermore, the anchorless SLM (ASLM) could produce SLM parts that can remain in the stress-free state. The ASLM was found to be suitable for processing eutectic alloys, as well as hypo eutectic and hyper eutectic alloys. In addition, they studied the in-situ alloy formation within SLM chamber. The residual stress was also found to be less with the ASLM processed AlSi12 alloy.
Suryawanshi [120] investigated the tensile strength and toughness of SLM AlSi12 and found that mechanical properties were relatively better than the cast counterparts, except the ductility. The scan strategy especially linear vs checker-board hatch style was analysed and the later was found to have significant effect on the tensile strength. Furthermore, the meso-structure due to the laser hatch tracking leads to improved fracture toughness. In addition, to attain higher fatigue strength, the residual stresses, porosity, and un-melted powder particles needed to be removed. The SLM AlSi12 was found to give more avenues for material design and fabrication with enhanced strength and toughness.
In a study by Li et al. [82], the SLM AlSi12 was reported to have controllable and ultrafine microstructure. The excellent mechanical properties were achieved through solution heat treatment. They introduced a novel approach for refining the eutectic alloy of AlSi12, which yielded better tensile properties than cast counterparts. The solution treated AlSi12 was found to produce the tensile ductility of ~25%. Furthermore, the tailoring of the mechanical properties according to the applications was possible by controlling the solution heat treatment time.
Louvis et al. [8] investigated the process parameters of SLM AlSi12 to achieve uniform relative density. The process parameters investigated were laser power and the laser scanning rate. The investigation was extended to understand the difficulty of processing AlSi12 when compared to stainless steel and titanium alloy. The major factor that affected the relative density was the oxidation factor. The process parameters were varied using two different SLM machines, one with 50 W laser power and the other with 100 W laser power. Even with the optimum process parameters combination, the machine with 100 W laser power yielded only the relative density of 89.5%. Furthermore, it was recommended that to produce SLM AlSi12 parts with 100% relative density, it was essential to develop methods to disrupt the oxide formation or to prevent oxidation.
Ackermann et al. [157] studied the fabrication of thin structures and their applications using SLM AlSi12 parts. In service, the applications of SLM AlSi12 parts were found on microelectronics, fine mechanical structures, and automotive mechanisms. The powder characteristics such as mean particle size and powder shape, the process parameters such as laser spot size and scanning speed were found to influence the thickness of fine structures. They arrived at 0.21 mm as the optimum thickness for thin structures, for sufficient strength.
Rathod et al. [106] investigated the effect of scanning strategy and heat treatment on the tribological properties of the SLM AlSi12 parts and compared with cast alloy. The process of annealing lead to Si precipitation resulting in the reduction of hardness. The as-built AlSi12 SLM samples were reported to have less wear rate when compared to heat treated SLM samples and cast samples.
3.3. SLM-Printed A356 and A357
There are two other types of Al-Si alloys, A356 and A357, which have been processed by SLM. These two alloys are also Al-Si-Mg alloys. They both contain 7%Si by weight, but they have a slightly different Mg content. The alloy A356 is AlSi7Mg0.3 and alloy A357 is AlSi7Mg0.7. Very few studies have been made on mechanical characterisation of these two alloys processed by SLM. The mechanical properties of SLM-printed A356 and A357 are summarized in Table 6.
Table 6.
Mechanical properties of SLM-printed A356 and A357.
| Effect of Build Orientation: | |||||
| Build Orientation a | Hardness b | YS (MPa) | UTS (MPa) | Strain (%) | Reference |
| H, V | - | 257 (H) | 398 (H) | 4.4 | [48] |
| 216 (V) | 400 (V) | 2.2 | |||
| H, I, V | - | 184 (H) | 284 (H) | - | [51] |
| - | 195 (I) | 298 (I) | - | ||
| - | 192 (V) | 305 (V) | - | ||
| Effect of Heat Treatment: | |||||
| AB/HT c | Hardness b | YS (MPa) | UTS (MPa) | Strain (%) | Reference |
| AB * | - | 250 | 400 | - | [20] |
| HT–T5 * | - | 125 | 200 | - | |
| AB | - | 279 | 426 | - | [25] |
| HT | 205 | 307 | - | ||
| AB | - | 279 | 426 | - | [24] |
| SR | - | 165 | 240 | - | |
| AB | - | 225 | 375 | - | [26] |
| SR | - | 125 | 220 | - | |
| HT–T6 | 138 | 200 | 400 | 5.5 | [32] |
| Fatigue and Fracture Toughness: | |||||
| Other tests d | Fatigue Strength/No. of cycles | Fracture Toughness (MPa.m0.5) | Reference | ||
| AF | 2 × 106 at 60 MPa | - | [36] | ||
Key:a—H (Horizontal), I (Inclined at 45°), V (Vertical); b—Measurements reported in HV (Vickers Hardness), unless otherwise specified differently; c—AB (As-built), HT (Heat-treated), SR (Stress Relief); d—AF (Axial Fatigue), FT (Fracture Toughness); *—A356 alloy.
Kimura and Nakamoto [20] optimised process parameters to arrive at dense SLM A356 (AlSi7Mg0.3). The relative density attained was 99.8% with the laser irradiation conditions. The mechanical test results found the ultimate tensile strength of ~400 MPa, the yield strength of ~200 MPa and the elongation from 12–17%. The heat treatment revealed the difference in microstructure and mechanical properties of SLM A356 samples and as-cast samples. After annealing, the SLM samples became elongated to 30%, while the tensile strength of A356 samples reduced by half the value and became ~200 MPa.
Rao et al. [25] investigated the mechanical properties and microstructure of SLM A357. The processing parameters were optimised to achieve dense A357 samples, along with fine microstructure. The porosity was also analysed based on relative density and laser parameters. The anisotropy of SLM A357 Al alloy samples were investigated in the horizontal and vertically built tensile samples. Fractographic studies revealed that horizontal orientation was better for printing the A357 tensile samples. In another study Rao et al. [24], the tensile behaviour of SLM A357 in the as-built and heat treated condition was investigated. The as-built sample displayed ultrafine microstructure. The tensile samples of SLM A357 were found to have better properties than their cast counterparts. The Al grains in the as-built parts had eutectic nano-sized Si particles, contributing for higher strength. However, the nano-sized Si particles did not favour the ductility. After the heat treatment of SLM A357, as anticipated, the tensile ductility improved and was reported to be about 23% with reduced tensile strength.
Yang et al. [26] investigated the effect of heat treatment on SLM A357 by focusing on stress relief to analyse the mechanical property and microstructure. For the as-built A357 samples, the rapid melting and rapid cooling affects the intermetallic phases such as Mg2Si precipitates. During the heat treatment process, the breaking up of the Si network was said to occur, which lead to high ductility. Si particles at grain boundaries were observed to coarsen. Furthermore, anisotropy was observed to disappear in terms of affecting yield strength and ductility when the microstructure became more homogenised.
3.4. Other Aluminium Alloys Processed Using SLM
From the research perspective and for the applications with desired mechanical properties, new Aluminium alloy are being developed and processed using SLM. These new aluminium alloys have been developed by alloying them with new elements, such as Cu, Ni, Sc, Zr, V, and Zn, to impart improved properties and better processing by SLM.
Aversa et al. [158] developed Al-Si-Ni alloy samples for SLM with a combination of AlSi10Mg and Ni powders. This combination was found to be near eutectic by composition. Furthermore, this combination of AlSi10Mg and Ni were reported to have better hardness than AlSi10Mg. The increase in hardness was mainly attributed to the addition of Ni, which was demonstrated through nano-indentation measurements. The SLM process parameters were optimised to reduce porosity. The results obtained with the combination of AlSi10Mg and Ni had also yielded Al3Ni agglomerates.
Spierings et al. [159] developed Sc and Zr-modified AlMg alloys for SLM processing. The Sc and Zr-modified Al alloy is commercially known as “Scalmalloy” and offers more advantages over traditional 4xxx as-cast alloys. These advantages include high strength and high ductility at low anisotropy. Furthermore, fine grain microstructure and weak texture along the build direction causes low anisotropy. They also analysed the influence of larger scan speeds on the mechanical properties of Scalmalloy and found that grain sizes were reduced from 1.1 µm to 600 nm.
Zhang et al. [160] investigated the manufacturing of Al-Cu-Mg alloys using SLM. They studied the effect of process parameters on the density of SLM Al-Cu-Mg alloys. The energy density was found to have significant influence on the densification of Al-Cu-Mg alloys. The threshold value of energy density was 340 J/mm3, that yielded the sample density of 99.8%. Furthermore, fine microstructure was obtained without any imperfections and micro-cracks. A high value of ultimate tensile strength of ~400 MPa and the yield strength of ~275 MPa were obtained for the SLM Al alloy part. In addition, they found fine grains and solid solution strengthening mechanism for the higher mechanical strength. In another study, Zhang et al. [161] investigated the microstructure and mechanical behaviour of SLM Al-Cu-Mg alloy and Zirconium modified SLM Al-Cu-Mg alloys. The addition of Zr had the effect of reducing the hot cracking in the SLM part. The comparison of Zr modified Al-Cu-Mg alloy and Al-Cu-Mg alloy was found to show an ultrafine grain with Zr addition. Furthermore, Zr modified Al alloy had significantly higher yield strength close to its ultimate tensile strength of ~450 MPa.
Nie et al. [162] studied the effect of Zr on the formability, mechanical properties and microstructure of SLM Al-Cu-Mg-Mn alloys. The addition of Zr to SLM Al-Cu-Mg-Mn alloy was observed to be effective in crack controlling mechanism, grain refinement and in the controlling of mechanical properties. The addition of Zr was found to cause the transformation of grain type from columnar to equiaxed type. Furthermore, they investigated crack inhibition and enhancement of mechanical properties due to the addition of Zr with SLM Al alloy.
Karg et al. [163] investigated the laser beam melting of EN AW-2219 and observed that laser processing of EN AW-2219 (Al-Cu alloys) was very challenging. Porosity and tensile tests were conducted for the SLM Al-Cu alloy. Then, T6 heat treatment was applied to some built samples and the elongation was observed. The elongation was found to exceed in the build direction by a factor of two when compared to traditional cast counterpart.
Martin et al. [164] stated that several types of aluminium alloys cannot be processed using SLM due to the complex melting and solidification dynamics. The issues were found to be microstructures with larger columnar grains and periodic cracks. However, they suggested methods to resolve these issues by introducing nanoparticles that would control the solidification. Then the powder particles were found to be qualified for SLM. Furthermore, the technique of solidification control could be applied for the conventional process as well, where hot cracking and hot tearing occurs commonly.
Montero-Sistiaga et al. [9] studied the SLM Al7075 (Al-Zn-Cu-Mg), a wrought alloy, to improve its density. The SLM Al7075 initially displayed poor density and micro-cracking, but it was improved by adding 4% Si. Heat treatment was carried out to improve the hardness of SLM Al7075. Furthermore, the focus was more on producing high strength aluminium alloys.
Aversa et al. [165] investigated the mechanical, metallurgical and the thermal properties for SLM of Al-Si-Zn-Mg-Cu alloy. The introduction of Si was analysed with respect to Al-Zn-Mg-Cu alloy and the crack density was found to be reduced. This crack density reduction was due to improved molten phase fluidity and the reduction of the co-efficient of thermal expansion. Furthermore, the SLM Al-Si-Zn-Mg-Cu alloy was found to be promising in terms of microstructure, microhardness, and the tensile properties.
Zheng et al. [166] reported the variation of microstructure and hardness of an SLM Al-8.5Fe-1.3V-1.7Si. Among the melt pool, three different zones namely laser melted zone, melting pool border and heat affected zone were identified. Microhardness results of the SLM process exceeded the as-cast counterpart. Furthermore, with the decrease in laser scanning speed, laser melted zone was found to reduce significantly.
Croteau et al. [167] investigated the microstructure and mechanical properties of SLM Al-Mg-Zr alloys. The energy densities applied for the fabrication of SLM parts ranged between 123 and 247 J/mm3 and the resultant relative density was verified using X-ray tomography. The alloying elements have a significant role, where Mg acted as a solid solution strengthener and Zr contributed towards metastable precipitates resulting in grain refinement and prevention of hot tearing. Furthermore, Zr alloy had improved the mechanical properties.
In a study by Maamoun et al. [88], the influence of process parameters of SLM AA 6061 and AlSi10Mg were investigated, based on the relation between microstructure and mechanical properties. AA 6061 is also an Al-Si-Mg alloy with a higher coefficient of thermal expansion (CTE). The process optimisation was carried out on both the aluminium alloys to reduce the defect in microstructure. The mechanical behaviour of the aluminium alloys was analysed through the design of experiments and the results were presented for hardness, yield strength and ultimate tensile strength. The results obtained was useful in improving the part quality that had reduced the post processing requirements.
Uddin et al. [168] analysed AA 6061 using high temperature heating in an SLM environment to yield crack-free parts. The hardness was found to be 54 HV, the yield strength as 60 MPa, ultimate tensile strength of 130 MPa and the elongation of 15%. Furthermore, they revealed that AA 6061 could be successfully manufactured with SLM without displaying the cracking phenomenon.
4. Summary and Research Gaps
Although aluminium can be with Zn, Cu, Mg, Mn, and Si to produce age-hardening alloys, casting alloys, and work-hardening alloys, the area of focus in this review was the Al-Si alloys processed by selective laser melting (SLM) metal additive manufacturing technique and their mechanical properties. The Al-Si alloy has the cast-ability and weldability, which forms the unique combination and a suitable candidate for processing in SLM. As mentioned, the most common SLM aluminium alloys are AlSi10Mg and AlSi12 based on the literature review. This review has focused on classification of published research on SLM-processed aluminium alloys in terms of research carried out on the effects of process optimisation, build orientation and heat treatment on four main types of Al-Si aluminium alloys. The published papers have also been categorised for various types of mechanical properties considered in SLM parts to identify research gaps on which mechanical properties needs more in-depth investigation from the point of view of industrial applications.
This review has revealed that even though many studies are reported for the tensile mechanical properties of SLM aluminium alloys, very few studies were carried out on the dynamic behaviour in tension and compression, fatigue, impact, wear, and flexural response of the printed parts. Specially very few studies were published on high strain rate loading behaviour of parts made by any metal based additive manufacturing processes like DMD, EBM, and SLM.
One of the other research gaps found in this review is the effect of build orientations on the quasi-static and dynamic compression properties of SLM-processed various other aluminium alloys. It was also observed that some important mechanical properties such as fatigue, impact, flexural, bending, and wear have received very little attention. Moreover, the mechanical performance of SLM-processed aluminium alloys operating at elevated temperatures has also not received much attention. These properties are of significance in many automotive, aerospace, and biomedical applications.
Another important research avenue is to understand the effect of machine-specific characteristics on the properties of the printed components. It was found in this review that researchers have used different SLM machines supplied by various machine manufacturers globally. It is interesting that the same material when printed using different machines yield different mechanical and microstructural characteristics. This can be attributed to the differences in the laser systems used, inherent characteristics of the machine itself, and various other parameters which are not quite understood. Moreover, the repeatability of the mechanical performance of printed parts using same and/or different machines is to be further explored.
Lastly, the post heat treatment plays a crucial role in tuning the microstructural characteristics of the printed parts and render them suitable for desired applications. Most researchers have investigated the heat treatment protocol typically used for conventionally fabricated aluminium alloys, which may not be ideal for SLM-printed parts, as they have different inherent properties. Therefore, further research is required to be carried out to assess the effects of different heat treatment strategies on the performance of printed parts.
Acknowledgments
This research project was supported by DMTC Limited (Australia). The paper has been written in line with the intellectual property rights granted to research partners from the original DMTC project.
Author Contributions
Conceptualization, S.H.M. and R.A.R.R.; formal analysis, P.P.; data curation, P.P. and R.A.R.R.; writing—original draft preparation, P.P. and R.A.R.R.; writing—review and editing, R.A.R.R., S.H.M., D.R., and S.P.; supervision, S.H.M., D.R., and S.P.; project administration, S.P.; funding acquisition, S.P. All authors have read and agreed to the published version of the manuscript.
Funding
This research was funded by Defence Materials Technology Centre (DMTC) Limited, Project 5.01.
Conflicts of Interest
The authors declare no conflict of interest.
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