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. 2021 Mar 3;16(3):e0247599. doi: 10.1371/journal.pone.0247599

Investigation on cement-improved phyllite based on the vertical vibration compaction method

Yingjun Jiang 1,#, Jiangtao Fan 1,*,#, Yong Yi 1,, Tian Tian 1,, Kejia Yuan 1, Changqing Deng 1
Editor: Ahmed Mancy Mosa2
PMCID: PMC7928446  PMID: 33657170

Abstract

The vertical vibration compaction method (VVCM), heavy compaction method and static pressure method were used to form phyllite specimens with different degrees of weathering. The influence of cement content, compactness, and compaction method on the mechanical properties of phyllite was studied. The mechanical properties of phyllite was evaluated in terms of unconfined compressive strength (Rc) and modulus of resilience (Ec). Further, test roads were paved along an expressway in China to demonstrate the feasibility of the highly weathered phyllite improvement technology. Results show that unweathered phyllite can be used as subgrade filler. In spite of increasing compactness, phyllite with a higher degree of weathering cannot meet the requirements for subgrade filler. With increasing cement content, Rc and Ec of the improved phyllite increases linearly. Rc and Ec increase by at least 15% and 17%, respectively, for every 1% increase in cement content and by at least 10% and 6%, respectively, for every 1% increase in compactness. The higher the degree of weathering of phyllite, the greater the degree of improvement of its mechanical properties.

1. Introduction

The Qinba mountainous area of southern Shaanxi is rich in phyllite. But because phyllite is a kind of soft rock with low strength, poor stability and fragility [15], its unconfined compressive strength (Rc) and modulus of resilience (Ec) cannot meet the current subgrade design specifications. Therefore, it is not suitable for subgrade filling [69]. However, because of the lack of suitable fillers for subgrade filling along the line coupled with the inconvenience and difficulties in transportation in mountainous areas, projects in this region are compelled to use phyllite spoils for subgrade filling [10]. Local sourcing of materials and use of phyllite spoils as subgrade fillers will not only reduce the project cost and protect limited land resources, but also minimize the damage to the surrounding environment [1114].

The feasibility of using phyllite as subgrade filler was explored in many domestic and international studies. Based on the research and analysis of the basic mineral composition, strength, and compaction characteristics of weathered soft rock, initially, the feasibility of using weathered soft rock to fill the subgrade was determined, and a preliminary determination method was proposed [1519]. Yang et al. discussed the standard of soft rock as a filler and studied the influence of the weathering degree and rock structure on weathered soft rock through rock strength test and particle-breaking test [20]. In related work, the physical and mechanical properties of phyllite and determined the engineering characteristics such as the mineral composition and mechanical strength of phyllite [2124]. Xiong and Xu conducted an experimental study on the water content and particle size distribution of weathered phyllite subgrade and concluded that phyllite-filled subgrade can meet the requirements for the stable settlement of the subgrade and the sharp drop in strength after the immersion of phyllite. Thus, the feasibility of using phyllite as one of the important bases for subgrade filling was established [25]. Experimental research on phyllite under different pressure levels showed that the pressure level of 600 kPa can meet the requirements of subgrade filling [26]. The improved filling technology of phyllite subgrade was studied in combination with the field test section, and it was found that after the road performance was greatly improved after phyllite was mixed with cement, thus fully meeting the requirements of subgrade filling, and hence, it can be regarded as qualified subgrade filling [6]. Zhu studied the gradation, strength, compaction characteristics, and CBR (California bearing ratio) of phyllite before and after improvement and concluded that phyllite can be used as subgrade filler after improvement [27]. Cen compared and analyzed the test situation of improving the phyllite subgrade with cements of different grades. It was discovered that the weathered phyllite improved by adding 3% cement can not only ensure the quality of highway subgrade engineering, but also save investment and reduce construction costs [1]. Vazquez used cement and lime to improve the phyllite and compared the strength characteristics and improvement effects of the two improved phyllite [28]. Mark added phyllite during the process of mixing cement concrete and studied the strength characteristics and growth law of concrete specimens [2]. Based on indoor classification, compaction, and bearing ratio tests, Gidigasu found that phyllite did not meet the specification requirements of subgrade fillers, but it could meet the requirements after improvement with 5% cement [29].

At present, the heavy compaction method is widely used for forming phyllite samples at home and abroad. But the aggregate is easy to be crushed when the specimen is formed by this method. Therefore, heavy compaction method is not suitable for aggregates with large particle size. In addition, when using the traditional heavy compaction method, is difficult to ensure the uniformity of the aggregate. With the continuous development of subgrade engineering machinery and equipment, especially the technology of road rollers, the heavy compaction method may no longer agree with the actual situation of the site. Therefore, in this study, the vertical vibration compaction method (VVCM) and heavy compaction method are compared to determine the method of indoor molding of specimens that is more in line with the actual field conditions so that the indoor test and the field compaction are more consistent. Moreover, the research on phyllite filling subgrade mainly focuses on the influence of cement content on the mechanical properties of the improved soil, and little research is reported on the influence of the compactness on the mechanical properties of the improved soil [30].

This paper takes China’s Anping Expressway as the research object. The maximum dry density and optimal water content of weathered phyllite under different compaction methods are compared. The mechanical properties of the subgrade fillers of phyllite are studied from three aspects of cement content, compactness and compaction method. The construction technology for phyllite subgrade filling was determined. This technology has great practical significance and practical value.

2. Materials and methods

2.1 Phyllite sampling

The raw materials were taken from the phyllite found along the Anping expressway. According to the damage and hardness of the phyllite along the route, three representative types of phyllite, namely, A, B, and C were initially selected.

Phyllite A has a relatively complete rock mass, with a mainly plate-like structure, and the core is mostly a 10–15-cm-long block or column. The hammering sound is not clear, and the rock is brittle. The rock mass of phyllite B is relatively complete, mostly shaped as plates, blocks, or short columns. The core is mostly a 4–10-cm-long block with 3–4-cm-long fragments. The hammering sound is dull, and the rock is brittle. The parent rock structure of phyllite C has been destroyed, and the rock mass is strongly weathered and mostly scaly. After mechanical crushing, the core is mostly fragmenting of length 1–5 mm with a small number of fragments that are 1–2 cm long. The hammering sound is dull, and the rock is brittle and becomes muddy after being immersed in water.

The physical indexes of the A, B, and C types retrieved from the site were tested. The test results are listed in Table 1.

Table 1. Physical index of phyllite.

Phyllite type Moisture content (%) Particle density (g/cm3) Block density (g/cm3) Water absorption (%) Porosity (%)
phyllite A 1.9 2.726 2.702 1.01 2.83
phyllite B 3.3 2.701 2.678 2.62 3.96
phyllite C 4.5 2.682 2.657 4.59 8.57

The data in Table 1 show that as the degree of weathering increases, the particle density and block density phyllite A, B, and C gradually decreased, while the water content, water absorption, and porosity gradually increase.

2.2 Cement

The cement selected is Shaanxi Jinlong brand P.O42.5, and the technical parameters of the cement are summarized in Table 2.

Table 2. Technical parameters of the cement used in this study.

index Specific surface area (m2/kg) Stability (mm) 3d compressive strength (MPa) 3d flexural strength (MPa)
Measured value 331 1.0 23.1 5.8
Standards ≥300 ≤5 ≥17.0 ≥3.5

2.3 Test plans

2.3.1 Specimen preparation

The heavy compaction method currently used for compaction quality control does not match the rolling characteristics of on-site tools, and the heavy compaction method does not match the vibration compaction mechanism of the on-site roller. To address this problem, a VVCM that is more in line with the actual situation is introduced herein [3134].

During the rolling operation of the vibratory roller, the eccentric block is driven by the vibrating shaft to rotate rapidly, forming the interference force of the vibration system of the “roller-compressed material.”. Under the action of the interference force, the vibrating wheel vibrates with a frequency equal to that of the interference force [3134]. The vibration is further transferred to the material to be pressed, making the material gradually denser.

In order to ensure the consistency of the indoor compaction effect and the on-site rolling effect and based on the working principle of the directional vibration roller, the vertical vibration testing equipment (VVTE) was used, as shown in Fig 1. Based on the existing research results [3134], the parameters listed in Table 3 were used in the experiments.

Fig 1. Schematic of VVTE.

Fig 1

Table 3. Vibration parameters.
Vibration frequency (Hz) Vibration time (s) Static pressure (kPa) Weight (kg)
Upper system Lower system
40 20 40 108 167

The VVCM specimen was prepared as follows:

  1. The phyllite filler is put into the oven, heated and dried at 105 ± 5°C for 4–6 h; subsequently, water was added for mixing.

  2. The cushion block was placed in the lower part of the test mold, ensuring that the bottom was flat; the mixed phyllite sample was kept in the test mold, and the plunger was used for even insertion during the filling process.

  3. The test mold with the phyllite sample was mounted in the VVTE, clamped using the control platform, and vibrated for 20s.

  4. After the compaction was completed, the height of the sample was measured to ensure that the height of the sample meets the specified requirements.

  5. Finally, the sample was removed with a stripper.

The heavy compaction test and static pressure test were carried out in accordance with the relevant requirements in the Test Methods of Rock for Highway Engineering (JTG E41-2005) [35].

2.3.2 Uniaxial compression test

For uniaxial compressive strength testing, the rock sample must be a regular cylinder or cube. Since complete rock samples could be extracted only from weathered phyllite A, the uniaxial compressive strength test of this type of phyllite was performed in accordance with the Test Methods of Rock for Highway Engineering (JTG E41-2005) [35].

The regular saturated phyllite sample was placed at the center of the bearing plate of the pressure-testing machine to ensure that the sample, pressure plate, and ball seat surface were aligned with each other so that the sample received uniform force during pressure. When loading, the speed was maintained between 0.5 MPa/s and 1.0 MPa/s, and the test was stopped when the sample broke. The load at which the sample broke was recorded. During the test, a series of phenomena caused by the pressure failure of the sample was observed simultaneously.

The uniaxial compressive strength of the rock was determined according to Eq (1).

R=PA (1)

where R is the uniaxial compressive strength of the specimen; P is the maximum load of the damaged specimen; and A is the cross-sectional area of the specimen.

A sample of weathered phyllite A was collected on site, and the uniaxial compressive strength test under water saturation was carried out to obtain the average value of uniaxial compressive strength. The results are listed in Table 4.

Table 4. Uniaxial compressive strength.
Phyllite type Number of samples Average uniaxial compressive strength (MPa)
Phyllite A 10 8.73

The data in Table 4 show that the uniaxial compressive strength value of weathered phyllite A after saturation was less than 15 MPa. According to Standard for engineering classification of rock mass (GB50218-2014) [36], this rock belongs to the category of soft rock.

2.3.3 Point load test

In the case of phyllite B and C, it was difficult to extract a complete rock sample on site owing to their high degree of weathering. Therefore, the uniaxial compression test cannot be used on these two phyllites, so only the point load strength test was used for these samples. Because the point load test has no specific requirements on the shape of the specimen, and it does not require that the specimen must be a regular cylinder or cube. The test is carried out with a point load tester, the rock sample is placed between the upper and lower load cones. Then, load is applied by means of the jack at uniform speed, and it is stopped when the sample breaks. Then, the point load strength is calculated.

The point load strength of the rock is determined according to Eq (2).

Is=PDe2 (2)

where Is is the uncorrected rock point load strength index; P is the maximum load of the specimen when damaged; and De is the equivalent core diameter.

The point load strength test results of weathered phyllite A, B, and C samples in the saturated state are listed in Table 5.

Table 5. Point load strength of phyllite.
Phyllite type Point load strength test value (MPa) Average value (MPa)
1 2 3 4 5
Phyllite A 4.32 4.75 4.19 3.94 4.47 4.33
Phyllite B 2.29 2.17 2.06 2.35 2.11 2.20
Phyllite C 1.29 1.05 1.28 1.17 1.22 1.20

The data in Table 5 show that in the saturated state, the point load strength of weathered phyllite samples of A, B, and C types decreases in that order. The main reason is that the porosity of phyllite increases with the degree of weathering, resulting in a decrease in the effective contact area that is reflected in the trend of decreasing strength.

2.3.4 Modulus of resilience test

According to the Test Methods of Soils for Highway Engineering (JTG E40-2007) [37], the test methods of Ec include the bearing plate method and the strength meter method. In this study, the strength meter method was used for testing.

2.3.5 CBR test

The CBR test method adopted for the current specification [38] requires the specimen to be immersed in water for 96h. For weathered phyllite, it is difficult to meet the specification requirements. Considering only the requirements of the CBR will cause wastage of resources and serious ecological damage. In addition, the starting point of the standard CBR test method is to simulate the most unfavorable conditions during the use of the on-site subgrade materials, but often the standard test method does not match the actual situation of the subgrade site. In this study, using the existing research results, the CBR test method was improved with regard to three aspects: the soaking method, soaking time, and overlying pressure.

  1. Soaking method: The upper soaking method is changed to side soaking. During the soaking process, the water level should be as high as possible, but the test tube should not be submerged.

  2. Soaking time: Considering the permeability of phyllite, the soaking time is changed to 2 days.

  3. Overburden pressure: When used to fill subgrade, upper subgrade, and lower subgrade, the overburden pressures used are 10, 20, and 30 kPa, respectively.

2.3.6 Unconfined compressive strength test

The Rc of the specimen was tested according to the Specification for Design of Highway Subgrades (JTG D30-2015) [38].

3. Results and discussion

3.1 Comparison of VVCM and heavy compaction method

The weathered phyllite was subjected to heavy compaction and VVCM tests. The results are shown in Fig 2.

Fig 2. Comparison of maximum dry density and optimal water content between heavy compaction and VVCM tests.

Fig 2

3.1.1 Maximum dry density

The comparison results of the maximum dry density of the on-site phyllite filler with the maximum dry density in VVCM and heavy compaction tests are listed in Table 6.

Table 6. Comparison of maximum dry density between on-site and indoor compaction tests.
Phyllite type The maximum dry density (g/cm3)
On-site compaction VVCM Heavy compaction method VVCM/ On-site compaction VVCM/ Heavy compaction method
Phyllite A 2.260 2.268 2.210 1.004 0.978
Phyllite B 2.221 2.231 2.182 1.005 0.982
Phyllite C 2.198 2.219 2.151 1.010 0.979

The data in Table 6 show that the maximum dry density on site is significantly higher than that obtained by VVCM, the compactness exceeds 100%. The main reason is that there are limitations to the compaction power and compaction method of heavy compaction, and hence, the phyllite filler fails to achieve high compactness. It also shows that the heavy compaction method is not consistent with the on-site vibration rolling method. In contrast, the VVCM gradually fills the pores between the large particles with fine particles through vibration, thereby improving the compactness of the sample. This is consistent with the characteristics of on-site vibration rolling, and the maximum dry density obtained based on VVCM has a high correlation with the field. Therefore, the VVCM is more compatible with on-site vibration rolling characteristics [32, 33].

3.1.2 Optimal water content

Specimens were formed by heavy compaction method and VVCM to determine the optimal water content. The results are listed in Table 7.

Table 7. Comparison of optimal water content between heavy compaction method and VVCM.
Phyllite type Optimal water content (%)
Heavy compaction method VVCM Heavy compaction method/ VVCM
Phyllite A 7.2 5.8 1.24
Phyllite B 8.2 7.0 1.17
Phyllite C 8.3 7.7 1.08

As seen from the data in Table 7, the optimal water contents of weathered phyllite A, B, and C determined by heavy compaction method are all higher than those determined by VVCM. This is because water mainly plays a role of lubrication during the compaction of subgrade fillers to reduce the resistance generated by the mutual compaction of particles. VVCM mainly uses vibration to rearrange and compact the phyllite particles, while heavy compaction method uses shear stress on the phyllite to further compact it. The frictional resistance that needs to be overcome in the heavy compaction process is greater, and the dependence on water lubrication is higher, resulting in a larger optimal water content. Therefore, the best water content determined by VVCM should be used to control the construction on site.

3.2 Mechanical properties of phyllite subgrade filling

3.2.1 Modulus of resilience

3.2.1.1 Influence of compaction method on Ec. Under the optimal water content conditions, heavy compaction method and VVCM were used to form phyllite specimens with different compactness, and then the Ec values of the specimens was tested in accordance with the Test Methods of Rock for Highway Engineering (JTG E41-2005) [35]. The results are summarized in Table 8. The compaction values listed in the table were calculated based on the maximum dry density of heavy compaction method.

Table 8. Ec values of phyllite samples under different compaction methods.
Compaction method Phyllite A Phyllite B Phyllite C
Compactness (%) Ec value (MPa) Compactness (%) Ec value (MPa) Compactness (%) Ec value (MPa)
VVCM 98.4 65.1 98.8 50.7 98.1 29.6
99.8 72.5 99.6 53.5 99.8 34.5
100.8 77.9 100.5 57.3 100.7 38.3
102.5 90.6 102.7 66.4 102.9 43.2
Heavy compaction method 92.8 35.8 93.8 29.3 94.3 20.9
96.7 42.6 96.5 35.8 96.1 22.1
98.4 52.1 98.5 42.3 97.5 23.7
99.8 67.0 99.8 50.2 99.7 31.5

The data in Table 8 show that as the compactness increases, Ec of the phyllite subgrade filling also increases. The Ec obtained by VVCM is generally greater than the heavy compaction method. For every 1% increase in compactness, Ec of VVCM and heavy compacted phyllite A, B, and C samples increased by10%, 11%, and 13% on average. As the compactness increased, Ec values obtained by the two compaction methods decreased continuously.

This behavior is attributed to the fact that as the compactness increases, the internal porosity of the specimen decreases, thereby increasing the effective area of the load. Owing to the differences in the mechanisms of the two compaction methods, the changes caused to the phyllite packing structure are greater in the case of VVCM. Under the action of vibration, the phyllite particles are more evenly distributed, and the pores in the sample are smaller. The friction and compaction between phyllite particles are correspondingly larger, and hence, Ec of the phyllite formed by VVCM is larger than that of the phyllite formed by the heavy compaction method.

3.2.1.2 Influence of compactness on modulus of resilience. Under the optimal water content conditions, VVCM was used to form phyllite samples with different compactness. The results are shown in Fig 3.

Fig 3. The relationship between Ec and compactness of the weathered phyllite.

Fig 3

Fig 3 shows that when the water content is constant, Ec of phyllite increases linearly with compactness. When the specimen is formed by VVCM, for every 1% increase in compactness, Ec of the weathered phyllite A, B, and C samples increased by 4.6, 3.2, and 2.1 MPa respectively; that is, for every 1% increase in compactness, Ec increased by 15% to 17%. Thus, increasing the compactness can increase the Ec correspondingly. The main reason is that while the compactness is increased, the porosity of the specimen is reduced, and the mechanical strength is also improved.

3.2.2 CBR

3.2.2.1 Influence of compaction method on CBR. Under the optimal water content conditions, heavy compaction method and VVCM were used to form phyllite specimens with different compactness. After the specimens were formed, the CBR test was performed according to the improved CBR test method. The test results are shown in Fig 4.

Fig 4. CBR of the weathered phyllite samples under different compaction methods.

Fig 4

Fig 4 shows that as the compactness increases, the CBR of the phyllite subgrade filling too increases, and the CBR obtained by VVCM is greater than by the heavy compaction method. For every 1% increase in compactness, the CBR values of VVCM and heavy compaction phyllite increased by an average of 24% and 13%, respectively. Further, as the compactness increased, the ratio between the CBR obtained by the two molding methods too increased.

The main reason for this phenomenon is the differences between the mechanisms of the two compaction methods. In the heavy compaction method, the phyllite subgrade filler needs to overcome its own shear stress, which will result in more pores in the specimen. VVCM changes the internal structure of the phyllite filler, making the phyllite particles more evenly distributed. The pores in the specimen become smaller, forming a compact overall structure, and the friction and intercalation between the phyllite particles are correspondingly larger. Therefore, the strength of the phyllite formed by VVCM is greater than that of the sample formed by the heavy compaction method [34].

3.2.2.2 Influence of compactness on CBR. Under the optimal water content conditions, the heavy compaction method was used to form phyllite specimens with different compactness. The test was carried out according to the improved CBR method. The results are shown in Fig 5.

Fig 5. Relationship between CBR and compactness of phyllites.

Fig 5

From Fig 5, it is clear that the CBR of the three weathered phyllite types all increase with the increase in compactness.

  1. Phyllite A can meet the requirements of subgrade filling under 2.7 kPa overburden pressure. Hence, only the relationship between compactness and CBR under 10 kPa overburden pressure was analyzed. Under the compactness required by specification, the CBR of phyllite A cannot meet the requirements, but it can meet the requirements when the compactness is increased to more than 97%.

  2. The CBR of phyllite B meets the requirements for subgrade filling under the overburden pressure of 20 kPa and 30 kPa. When the compactness is increased to 98%, phyllite B can meet the CBR requirements of the lower subgrade at an overburden pressure of 10 kPa. When phyllite B is used as the upper subgrade filler, the compactness must reach 113% or more. It can be seen that when phyllite B is used as the upper subgrade filler, the compactness capacity of compaction equipment has been exceeded.

  3. Under the compactness required by the specification, when phyllite C is used as the lower subgrade filler, its CBR value cannot meet the requirements. It can meet the requirements when the compactness reaches 97%. When phyllite C is used as the upper subgrade filler, the compactness needs to be increased to more than 100%. Hence, the dynamic compaction method must be used when phyllite C is used as the upper subgrade filler.

3.3 Mechanical properties of cement-improved phyllite subgrade filling

From the CBR test results of phyllite subgrade filling, it is seen that even if the compactness is increased, the CBR of phyllite B still cannot meet the requirements of the upper subgrade, and the CBR of phyllite C cannot meet the requirements of upper subgrade and subgrade. Therefore, it is necessary to add an external admixture to improve the phyllite subgrade filler. In this test, cement was selected as the external admixture.

3.3.1 Compaction characteristics of cement-improved phyllite

According to Test Methods of Materials Stabilized with Inorganic Binders for Highway Engineering (JTG E51-2009) [39], VVCM and heavy compaction method were applied for three types of cement-improved phyllite, with the initial cement contents of 2%, 3%, 4%, and 5%. The relationship among the optimal water content, maximum dry density, and cement content of cement-improved phyllite is shown in Fig 6.

Fig 6. Comparison of VVCM and heavy compaction method.

Fig 6

From Fig 6, it is seen that with an increase in cement content, the maximum dry density of the improved phyllite increased continuously. However, the increase rate was not obvious, indicating that the cement content has little effect on the maximum dry density of phyllite subgrade filler, but that it is still greater than the maximum dry density of unimproved phyllite subgrade filler. The optimum water content also shows an increasing trend with an increase in cement content. The main reason for this result is that in addition to the lubricating effect of water, the greater the amount of cement, the more is the amount of water required for cement hydration. In addition, the influence of compaction method on the maximum dry density and optimal water content of the improved phyllite is consistent with Section 3.1, further showing the advantages of VVCM.

3.3.2 Mechanical properties of cement-improved phyllite

3.3.2.1 Unconfined compressive strength.

  • (1) Cement content

The specimens were molded by VVCM under the optimal water content conditions, and tests were performed for cement contents of 2%, 3%, 4%, and 5%. After curing for 7 days under standard humidity and temperature conditions, Rc was tested. The influence of cement content on Rc of the improved phyllite subgrade filler is shown in Fig 7.

Fig 7. Influence of cement content on Rc.

Fig 7

It can be seen from Fig 7 that the 7d Rc of the improved phyllite shows an increasing trend with the increase in cement content. For every 1% increase in the cement content, Rc increased by at least 15%. The largest increase in Rc was observed for cement-improved phyllite A; for every 1% increase in cement content, its Rc increases by 0.36 MPa. This is because with the increase of the cement content, the amount of new cementitious substances generated after the hydration reaction of the cement will also increase, effectively enhancing the bonding between the phyllite particles. The increase in cement content will cause more cement stones to be formed in the pores of the specimen, reduce the pores inside the specimen and increase its strength.

  • (2) Compactness

The relationship between the Rc and the compactness of the improved phyllite is shown in Fig 8.

Fig 8. The relationship between 7d Rc and compactness.

Fig 8

It can be seen from Fig 8 that when the cement content is constant, with an increase in compactness, Rc of the improved phyllite subgrade filling shows a linear growth trend. For every 1% increase in compactness, Rc of the improved phyllite increases by at least 11%. Phyllite B has the largest increase in Rc when the cement content is 5%, and the Rc increases by 0.12 MPa for every 1% increase in compactness. It can be seen that the compactness has a significant effect on the Rc of the improved phyllite subgrade filler. This mainly because of the increase in compactness, the porosity inside the specimen decreases, and the contact area of the specimen increases.

  • (3) Compaction method

VVCM and static pressure method were used to prepare cement-improved phyllite specimens with different compactness. The cement content was 4%, and the specimen was cured for 7 days under standard curing conditions, and the Rc of the phyllite specimen was tested. The results are shown in Fig 9.

Fig 9. Relationship between 7d Rc and compaction method.

Fig 9

It can be seen from Fig 9, when the cement content was 4%, regardless of the compaction method, 7d Rc shows a linear growth trend with the increase of compactness. Further, Rc of improved phyllite specimens by VVCM can be increased by 15% to 23% for every 1% increase in compactness, which is far greater than the 12–18% of the static pressure method. It shows that the compaction method also has a certain influence on the Rc of the improved phyllite subgrade filler. Phyllite particles are in a relatively flowing state under the action of vibration, and the resistance between the particles is reduced, thus forming a relatively dense state. The static pressure method simply relies on the vertical pressure to overcome the shear force between the particles, and it cannot make the particles fill each other to form a compact whole.

3.3.2.2 Modulus of resilience.

  • (1) Cement content

The specimens were compacted by VVCM under the optimal water content conditions, and the cement contents were 2%, 3%, 4%, and 5%. After curing for 7 days under standard humidity and temperature conditions, the Ec were determined. The influence of cement content on Ec of improved phyllite subgrade filler is shown in Fig 10.

Fig 10. The influence of cement content on Ec.

Fig 10

The figure shows that the 7d Ec of the improved phyllite tends to increase with an increase in cement content. For every 1% increase in cement, its Ec increases by at least 17%. The Ec of cement-improved phyllite A has the largest increase. For every 1% increase in cement content, the Ec increases by 62 MPa. This relationship is consistent with the Rc.

  • (2) Compactness

The relationship between 7d Ec and compactness is shown in Fig 11.

Fig 11. Relationship between 7d Ec and compactness.

Fig 11

The figure shows that when the cement content is constant, with an increase of compactness, the Ec of the improved phyllite subgrade filling shows a linear growth trend. For every 1% increase in compactness, the Ec of the improved phyllite increased by at least 6%. Phyllite B has the largest increase in Ec when the cement content is 5%, and the Ec increases by 19 MPa for every 1% increase in compactness. It can be seen that the compactness also has a significant effect on the Ec of the improved phyllite subgrade filler.

  • (3) Compaction method

VVCM and static pressure method were used to prepare cement-improved phyllite specimens with different compactness. The cement content was 4%, and the specimen was cured for 7 days under standard curing conditions, and then, the Ec values of the phyllite specimen were tested. The results are shown in Fig 12.

Fig 12. The relationship between 7d Ec and compaction method.

Fig 12

From the figure, it is clear that when the cement content is 4%, regardless of the compaction method, the 7d Ec shows a linear growth trend with increase of compactness. The Ec of the improved phyllite specimens formed by VVCM can be increased by 5% to 10% for every 1% increase in compactness, which is greater than the rise seen in the samples formed by the static pressure method. It shows that the compaction method also has a certain influence on the Ec of the improved phyllite subgrade filler, and it also reflects the superiority of VVCM.

4. Field test analysis of improved phyllite filling subgrade

4.1 Test section

Field tests on the improvement of strongly weathered phyllite fillers were carried out in the K18+440—K18+540 and K20+220—K20+320 sections of the No. 4 bid section of the Ankang–Pingli expressway in Shaanxi. The test road sections were improved with cements of 2%, 3%, 4%, and 5%, and each sample was 50 m long.

4.2 On-site rebound deflection test method

Ec is the main design parameter that reflects the strength, stiffness, and stability of subgrade, and it is also the main mechanical parameter that characterizes the ability of subgrade to resist deformation under traffic load. Therefore, according to the Field Test Methods of Subgrade Pavement for Highway Engineering (JTG 3450–2019) [40], the load-bearing plate method was adopted to test Ec of the field subgrade.

4.3 Test result analysis

The sand-filling method was used to detect the compactness of the test section. The minimum compactness of the tested embankment cement-improved phyllite filler is 95.3%. It can meet the 94% compactness required by the Specifications for Design of Highway Subgrades (JTG D30-2015) [38]. Ec tests were carried out on modified road sections with different cement content. The test results are summarized in Table 9.

Table 9. Ec of strongly weathered phyllite filling subgrade under different cement content.

Test bid Cement content (%) Ec (MPa)
K18+440—K18+490 2 64.08
K18+490—K18+540 3 79.15
K20+220—K20+270 4 95.25
K20+270—K20+320 5 108.47

The data in Table 9 show that Ec of subgrade increases linearly with an increase in cement content. When the cement content is 2%, the subgrade Ec is 64.08 MPa. When the cement content is 5%, the Ec reaches 108.47 MPa, which is 69% higher than that of the subgrade with 2% cement. According to the Specifications for Design of Highway Asphalt Pavement (JTG D50-2017) [41], Ec of highways and first-class highway subgrades should be 30 MPa. This shows that after the phyllite filler is improved by cement addition and that Ec of the subgrade can meet the specification requirements. Further, comparison with the indoor test results shows that VVCM has better field correlation than the heavy compaction method, this is consistent with Yuan’s research results [42].

5. Conclusions

  1. The physical and mechanical properties of three typical phyllites along the Anping expressway were studied. The results show that as the degree of weathering increases, the porosity of the phyllite increases, and the effective contact area decreases, eventually leading to a continuous decrease in strength.

  2. VVCM was proposed and used to evaluate the compaction characteristics of phyllite subgrade filling. The results show that the maximum dry density of the specimen formed by VVCM is larger and its optimal water content is lower.

  3. The effects of compaction method and compactness on the mechanical properties of phyllite subgrade filling were studied. The results show that the Ec and CBR of phyllite subgrade fillings increase with an increase in compactness. For every 1% increase in compactness, the Ec of the phyllite specimen increased by at least 10%, and the CBR increased by at least 8%. In addition, Ec and CBR of the VVCM specimen were greater than those of the specimen formed by the heavy compaction method. Thus, the merits of the VVCM were established.

  4. The compaction and mechanical properties of cement-improved phyllite subgrade fillers were studied. The results show that with an increase in cement content, the maximum dry density and optimal water content both increases. In addition, the physical and mechanical properties of phyllite subgrade fillers improved greatly. The performance of cement-improved phyllite subgrade filler was also affected by the compactness and compaction method, and the performance of the VVCM-molded specimen was better than that of the specimen formed by the heavy compaction method.

  5. Test subgrade Ec was tested on the test section of the site, and the results showed that under identical loads, the larger the cement content, the smaller is the rebound deformation; the higher the subgrade strength. Using cement contents of 2%, 3%, 4%, and 5% improved phyllite subgrade specimens were obtained, and Ec increased with the cement content.

Supporting information

S1 Data

(DOCX)

Data Availability

All relevant data are within the paper and its Supporting information files.

Funding Statement

This study was funded by the Transportation Technology plan project from Jilin Provincial in the form of a grant (No. 2017ZDGC-7) awarded to YJ, the Scientific Research of Central Colleges of China for Chang’an University in the form of a grant (No. 300102218212) awarded to YJ, and the Scientific Project from Henan Provincial Communication in the form of a grant (No. 2020J-2-2 95) awarded to YJ.

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Decision Letter 0

Ahmed Mancy Mosa

19 Jan 2021

PONE-D-20-39942

Research on the mechanical properties of cement-improved phyllite based on the vertical vibration compaction method

PLOS ONE

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Reviewer #1: - More suitable title should be selected for the article. Title should decrease to 10-12 words.

- The abstract should state briefly the purpose of the research, the principal results and major conclusions. An abstract is often presented separately from the article, so it must be able to stand alone.

- It is suggested to present the structure of the article at the end of the introduction.

- The necessity and innovation of the article should be presented to the introduction.

- A flowchart should be added to the article to show the research methodology.

- It is suggested to add articles entitled “Arshid and Kamal. Appraisal of Bearing Capacity and Modulus of Subgrade Reaction of Refilled Soils” and “Fazelabdolabadi and Golestan. Towards Bayesian Quantification of Permeability in Micro-scale Porous Structures – The Database of Micro Networks” to the literature review.

- The major defect of this study is the debate or Argument is not clear stated in the introduction session. Hence, the contribution is weak in this manuscript. I would suggest the author to enhance your theoretical discussion and arrives your debate or argument.

- More suitable title should be selected for the figure 6 instead of “Comparison of maximum dry density between heavy compaction and VVCM tests”.

- It is suggested to compare the results of the present research with some similar studies which is done before.

- Following, you will find some new related references which should be added to literature review:

Alzaim et al. Effect of Modulus of Bituminous Layers and Utilization of Capping Layer on Weak Pavement Subgrades;

Majeed et al. Evaluation of Concrete with Partial Replacement of Cement by Waste Marble Powder.

- Page 3: the following paragraph is unclear, so please reorganize that:

“In the case of phyllite B and C, it was difficult to extract a complete rock sample on site owing to their high degree of weathering. Hence, only a point load strength test was performed for these samples. The point load test has no specific requirements on the shape of the specimen, and it does not require that the specimen must be a regular cylinder or cube.”

- Much more explanations and interpretations must be added for the Results, which are not enough.

- Please make sure your conclusions' section underscore the scientific value added of your paper, and/or the applicability of your findings/results, as indicated previously. Please revise your conclusion part into more details. Basically, you should enhance your contributions, limitations, underscore the scientific value added of your paper, and/or the applicability of your findings/results and future study in this session.

- “Notation” should be added to the article.

- DOI of the references must be added (you can use “" ext-link-type="uri" xlink:type="simple">https://crossref.org/").

Reviewer #2: The paper "Research on the mechanical properties of cement-improved phyllite based on the

vertical vibration compaction method " is very interesting and helpful for the reader. The paper is very well written and has readable structure. Therefore, it deserved to publish in the journal.

However, the following points need explanation.

1- Please provide the latest references in the literature review.

2- The text in the figures are not readable please increase the axis label size.

3- Please provide the mechanics of the crack patter.

4- Describe about the experimental case study in more detail.

Reviewer #3: The manuscript entitled "Research on the mechanical properties of cement-improved phyllite based on the vertical vibration compaction method" has been investigated in detail. The topic addressed in the manuscript is potentially interesting and the manuscript contains some practical meanings, however, there are some issues which should be addressed by the authors:

1) The readability and presentation of the study should be further improved. The paper suffers from language problems. The paper should be proofread by a native speaker or a proofreading agent.

2) The Introduction section needs a major revision in terms of providing more accurate and informative literature review and the pros and cons of the available approaches and how the proposed method is different comparatively. Also, the motivation and contribution should be stated more clearly.

3) The importance of the material carried out in this manuscript can be explained better than other important studies published in this field. I recommend the authors to review other recently developed works.

4) What makes the proposed material suitable for this unique mixture? What new findings to the proposed material have the authors added (compared to the existing experiments)? These points should be clarified.

5) "Conclusion" section should be edited in a more highlighting, argumentative way. The authors should analysis the reason why the tested results is achieved.

6) The main contributions of the study should be clearly explained in both theoretical and practical aspects.

7) The authors should clearly emphasize the contribution of the study. Please note that the up-to-date of references will contribute to the up-to-date of your manuscript.

8) It will be helpful to the readers if some discussions about insight of the main results are added as Remarks or Discussion.

This study may be proposed for publication if it is addressed in the specified problems.

Reviewer #4: The authors of this paper made an appreciable effort, however the manuscript is unable to elaborate the novelty and applicability of this research in the field. However, the quality of this manuscript can be improved by adding few more test, by discussing the findings and the applicability f the result on the site. Few comments are listed below:

1. The authors has mentioned that the Phyllite is very soft rock available on the study site and not suitable for subbase or subgrade, however, the addition of cement will improve the property. The increase in strength after adding cement is obvious but what is the durability of the stabilized materials? Durability test need to be added in the manuscript.

2. The Phyllite rock bed is available on the site but the test performed in the laboratory is based on the crushed rock. Authors does not discussed that how the cement will be mixed with the Phyllite rock on the site.

3. The title need to be rewritten. Do not start the title with the word "Research."

4. The abstract need to be rewritten and must include some part of Introduction, methodology, result and conclusion.

5. More citation in the introduction is required closely related to the present study.

Reviewer #5: 1. The title can be changed to be

Investigation on cement-improved phyllite based on the vertical vibration compaction method

2. Be more specific, where?? Line 9

3. The discerption of the material may be by grain size distribution not by long. Line78

4. The methodology and the laboratory work must be shortened to include only the important details. The number of designation of standards should be mentioned.

5. Figures 1-3 could be removed.

6. The conclusions covered the finding of the study.

7. The references are sufficient and recent.

8. The overall structure of the article is fair.

**********

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Reviewer #1: No

Reviewer #2: Yes: Afaq Ahmad

Reviewer #3: No

Reviewer #4: Yes: SHAMSHAD ALAM

Reviewer #5: No

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PLoS One. 2021 Mar 3;16(3):e0247599. doi: 10.1371/journal.pone.0247599.r002

Author response to Decision Letter 0


26 Jan 2021

Dear editor,

I have revised the manuscript as required. Including the following:

1. Adjust the format of the manuscript to meet the requirements of PLOS ONE.

2. Deleted Figure 1, Figure 2, Figure 3 and Figure 5 in the manuscript.

3. The specific geographic coordinates of the phyllite sampling are along the Ankang-Pingli Expressway in Shaanxi Province, China.

4. A separate description is added for each figure in the manuscript.

The following is my specific response to the reviewers’ comments.

Dear reviewer 1,

Thank you again for reviewing and evaluating my manuscript, and the following is my reply and description.

Question 1: More suitable title should be selected for the article. Title should decrease to 10-12 words.

Response: Thanks for the reviewer’s comments. I have adjusted the title to 11 words. The current title reflects the core of this article.

Question 2: The abstract should state briefly the purpose of the research, the principal results and major conclusions. An abstract is often presented separately from the article, so it must be able to stand alone.

Response: Thanks for the reviewer’s comments. I have adjusted the abstract to make it an independent part. And delete the part except the purpose of the research, the principal results and major conclusions to make it simpler and clearer.

Question 3: It is suggested to present the structure of the article at the end of the introduction.

Response: Thanks for the reviewer’s comments. At the end of the introduction, I have summarized the research structure of the article to make it clearer.

Question 4: The necessity and innovation of the article should be presented to the introduction.

Response: Thanks for the reviewer’s comments. I have divided the last paragraph of the original introduction into two paragraphs. The first paragraph points out the current research status and deficiencies, and points out the necessity and innovation of this article. The second paragraph explains the research structure of the article.

Question 5: A flowchart should be added to the article to show the research methodology.

Response: Thanks for the reviewer’s comments. This article is a relatively conventional research paper. Except for VVCM, the test methods and compaction methods used are basically those widely used in the road industry. The research plan and the experimental methods used have been clearly presented in Section 2.3. So, I think that adding a flowchart is a bit repetitive, so I didn't add the flowchart to the manuscript.

Question 6: It is suggested to add articles entitled “Arshid and Kamal. Appraisal of Bearing Capacity and Modulus of Subgrade Reaction of Refilled Soils” and “Fazelabdolabadi and Golestan. Towards Bayesian Quantification of Permeability in Micro-scale Porous Structures – The Database of Micro Networks” to the literature review.

Response: Thanks for the reviewer’s comments. I have added "Arshid and Kamal. Appraisal of Bearing Capacity and Modulus of Subgrade Reaction of Refilled Soils" to the reference, but about "Fazelabdolabadi and Golestan. Towards Bayesian Quantification of Permeability in Micro-scale Porous Structures – The Database of Micro Networks", I did not find the source of the document. If it is convenient, can you provide me with the original text? I will add it to the reference after I read it.

Question 7: The major defect of this study is the debate or Argument is not clear stated in the introduction session. Hence, the contribution is weak in this manuscript. I would suggest the author to enhance your theoretical discussion and arrives your debate or argument.

Response: Thanks for the reviewer’s comments. I have readjusted the introduction debate to make it more convincing.

Question 8: More suitable title should be selected for the figure 6 instead of “Comparison of maximum dry density between heavy compaction and VVCM tests”.

Response: Thanks for the reviewer’s comments. The title of Figure 6 is indeed not appropriate, I have modified it to "Comparison of maximum dry density and optimal water content between heavy compaction and VVCM tests".

Question 9: It is suggested to compare the results of the present research with some similar studies which is done before.

Response: Thanks for the reviewer’s comments. I have added "Comparison of Mechanical Properties of Cement-Stabilized Loess Produced Using Different Compaction Methods" to prove that VVCM has a high correlation with the field, which is consistent with previous research results.

Question 10: Following, you will find some new related references which should be added to literature review: Alzaim et al. Effect of Modulus of Bituminous Layers and Utilization of Capping Layer on Weak Pavement Subgrades; Majeed et al. Evaluation of Concrete with Partial Replacement of Cement by Waste Marble Powder.

Response: Thanks for the reviewer’s comments. The two articles you provided are of great reference value, and I have added these two articles to the manuscript as references.

Question 11: Page 3: the following paragraph is unclear, so please reorganize that:“In the case of phyllite B and C, it was difficult to extract a complete rock sample on site owing to their high degree of weathering. Hence, only a point load strength test was performed for these samples. The point load test has no specific requirements on the shape of the specimen, and it does not require that the specimen must be a regular cylinder or cube.”

Response: Thanks for the reviewer’s comments. I have modified the third page of the manuscript to make it more fluent and easier to understand.

Question 12: Much more explanations and interpretations must be added for the Results, which are not enough.

Response: Thanks for the reviewer’s comments. What you said is of great value, and I have made the necessary adjustments in the manuscript.

Question 13: Please make sure your conclusions' section underscore the scientific value added of your paper, and/or the applicability of your findings/results, as indicated previously. Please revise your conclusion part into more details. Basically, you should enhance your contributions, limitations, underscore the scientific value added of your paper, and/or the applicability of your findings/results and future study in this session.

Response: Thanks for the reviewer’s comments. What you said is very important, and I have made the necessary adjustments in the manuscript. The purpose of this article is to illustrate the feasibility of phyllite as a subgrade filler, which is verified by a series of tests. Then in order to explain the superiority of the VVCM method compared with other methods, it is more relevant to the field core samples, which are explained in detail in the article and thesis.

Question 14: “Notation” should be added to the article.

Response: Thanks for the reviewer’s comments. I have made the necessary changes in the manuscript.

Question 15: DOI of the references must be added (you can use “https://crossref.org/").

Response: Thanks for the reviewer’s comments. I have added the DOI of all documents to the back of the corresponding references. For some conference papers without DOI, I have found the original link as a supplement.

Dear reviewer 2,

Thank you again for reviewing and evaluating my manuscript, and the following is my reply and description.

Question 1: Please provide the latest references in the literature review.

Response: Thanks for the reviewer’s comments. I have included some 2020 and 2021 articles in the references.

Question 2: The text in the figures is not readable please increase the axis label size.

Response: Thanks for the reviewer’s comments. The unreadable text of the picture is due to the stitching of the pictures, and formatting problems are likely to occur if they are placed separately. I have adjusted the picture in the manuscript to make it clearer.

Question 3: Please provide the mechanics of the crack patter.

Response: Thanks for the reviewer’s comments. The question you mentioned is very valuable. But I am very sorry that I did not understand exactly what you mean. If you are talking about the weathering cracks of phyllite A, B and C, then the principle is caused by the weathering of nature. If you are talking about cracks formed by the destruction of strength. Then the principle is that the upper and lower parts exert a force on the specimen. It produces shear deformation, resulting in damage. This is similar to the compressive strength failure in the reference "Engineering Comparison of Mechanical Properties of Cement-Stabilized Loess Produced Using Different Compaction Methods".

Question 4: Describe about the experimental case study in more detail.

Response: Thanks for the reviewer’s comments. I have made the necessary changes in the manuscript. One of the purposes of this article is to determine that VVCM is more relevant to the scene. Therefore, the field test research is based on this conclusion. Due to the limited conditions, there are not enough confirmatory field tests. I will explore this issue more in-depth in subsequent research.

Dear reviewer 3,

Thank you again for reviewing and evaluating my manuscript, and the following is my reply and description.

Question 1: The readability and presentation of the study should be further improved. The paper suffers from language problems. The paper should be proofread by a native speaker or a proofreading agent.

Response: Thanks for the reviewer’s comments. The question you raised is very valuable. In response to language issues, I have made necessary adjustments in the manuscript.

Question 2: The Introduction section needs a major revision in terms of providing more accurate and informative literature review and the pros and cons of the available approaches and how the proposed method is different comparatively. Also, the motivation and contribution should be stated more clearly.

Response: Thanks for the reviewer’s comments. I have adjusted the introduction in the manuscript. Added the latest references for explanation and demonstration. It also explains the shortcomings of the existing methods and the applicability of the proposed methods. I divided the original last paragraph into two paragraphs. The first part explains the shortcomings of the current method and the lack of relevance to the scene. The second part leads to my own research content and research ideas.

Question 3: The importance of the material carried out in this manuscript can be explained better than other important studies published in this field. I recommend the authors to review other recently developed works.

Response: Thanks for the reviewer’s comments. Your question is very valuable. I have added other latest literature on phyllite materials in the manuscript to better explain it.

Question 4: What makes the proposed material suitable for this unique mixture? What new findings to the proposed material have the authors added (compared to the existing experiments)? These points should be clarified.

Response: Thanks for the reviewer’s comments. Weathered phyllite is extremely difficult to meet the minimum requirements of subgrade filling specifications. But adding cement to improve can meet the requirements, which is also explained in the second part of the introduction. However, due to the low correlation between the heavy compaction method and the site, the results obtained from the indoor test pieces cannot be used to better guide the site practice. Most of the existing researches are based on the heavy compaction method, but the VVCM method can better establish a connection with the present, so as to judge whether the cement-improved phyllite can meet the requirements of on-site construction.

Question 5: "Conclusion" section should be edited in a more highlighting, argumentative way. The authors should analysis the reason why the tested results are achieved.

Response: Thanks for the reviewer’s comments. I have revised the conclusion in the manuscript. The reason for obtaining the test result has been explained and supplemented in the results and discussion.

Question 6: The main contributions of the study should be clearly explained in both theoretical and practical aspects.

Response: Thanks for the reviewer’s comments. I have made the necessary changes in the manuscript. For the theoretical explanation, I have added a few recent references to prove the correctness of the theory. Regarding practice, I am sorry that due to the limited site conditions, the collected data is not enough, so I quoted the previous research results to deepen the explanation of the site relevance. I will focus on this in future research.

Question 7: The authors should clearly emphasize the contribution of the study. Please note that the up-to-date of references will contribute to the up-to-date of your manuscript.

Response: Thanks for the reviewer’s comments. This question you mentioned is very valuable. I have added several recent research papers as references in the manuscript to enhance the value and contribution of this research.

Question 8: It will be helpful to the readers if some discussions about insight of the main results are added as Remarks or Discussion.

Response: Thanks for the reviewer’s comments. The question you mentioned is of great help to me, and I have made the necessary changes in the manuscript.

Dear reviewer 4,

Thank you again for reviewing and evaluating my manuscript, and the following is my reply and description.

Question 1: The authors has mentioned that the Phyllite is very soft rock available on the study site and not suitable for subbase or subgrade, however, the addition of cement will improve the property. The increase in strength after adding cement is obvious but what is the durability of the stabilized materials? Durability test need to be added in the manuscript.

Response: Thanks for the reviewer’s comments. What you said is very meaningful. I am sorry that I did not perform the durability test of cement modified phyllite in the article. This will be the focus of my follow-up research, and I will focus on this in subsequent research. In the introduction, I referred to previous research results, which indirectly demonstrated that cement-improved phyllite has better stability. And the improvement of a variety of materials by cement, such as loess, expansive soil and other soft rocks, has been shown to improve its performance.

Question 2: The Phyllite rock bed is available on the site but the test performed in the laboratory is based on the crushed rock. Authors does not discuss that how the cement will be mixed with the Phyllite rock on the site.

Response: Thanks for the reviewer’s comments. It can be seen from Figure 9 that phyllite with different weathering degrees can meet the specifications for different requirements for subgrade filling. The direct use of phyllite as subgrade filler on site also has higher requirements for compaction. During the indoor test, I first studied the phyllite without cement and judged whether it can meet the standard of subgrade filling, so the conclusion drawn in Figure 9 appeared. Then I studied the cement-improved phyllite, and judged the influence of different cement content, compaction degree, and molding method on it, so as to better guide the on-site construction. Therefore, indoor tests include both weathered phyllite and cement-modified phyllite.

For cement-improved phyllite, instead of directly using the phyllite materials along the line, the phyllite is further processed. In this process, cement is added for modification, and then transported back to the site for construction.

Question 3: The title needs to be rewritten. Do not start the title with the word "Research."

Response: Thanks for the reviewer’s comments. I have revised the title in the manuscript.

Question 4: The abstract need to be rewritten and must include some part of Introduction, methodology, result and conclusion.

Response: Thanks for the reviewer’s comments. I have rewritten the abstract, deleted some content not related to this research, and then highlighted the core and focus of the research.

Question 5: More citation in the introduction is required closely related to the present study.

Response: Thanks for the reviewer’s comments. The question you raised is very meaningful. I have added several recent studies as references in the manuscript, hoping to improve the research of this article.

Dear reviewer 5,

Thank you again for reviewing and evaluating my manuscript, and the following is my reply and description.

Question 1: The title can be changed to be“Investigation on cement-improved phyllite based on the vertical vibration compaction method”

Response: Thanks for the reviewer’s comments. I have revised the title in the manuscript.

Question 2: Be more specific, where?? Line 9

Response: Thanks for the reviewer’s comments. Sorry for not explaining clearly. Mountain highway here refers to the highway from Ankang to Pingli in Shaanxi Province. In fact, not only along this highway, but also along many highways in Northwest China, there will be a lot of weathered phyllite.

Question 3: The discerption of the material may be by grain size distribution not by long. Line78

Response: Thanks for the reviewer’s comments. For the classification of weathered phyllite, I did not use length to classify, but distinguished by its degree of weathering. The description of its length in the material part is to give readers a more intuitive feeling. Because the mechanical properties of phyllite with different weathering degrees are very different, this will also be involved in the following research. Because both strongly weathered phyllite and moderately weathered phyllite are extremely fragile, they are prone to fragmentation during sampling, so it is not accurate to judge by the particle size alone.

Question 4: The methodology and the laboratory work must be shortened to include only the important details. The number of designation of standards should be mentioned.

Response: Thanks for the reviewer’s comments. The question you raised is very valuable. I have revised the method part in the manuscript. However, in order to ensure that readers can clearly understand the experimental procedures, the various experiments performed must be fully presented in the manuscript, so the length is indeed relatively long, which is unavoidable. For the numbering of the standard, I have added it in the manuscript.

Question 5: Figures 1-3 could be removed.

Response: Thanks for the reviewer’s comments. Figure 1-3 is a bit redundant; I have deleted Figure 1-3 in the manuscript.

Attachment

Submitted filename: Response to Reviewers.docx

Decision Letter 1

Ahmed Mancy Mosa

5 Feb 2021

PONE-D-20-39942R1

Investigation on cement-improved phyllite based on the vertical vibration compaction method

PLOS ONE

Dear Dr. Fan,

Thank you for submitting your manuscript to PLOS ONE. After careful consideration, we feel that it has merit but does not fully meet PLOS ONE’s publication criteria as it currently stands. Therefore, we invite you to submit a revised version of the manuscript that addresses the points raised during the review process.

Please consider the comment of reviewer5 ( Apply unified numbering system for the sections and subsections)

Please submit your revised manuscript by 14 Feb. 2021. If you will need more time than this to complete your revisions, please reply to this message or contact the journal office at plosone@plos.org. When you're ready to submit your revision, log on to https://www.editorialmanager.com/pone/ and select the 'Submissions Needing Revision' folder to locate your manuscript file.

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If you would like to make changes to your financial disclosure, please include your updated statement in your cover letter. Guidelines for resubmitting your figure files are available below the reviewer comments at the end of this letter.

If applicable, we recommend that you deposit your laboratory protocols in protocols.io to enhance the reproducibility of your results. Protocols.io assigns your protocol its own identifier (DOI) so that it can be cited independently in the future. For instructions see: http://journals.plos.org/plosone/s/submission-guidelines#loc-laboratory-protocols

We look forward to receiving your revised manuscript.

Kind regards,

Ahmed Mancy Mosa, Ph.D.

Academic Editor

PLOS ONE

[Note: HTML markup is below. Please do not edit.]

Reviewers' comments:

Reviewer's Responses to Questions

Comments to the Author

1. If the authors have adequately addressed your comments raised in a previous round of review and you feel that this manuscript is now acceptable for publication, you may indicate that here to bypass the “Comments to the Author” section, enter your conflict of interest statement in the “Confidential to Editor” section, and submit your "Accept" recommendation.

Reviewer #1: All comments have been addressed

Reviewer #2: All comments have been addressed

Reviewer #3: All comments have been addressed

Reviewer #5: All comments have been addressed

**********

2. Is the manuscript technically sound, and do the data support the conclusions?

The manuscript must describe a technically sound piece of scientific research with data that supports the conclusions. Experiments must have been conducted rigorously, with appropriate controls, replication, and sample sizes. The conclusions must be drawn appropriately based on the data presented.

Reviewer #1: Yes

Reviewer #2: Yes

Reviewer #3: Yes

Reviewer #5: Partly

**********

3. Has the statistical analysis been performed appropriately and rigorously?

Reviewer #1: Yes

Reviewer #2: Yes

Reviewer #3: Yes

Reviewer #5: N/A

**********

4. Have the authors made all data underlying the findings in their manuscript fully available?

The PLOS Data policy requires authors to make all data underlying the findings described in their manuscript fully available without restriction, with rare exception (please refer to the Data Availability Statement in the manuscript PDF file). The data should be provided as part of the manuscript or its supporting information, or deposited to a public repository. For example, in addition to summary statistics, the data points behind means, medians and variance measures should be available. If there are restrictions on publicly sharing data—e.g. participant privacy or use of data from a third party—those must be specified.

Reviewer #1: Yes

Reviewer #2: Yes

Reviewer #3: Yes

Reviewer #5: Yes

**********

5. Is the manuscript presented in an intelligible fashion and written in standard English?

PLOS ONE does not copyedit accepted manuscripts, so the language in submitted articles must be clear, correct, and unambiguous. Any typographical or grammatical errors should be corrected at revision, so please note any specific errors here.

Reviewer #1: Yes

Reviewer #2: Yes

Reviewer #3: Yes

Reviewer #5: Yes

**********

6. Review Comments to the Author

Please use the space provided to explain your answers to the questions above. You may also include additional comments for the author, including concerns about dual publication, research ethics, or publication ethics. (Please upload your review as an attachment if it exceeds 20,000 characters)

Reviewer #1: (No Response)

Reviewer #2: The authors responded well against the suggested comments, please accept this interesting manuscript.

Reviewer #3: The authors have responded correctly to all comments and the new version of manuscript has been significantly improved. I recommend it for publication in PLOS ONE.

Reviewer #5: Apply unified numbering system for the sections and subsections

All comments were considered

The authors of this paper made an appreciable effort

**********

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Reviewer #1: No

Reviewer #2: Yes: Afaq Ahmad

Reviewer #3: No

Reviewer #5: No

[NOTE: If reviewer comments were submitted as an attachment file, they will be attached to this email and accessible via the submission site. Please log into your account, locate the manuscript record, and check for the action link "View Attachments". If this link does not appear, there are no attachment files.]

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PLoS One. 2021 Mar 3;16(3):e0247599. doi: 10.1371/journal.pone.0247599.r004

Author response to Decision Letter 1


5 Feb 2021

Dear editor,

First of all, thank you and all reviewers for your recognition of my article. I have numbered the sections and subsections uniformly in accordance with the requirements of reviewer 5.

Dear reviewer 5,

Thank you again for reviewing and evaluating my manuscript, and the following is my reply and description.

Question: Apply unified numbering system for the sections and subsections.

Response: Thanks for the reviewer’s comments. Sorry for this problem. In the first submission of the manuscript, I gave a unified number to the sections, but I saw that the article templates on the website did not use a unified number, so I deleted it in the second submission. This point you raised is very valuable. Without a uniform section number, the article will appear unorganized. I have added it to the manuscript.

Attachment

Submitted filename: Response to Reviewers.docx

Decision Letter 2

Ahmed Mancy Mosa

10 Feb 2021

Investigation on cement-improved phyllite based on the vertical vibration compaction method

PONE-D-20-39942R2

Dear Dr. Fan,

We’re pleased to inform you that your manuscript has been judged scientifically suitable for publication and will be formally accepted for publication once it meets all outstanding technical requirements.

Within one week, you’ll receive an e-mail detailing the required amendments. When these have been addressed, you’ll receive a formal acceptance letter and your manuscript will be scheduled for publication.

An invoice for payment will follow shortly after the formal acceptance. To ensure an efficient process, please log into Editorial Manager at http://www.editorialmanager.com/pone/, click the 'Update My Information' link at the top of the page, and double check that your user information is up-to-date. If you have any billing related questions, please contact our Author Billing department directly at authorbilling@plos.org.

If your institution or institutions have a press office, please notify them about your upcoming paper to help maximize its impact. If they’ll be preparing press materials, please inform our press team as soon as possible -- no later than 48 hours after receiving the formal acceptance. Your manuscript will remain under strict press embargo until 2 pm Eastern Time on the date of publication. For more information, please contact onepress@plos.org.

Kind regards,

Ahmed Mancy Mosa, Ph.D.

Academic Editor

PLOS ONE

Additional Editor Comments (optional):

Reviewers' comments:

Reviewer's Responses to Questions

Comments to the Author

1. If the authors have adequately addressed your comments raised in a previous round of review and you feel that this manuscript is now acceptable for publication, you may indicate that here to bypass the “Comments to the Author” section, enter your conflict of interest statement in the “Confidential to Editor” section, and submit your "Accept" recommendation.

Reviewer #5: All comments have been addressed

**********

2. Is the manuscript technically sound, and do the data support the conclusions?

The manuscript must describe a technically sound piece of scientific research with data that supports the conclusions. Experiments must have been conducted rigorously, with appropriate controls, replication, and sample sizes. The conclusions must be drawn appropriately based on the data presented.

Reviewer #5: Yes

**********

3. Has the statistical analysis been performed appropriately and rigorously?

Reviewer #5: N/A

**********

4. Have the authors made all data underlying the findings in their manuscript fully available?

The PLOS Data policy requires authors to make all data underlying the findings described in their manuscript fully available without restriction, with rare exception (please refer to the Data Availability Statement in the manuscript PDF file). The data should be provided as part of the manuscript or its supporting information, or deposited to a public repository. For example, in addition to summary statistics, the data points behind means, medians and variance measures should be available. If there are restrictions on publicly sharing data—e.g. participant privacy or use of data from a third party—those must be specified.

Reviewer #5: Yes

**********

5. Is the manuscript presented in an intelligible fashion and written in standard English?

PLOS ONE does not copyedit accepted manuscripts, so the language in submitted articles must be clear, correct, and unambiguous. Any typographical or grammatical errors should be corrected at revision, so please note any specific errors here.

Reviewer #5: Yes

**********

6. Review Comments to the Author

Please use the space provided to explain your answers to the questions above. You may also include additional comments for the author, including concerns about dual publication, research ethics, or publication ethics. (Please upload your review as an attachment if it exceeds 20,000 characters)

Reviewer #5: The authors of this paper made an appreciable effort

All comments have been addressed

Recommendation is accept

**********

7. PLOS authors have the option to publish the peer review history of their article (what does this mean?). If published, this will include your full peer review and any attached files.

If you choose “no”, your identity will remain anonymous but your review may still be made public.

Do you want your identity to be public for this peer review? For information about this choice, including consent withdrawal, please see our Privacy Policy.

Reviewer #5: No

Acceptance letter

Ahmed Mancy Mosa

19 Feb 2021

PONE-D-20-39942R2

Investigation on cement-improved phyllite based on the vertical vibration compaction method

Dear Dr. Fan:

I'm pleased to inform you that your manuscript has been deemed suitable for publication in PLOS ONE. Congratulations! Your manuscript is now with our production department.

If your institution or institutions have a press office, please let them know about your upcoming paper now to help maximize its impact. If they'll be preparing press materials, please inform our press team within the next 48 hours. Your manuscript will remain under strict press embargo until 2 pm Eastern Time on the date of publication. For more information please contact onepress@plos.org.

If we can help with anything else, please email us at plosone@plos.org.

Thank you for submitting your work to PLOS ONE and supporting open access.

Kind regards,

PLOS ONE Editorial Office Staff

on behalf of

Dr. Ahmed Mancy Mosa

Academic Editor

PLOS ONE

Associated Data

    This section collects any data citations, data availability statements, or supplementary materials included in this article.

    Supplementary Materials

    S1 Data

    (DOCX)

    Attachment

    Submitted filename: Response to Reviewers.docx

    Attachment

    Submitted filename: Response to Reviewers.docx

    Data Availability Statement

    All relevant data are within the paper and its Supporting information files.


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