Table 3.
Oxide |
Reactants |
Methodology |
Year |
T |
Shape |
Size[a] [nm] |
Size distribution [σd/d] |
Ref. |
---|---|---|---|---|---|---|---|---|
ZnO |
ZnCl2+NH4(CO2NH2) |
FIS |
1999 |
RT |
rods |
10–15[b] |
– |
[44] |
ZnO |
Zn(AcO)2+NaOH |
microreactor chip |
2014 |
60 °C |
spherical |
3–5 |
– |
[45] |
ZnO |
Zn(AcO)2+TMAOH (w/an organic acid) |
convective tangential micromixer+coil reactor |
2014 |
20–80 °C |
– |
3.7[c] |
0.11[c] |
[51] |
ZnO |
Zn(NO3)2+NaOH (microemulsions) |
micromixer+coil reactor |
2014 |
40–70 °C |
– |
10–20[d] |
– |
[49] |
ZnO |
Zn(NO3)2+NaOH |
microreactor chips |
2017 |
60 °C |
spheres |
10 nm |
– |
[46] |
|
|
|
|
|
spindles |
300–600 nm |
– |
|
ZnO |
Zn(AcO)2+NaOH |
droplet‐based mircroreactor |
2017 |
|
spherical |
49.6 |
0.16 |
[50] |
ZnO |
Zn(NO3)2+NaOH |
spiral microreactor |
2019 |
RT |
spheres |
583 |
0.21 |
[47] |
|
|
|
|
|
cubes |
153 |
0.24 |
[a] Calculated by TEM/SEM analysis. [b] Diameter. [c] At 20 °C. [d] The NPs size depended on the employed conditions (flow rate, T, zinc concentration) fairly monodispersed NPs were obtained in single runs.