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. 2022 Feb 17;28(14):e202104198. doi: 10.1002/chem.202104198

Figure 4.

Figure 4

a) Reaction kinetic plots to determine the order with respect to a) [PA] (0th order) b) and c) [Catalyst] and d) [CHO]. a) Reaction conditions: [cat]0:[CHD]0: [NA]0:[CHO]0=1 : 20 : 100 : 1000, [cat]0=10 mM, 100 °C. b)and c) Reaction conditions: [cat]x‐y:[CHD]0:[NA]0:[CHO]0=1–2 : 20 : 100 : 2000, [cat] x‐y=2.5 mM (x)–5 mM (y), 100 °C. d) [cat]0:[CHD]0:[NA]0:[CHO]0=1 : 20 : 180 : 150, [cat]0=5 mM in Tol (total volume 1.6 mL), 100 °C.