Natural djurleite with refined composition Cu_61.39S₃₂ revealing disorder of some Cu sites

The djurleite phase with composition Cu_61.39S₃₂ was refined from a natural twinned specimen and shows disorder of some of its Cu sites.

Abstract

A djurleite crystal was discovered from a natural sample originally labelled as chalcocite. The djurleite crystal under investigation has a refined composition of Cu_61.39S₃₂, thus revealing a Cu deficiency compared to the originally reported Cu₆₂S₃₂ phase [Evans (1979). Z. Kristallogr. 150, 299–320], where all atomic sites are reported to be fully occupied. In addition, the current refinement revealed a splitting of eight of the Cu sites into pairs.

Structure description

The Cu–S system has been the subject of structural research for nearly one century. Several well-defined compounds and their crystal structures have been reported, with high-chalcocite (Buerger & Wuensch, 1963 ▸), low-chalcocite and djurleite (Evans, 1979a ▸,b ▸) being the most prominent ones. Low-chalcocite and djurleite are difficult to distinguish, thus many samples labelled chalcocite represent in fact djurleite, or an intimately inter­grown mixture of low-chalcocite and djurleite (Evans, 1981 ▸). The existence of djurleite was not suspected until it was discovered and suggested to be of ortho­rhom­bic symmetry by Djurle (1958 ▸). This phase was later assigned as an independent mineral species (Roseboom, 1962 ▸; Morimoto, 1962 ▸). Further studies of this mineral revealed that the previously supposed space group of Pmmm is affected by systematic twinning and that djurleite actually crystallizes in the monoclinic space group P2₁/n (Takeda et al., 1967 ▸; Evans, 1979a ▸,b ▸). The final determination of the crystal structures of low-chalcocite and djurleite was accomplished by Evans (1979a ▸). Low-chalcocite from Bristol, Connecticut, crystallizes in space group P2₁/c and contains 48 formula units of Cu₂S [a = 15.246 (4), b = 11.884 (2), c = 13.494 (3) Å, β = 116.35 (1)°] while djurleite from the Ozark Lead Co. mine at Sweetwater, Missouri, contains eight formula units of Cu₃₁S₁₆ in space group P2₁/n [a = 26.897 (6), b= 15.745 (3), c= 13.565 (3) Å, β = 90.13 (3)°; Evans, 1979a ▸,b ▸]. All atoms in the above structure models were assumed to be fully occupied. However, there are some studies based on HRTEM revealing that there are vacancies of Cu in natural metadjurleite (Xu et al., 1991 ▸) or low-djurleite (Sun & Xue, 2001 ▸), but without a refined structure model. There are also some studies on synthetic copper-deficient copper sulfides, either considered as monoclinic djurleite (Yoon et al., 2015 ▸), or as cubic Cu₂S (Zhou et al., 2016 ▸.; Zhang et al., 2021 ▸).

Since the crystal structure of djurleite has been discussed in detail in the original description (Evans, 1979a ▸), here only the main differences are emphasized. For the present study, a crystal from a natural sample was used, revealing a refined composition of Cu_61.39S₃₂. In comparison with the original Cu₃₁S₁₆ model where all sites are ordered and fully occupied, eight Cu sites are split over two positions and one Cu site shows partial occupancy. The crystal under investigation used for the present study was twinned whereas that used for the original study was not reported to be twinned. The reported temperature of formation for the latter crystal was below 370 K.

Fig. 1 ▸ shows the overall atomic distribution of Cu_61.39S₃₂ in the unit cell. For simplicity, two different coordination polyhedra around Cu sites are highlighted, with a criterion of the Cu—S distances being less than 3.0 Å. Representative for the principal environment of Cu sites, Cu1 shows a triangular coordination by three S atoms (Fig. 2 ▸). Another environment of Cu sites is represented by Cu48, where the surrounding four S atoms form a distorted tetra­hedron, as shown in Fig. 3 ▸. The low-occupancy Cu12 site has the same environment as the Cu1 atom. The eight pairs of split Cu atoms have the same environment as Cu48, except the pairs Cu29A/B, Cu45A/B and Cu62A/B, which have the same environment as the Cu1 atom.

Figure 1.

The unit cell of Cu_61.39S₃₂, with sites Cu1 and Cu48 displayed with their different coordination environments as polyhedra.

Figure 2.

The environment of Cu1. Displacement ellipsoids are drawn at the 90% probability level. [Symmetry code: (i) x, y, z − 1.]

Figure 3.

The environment of Cu48. Displacement ellipsoids are drawn at the 90% probability level. [Symmetry code: (iii) x, y − 1, z.]

Synthesis and crystallization

Natural samples designated as chalcocite were purchased from Honghu Minerals (Hubei Province, China), Alibaba Taobao Co. Suitable single-crystal fragments were broken from a larger sample and glued on glass fibers for single-crystal X-ray diffraction experiments. Energy-dispersive X-ray spectroscopy measurements did not indicate the presence of elements other than Cu and S (see supporting information).

Refinement

Crystal data, data collection and structure refinement details are summarized in Table 1 ▸. Starting atomic coordinates and labels were adapted from the original structure investigation (Evans, 1979a ▸). The crystal under investigation was twinned by pseudo-merohedry, revealing a twin ratio of 0.92:0.08. Eight pairs of split Cu sites were assigned, in all cases assuming full occupancy using the same anisotropic displacement parameters (EADP) for each pair: Cu29A/Cu29B [occupancy ratio 0.808 (12)/0.192 (12)], Cu36A/Cu36B [0.815 (15)/0.185 (15)], Cu45A/Cu45B [0.860 (18)/0.140 (18)], Cu47A/Cu47B [0.561 (15)/0.439 (15)], Cu51A/Cu51B [0.580 (9)/0.480 (9)], Cu54A/Cu54B [0.770 (6)/0.230 (6)], Cu60A/Cu60B [0.687 (10)/0.313 (10)], and Cu62A/Cu62B [0.804 (6)/0.196 (6)]. In addition, the Cu12 site shows an occupancy less than 1, with a refined site occupation of 0.385 (9). The maximum residual electron density in the final difference-Fourier map is located 1.665 Å from atom Cu12 and the minimum electron density is located 0.487 Å from atom Cu51B.

Table 1. Experimental details.

Crystal data
Chemical formula	Cu61.39S32
M r	4926.40
Crystal system, space group	Monoclinic, P21/n
Temperature (K)	296
a, b, c (Å)	26.850 (1), 15.6862 (6), 13.5175 (6)
β (°)	90.062 (2)
V (Å3)	5693.2 (4)
Z	4
Radiation type	Mo Kα
μ (mm−1)	23.54
Crystal size (mm)	0.11 × 0.07 × 0.07
Data collection
Diffractometer	Bruker D8 Venture Photon 100 CMOS
Absorption correction	Multi-scan (SADABS; Krause et al., 2015 ▸)
T min, T max	0.526, 0.745
No. of measured, independent and observed [I > 2σ(I)] reflections	19946, 10098, 7077
R int	0.062
(sin θ/λ)max (Å−1)	0.597
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S	0.067, 0.132, 0.95
No. of reflections	10098
No. of parameters	881
Δρmax, Δρmin (e Å−3)	2.03, −1.59

Computer programs: APEX3 and SAINT (Bruker, 2015 ▸), SHELXT (Sheldrick, 2015a ▸), SHELXL (Sheldrick, 2015b ▸), DIAMOND (Brandenburg & Putz, 2017 ▸) and publCIF (Westrip, 2010 ▸).

Supplementary Material

CCDC reference: 2184537

Additional supporting information: crystallographic information; 3D view; checkCIF report

full crystallographic data

Crystal data

Cu61.39S32	F(000) = 9169
Mr = 4926.40	Dx = 5.748 Mg m−3
Monoclinic, P21/n	Mo Kα radiation, λ = 0.71073 Å
a = 26.850 (1) Å	Cell parameters from 9872 reflections
b = 15.6862 (6) Å	θ = 2.6–25.0°
c = 13.5175 (6) Å	µ = 23.54 mm−1
β = 90.062 (2)°	T = 296 K
V = 5693.2 (4) Å3	Fragment, dark grey
Z = 4	0.11 × 0.07 × 0.07 mm

Data collection

Bruker D8 Venture Photon 100 CMOS diffractometer	7077 reflections with I > 2σ(I)
phi and ω scans	Rint = 0.062
Absorption correction: multi-scan (SADABS; Krause et al., 2015)	θmax = 25.1°, θmin = 2.1°
Tmin = 0.526, Tmax = 0.745	h = 0→31
19946 measured reflections	k = −18→18
10098 independent reflections	l = −16→16

Refinement

Refinement on F2	881 parameters
Least-squares matrix: full	0 restraints
R[F2 > 2σ(F2)] = 0.067	w = 1/[σ2(Fo2) + (0.0431P)2 + 226.7933P] where P = (Fo2 + 2Fc2)/3
wR(F2) = 0.132	(Δ/σ)max = 0.050
S = 0.95	Δρmax = 2.03 e Å−3
10098 reflections	Δρmin = −1.59 e Å−3

Special details

Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes.

Refinement. Refined as a 2-component inversion twin.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq	Occ. (<1)
Cu1	0.05802 (8)	0.49828 (14)	0.00493 (17)	0.0241 (5)
Cu2	0.06237 (8)	0.75278 (15)	0.00218 (17)	0.0254 (5)
Cu3	0.06563 (8)	0.12723 (14)	0.24690 (16)	0.0218 (5)
Cu4	0.06530 (9)	0.99009 (15)	0.49282 (17)	0.0283 (6)
Cu5	0.05524 (8)	0.24246 (14)	0.50056 (17)	0.0246 (5)
Cu6	0.06408 (8)	0.50787 (14)	0.49479 (17)	0.0258 (6)
Cu7	0.06740 (8)	0.11292 (14)	0.75840 (16)	0.0205 (5)
Cu8	0.06409 (9)	0.36157 (15)	0.74230 (18)	0.0291 (6)
Cu9	0.06786 (8)	0.61680 (14)	0.75346 (16)	0.0201 (5)
Cu10	0.18823 (7)	0.99835 (14)	0.99856 (16)	0.0191 (5)
Cu11	0.19240 (8)	0.25413 (14)	0.99740 (17)	0.0237 (5)
Cu12	0.1821 (2)	0.7453 (4)	0.9908 (5)	0.032 (3)	0.385 (9)
Cu13	0.18979 (10)	0.12498 (17)	0.24019 (19)	0.0382 (6)
Cu14	0.19304 (8)	0.62310 (15)	0.24707 (17)	0.0262 (5)
Cu15	0.18958 (7)	0.87104 (14)	0.24350 (16)	0.0200 (5)
Cu16	0.18134 (8)	0.99834 (16)	0.48732 (18)	0.0297 (6)
Cu17	0.19465 (8)	0.75158 (14)	0.49793 (17)	0.0224 (5)
Cu18	0.18129 (8)	0.13355 (14)	0.75600 (17)	0.0245 (5)
Cu19	0.18859 (8)	0.38481 (14)	0.74382 (17)	0.0251 (5)
Cu20	0.19348 (9)	0.87522 (15)	0.74492 (18)	0.0295 (6)
Cu21	0.01578 (7)	0.15373 (14)	0.06607 (16)	0.0197 (5)
Cu22	0.01827 (8)	0.38946 (14)	0.14172 (17)	0.0230 (5)
Cu23	0.01800 (8)	0.63341 (15)	0.12577 (19)	0.0272 (6)
Cu24	0.01467 (7)	0.87550 (14)	0.12492 (17)	0.0203 (5)
Cu25	0.01418 (8)	0.28830 (14)	0.30698 (17)	0.0213 (5)
Cu26	0.01536 (8)	0.46557 (15)	0.32197 (18)	0.0267 (6)
Cu27	0.01788 (8)	0.73844 (18)	0.3340 (2)	0.0370 (7)
Cu28	0.01314 (8)	0.10450 (16)	0.5913 (2)	0.0355 (7)
Cu29A	0.01089 (14)	0.3892 (2)	0.5656 (4)	0.0255 (12)	0.808 (12)
Cu29B	0.0002 (6)	0.3741 (11)	0.5212 (18)	0.0255 (12)	0.192 (12)
Cu30	0.01741 (8)	0.85988 (15)	0.6313 (2)	0.0304 (6)
Cu31	0.01468 (7)	0.96688 (13)	0.81303 (16)	0.0189 (5)
Cu32	0.10780 (7)	0.08082 (14)	0.07141 (16)	0.0186 (5)
Cu33	0.10697 (7)	0.34458 (15)	0.06377 (17)	0.0243 (5)
Cu34	0.10323 (7)	0.90973 (14)	0.04937 (16)	0.0191 (5)
Cu35	0.10851 (8)	0.53484 (16)	0.31335 (17)	0.0257 (6)
Cu36A	0.11275 (12)	0.7659 (3)	0.3107 (6)	0.0371 (14)	0.815 (15)
Cu36B	0.1151 (6)	0.7567 (14)	0.361 (2)	0.0371 (14)	0.185 (15)
Cu37	0.10822 (8)	0.95624 (16)	0.31530 (17)	0.0267 (6)
Cu38	0.10853 (7)	0.65868 (14)	0.56067 (16)	0.0202 (5)
Cu39	0.10823 (8)	0.83533 (16)	0.55721 (19)	0.0316 (6)
Cu40	0.10540 (8)	0.00731 (14)	0.88738 (17)	0.0207 (5)
Cu41	0.10783 (8)	0.24996 (15)	0.87892 (19)	0.0275 (6)
Cu42	0.11246 (9)	0.47519 (18)	0.8395 (2)	0.0447 (7)
Cu43	0.10950 (8)	0.77570 (15)	0.81362 (17)	0.0237 (5)
Cu44	0.13962 (7)	0.50212 (14)	0.12734 (17)	0.0239 (5)
Cu45A	0.13951 (17)	0.7440 (5)	0.1307 (4)	0.0431 (15)	0.860 (18)
Cu45B	0.1290 (10)	0.708 (3)	0.149 (3)	0.0431 (15)	0.140 (18)
Cu46	0.14045 (9)	0.16731 (19)	0.4294 (2)	0.0438 (7)
Cu47A	0.1400 (4)	0.3927 (8)	0.4268 (10)	0.0390 (19)	0.561 (15)
Cu47B	0.1398 (5)	0.3538 (9)	0.4288 (13)	0.0390 (19)	0.439 (15)
Cu48	0.14012 (8)	0.00475 (15)	0.66288 (19)	0.0286 (6)
Cu49	0.14479 (8)	0.25517 (15)	0.6138 (2)	0.0314 (6)
Cu50	0.14618 (8)	0.50105 (15)	0.6134 (2)	0.0305 (6)
Cu51A	0.1412 (2)	0.6334 (6)	0.9080 (6)	0.0414 (16)	0.580 (9)
Cu51B	0.1421 (4)	0.5940 (8)	0.9353 (8)	0.0414 (16)	0.420 (9)
Cu52	0.22434 (8)	0.28965 (16)	0.18953 (18)	0.0291 (6)
Cu53	0.23055 (8)	0.46425 (15)	0.20081 (18)	0.0261 (6)
Cu54A	0.23507 (12)	0.1357 (3)	0.4194 (3)	0.0525 (13)	0.770 (6)
Cu54B	0.2463 (4)	0.1889 (11)	0.3907 (12)	0.0525 (13)	0.230 (6)
Cu55	0.23404 (9)	0.3859 (2)	0.3949 (3)	0.0576 (9)
Cu56	0.23085 (8)	0.59121 (16)	0.43753 (17)	0.0270 (6)
Cu57	0.23338 (8)	0.54026 (15)	0.69488 (18)	0.0274 (6)
Cu58	0.23099 (8)	0.71556 (15)	0.68504 (18)	0.0245 (5)
Cu59	0.23013 (8)	0.41014 (17)	0.93999 (19)	0.0343 (6)
Cu60A	0.23741 (15)	0.6351 (3)	0.8782 (5)	0.0335 (14)	0.687 (10)
Cu60B	0.2353 (4)	0.6181 (8)	0.9294 (11)	0.0335 (14)	0.313 (10)
Cu61	0.23358 (10)	0.8427 (2)	0.9271 (3)	0.0686 (11)
Cu62A	0.12704 (11)	0.2611 (2)	0.2464 (3)	0.0336 (11)	0.804 (6)
Cu62B	0.1372 (5)	0.2355 (9)	0.1835 (14)	0.0336 (11)	0.196 (6)
S1	0.06574 (14)	0.9910 (3)	0.1732 (3)	0.0126 (9)
S2	0.05702 (14)	0.2565 (3)	0.1614 (3)	0.0136 (9)
S3	0.05843 (14)	0.5128 (3)	0.1762 (3)	0.0132 (9)
S4	0.05761 (14)	0.7543 (3)	0.1732 (3)	0.0148 (9)
S5	0.06260 (15)	0.1181 (3)	0.4159 (3)	0.0160 (10)
S6	0.05801 (14)	0.3714 (3)	0.4213 (3)	0.0148 (9)
S7	0.07091 (14)	0.6340 (3)	0.4117 (3)	0.0130 (9)
S8	0.06749 (15)	0.8621 (3)	0.4134 (3)	0.0175 (10)
S9	0.05634 (14)	0.9928 (3)	0.6624 (3)	0.0127 (9)
S10	0.06507 (14)	0.2353 (3)	0.6692 (3)	0.0156 (10)
S11	0.06584 (15)	0.4910 (3)	0.6667 (3)	0.0166 (10)
S12	0.06836 (14)	0.7467 (3)	0.6704 (3)	0.0142 (9)
S13	0.06560 (14)	0.1321 (3)	0.9276 (3)	0.0106 (9)
S14	0.06372 (14)	0.3742 (3)	0.9150 (3)	0.0132 (9)
S15	0.05939 (15)	0.6254 (3)	0.9224 (3)	0.0191 (10)
S16	0.06580 (14)	0.8742 (3)	0.9023 (3)	0.0119 (9)
S17	0.18785 (15)	0.1288 (3)	0.0752 (3)	0.0164 (10)
S18	0.18758 (14)	0.3836 (3)	0.0823 (3)	0.0162 (10)
S19	0.18235 (15)	0.6249 (3)	0.0769 (3)	0.0157 (9)
S20	0.18465 (15)	0.8681 (3)	0.0736 (3)	0.0152 (9)
S21	0.18876 (15)	0.0012 (3)	0.3234 (4)	0.0192 (10)
S22	0.19085 (18)	0.2561 (3)	0.3414 (3)	0.0248 (11)
S23	0.18798 (15)	0.4987 (3)	0.3416 (3)	0.0163 (10)
S24	0.19465 (15)	0.7475 (3)	0.3320 (3)	0.0163 (10)
S25	0.18212 (14)	0.1233 (3)	0.5801 (3)	0.0152 (10)
S26	0.18557 (15)	0.3751 (3)	0.5748 (3)	0.0194 (10)
S27	0.19055 (14)	0.6241 (3)	0.5811 (3)	0.0136 (9)
S28	0.18839 (15)	0.8785 (3)	0.5788 (3)	0.0198 (10)
S29	0.18594 (15)	1.0002 (3)	0.8265 (3)	0.0151 (10)
S30	0.18823 (15)	0.2604 (3)	0.8296 (3)	0.0171 (10)
S31	0.19344 (15)	0.5075 (3)	0.8398 (3)	0.0151 (10)
S32	0.19131 (15)	0.7493 (3)	0.8303 (3)	0.0161 (10)

Atomic displacement parameters (Ų)

	U11	U22	U33	U12	U13	U23
Cu1	0.0320 (13)	0.0188 (13)	0.0214 (14)	0.0006 (10)	−0.0004 (10)	−0.0054 (10)
Cu2	0.0297 (12)	0.0247 (14)	0.0217 (14)	−0.0014 (10)	0.0000 (10)	0.0059 (11)
Cu3	0.0284 (12)	0.0182 (12)	0.0189 (13)	−0.0031 (10)	0.0024 (9)	0.0010 (10)
Cu4	0.0491 (15)	0.0183 (13)	0.0176 (14)	0.0029 (11)	0.0057 (11)	−0.0028 (11)
Cu5	0.0326 (13)	0.0165 (12)	0.0248 (14)	0.0034 (10)	0.0007 (10)	0.0010 (11)
Cu6	0.0338 (13)	0.0209 (13)	0.0228 (15)	−0.0069 (10)	−0.0056 (10)	0.0069 (11)
Cu7	0.0321 (12)	0.0162 (12)	0.0132 (12)	−0.0013 (9)	−0.0001 (9)	−0.0005 (10)
Cu8	0.0454 (14)	0.0197 (13)	0.0221 (14)	0.0005 (11)	−0.0026 (11)	−0.0012 (11)
Cu9	0.0237 (11)	0.0160 (12)	0.0206 (13)	−0.0003 (9)	0.0016 (9)	−0.0004 (10)
Cu10	0.0210 (11)	0.0154 (12)	0.0208 (13)	0.0001 (9)	0.0001 (9)	−0.0021 (10)
Cu11	0.0267 (12)	0.0202 (13)	0.0240 (14)	−0.0028 (10)	−0.0047 (10)	−0.0005 (11)
Cu12	0.047 (4)	0.027 (4)	0.021 (4)	−0.008 (3)	0.006 (3)	0.005 (3)
Cu13	0.0548 (16)	0.0343 (16)	0.0256 (15)	−0.0014 (13)	−0.0020 (12)	0.0046 (13)
Cu14	0.0337 (13)	0.0229 (13)	0.0220 (14)	−0.0049 (10)	0.0004 (10)	0.0007 (11)
Cu15	0.0220 (11)	0.0186 (12)	0.0194 (13)	−0.0004 (9)	−0.0019 (9)	−0.0010 (10)
Cu16	0.0369 (14)	0.0256 (14)	0.0265 (15)	0.0024 (11)	0.0038 (11)	0.0022 (11)
Cu17	0.0287 (12)	0.0199 (13)	0.0185 (13)	0.0022 (10)	0.0026 (9)	0.0012 (10)
Cu18	0.0296 (12)	0.0163 (12)	0.0276 (14)	−0.0003 (10)	−0.0044 (10)	−0.0030 (11)
Cu19	0.0365 (13)	0.0198 (13)	0.0189 (13)	0.0027 (10)	−0.0036 (10)	−0.0012 (10)
Cu20	0.0367 (13)	0.0211 (13)	0.0308 (15)	0.0040 (10)	0.0002 (11)	−0.0037 (11)
Cu21	0.0148 (11)	0.0248 (13)	0.0195 (13)	−0.0017 (9)	0.0026 (9)	0.0007 (10)
Cu22	0.0206 (11)	0.0188 (13)	0.0295 (14)	−0.0036 (9)	0.0038 (9)	−0.0018 (11)
Cu23	0.0206 (12)	0.0206 (13)	0.0406 (16)	0.0002 (10)	−0.0021 (10)	0.0032 (12)
Cu24	0.0120 (10)	0.0219 (12)	0.0269 (13)	−0.0003 (9)	0.0010 (9)	−0.0026 (11)
Cu25	0.0211 (12)	0.0203 (12)	0.0225 (13)	−0.0017 (9)	−0.0002 (9)	0.0012 (10)
Cu26	0.0225 (12)	0.0279 (14)	0.0297 (15)	0.0008 (10)	−0.0066 (10)	0.0017 (12)
Cu27	0.0157 (12)	0.0515 (17)	0.0438 (17)	−0.0020 (11)	−0.0002 (11)	0.0080 (14)
Cu28	0.0247 (13)	0.0284 (14)	0.0535 (19)	0.0084 (11)	−0.0077 (12)	−0.0010 (13)
Cu29A	0.0198 (17)	0.0252 (18)	0.032 (3)	0.0002 (13)	0.0107 (18)	0.0028 (19)
Cu29B	0.0198 (17)	0.0252 (18)	0.032 (3)	0.0002 (13)	0.0107 (18)	0.0028 (19)
Cu30	0.0167 (11)	0.0204 (13)	0.0541 (17)	0.0026 (10)	0.0029 (11)	0.0101 (12)
Cu31	0.0148 (11)	0.0180 (12)	0.0239 (13)	0.0017 (9)	0.0001 (9)	0.0039 (10)
Cu32	0.0194 (11)	0.0186 (12)	0.0180 (13)	0.0003 (9)	0.0050 (9)	−0.0018 (10)
Cu33	0.0164 (11)	0.0279 (14)	0.0284 (14)	−0.0017 (9)	0.0007 (10)	0.0006 (11)
Cu34	0.0176 (11)	0.0210 (12)	0.0187 (13)	−0.0016 (9)	0.0010 (9)	−0.0039 (10)
Cu35	0.0175 (11)	0.0396 (15)	0.0201 (13)	−0.0001 (10)	−0.0010 (9)	−0.0055 (11)
Cu36A	0.0159 (14)	0.057 (2)	0.039 (4)	0.0053 (13)	−0.0004 (18)	−0.001 (2)
Cu36B	0.0159 (14)	0.057 (2)	0.039 (4)	0.0053 (13)	−0.0004 (18)	−0.001 (2)
Cu37	0.0210 (12)	0.0362 (15)	0.0228 (14)	−0.0022 (10)	0.0009 (10)	0.0028 (12)
Cu38	0.0208 (11)	0.0206 (12)	0.0191 (13)	0.0001 (9)	−0.0006 (9)	−0.0037 (10)
Cu39	0.0200 (12)	0.0378 (15)	0.0371 (16)	0.0023 (10)	0.0014 (11)	0.0151 (12)
Cu40	0.0213 (11)	0.0171 (12)	0.0237 (14)	0.0024 (9)	−0.0047 (9)	0.0003 (10)
Cu41	0.0197 (12)	0.0229 (13)	0.0397 (16)	−0.0019 (10)	0.0021 (10)	0.0037 (12)
Cu42	0.0240 (13)	0.0472 (18)	0.063 (2)	−0.0169 (12)	0.0060 (13)	−0.0022 (15)
Cu43	0.0173 (11)	0.0266 (13)	0.0271 (14)	0.0046 (10)	−0.0021 (10)	−0.0081 (11)
Cu44	0.0177 (11)	0.0253 (13)	0.0286 (15)	0.0041 (10)	0.0003 (10)	−0.0037 (11)
Cu45A	0.0188 (18)	0.032 (4)	0.078 (3)	0.002 (2)	−0.0005 (17)	−0.019 (2)
Cu45B	0.0188 (18)	0.032 (4)	0.078 (3)	0.002 (2)	−0.0005 (17)	−0.019 (2)
Cu46	0.0242 (14)	0.0532 (19)	0.0541 (19)	−0.0117 (12)	0.0112 (12)	0.0015 (15)
Cu47A	0.0180 (14)	0.052 (6)	0.047 (2)	−0.001 (5)	−0.0026 (13)	0.012 (6)
Cu47B	0.0180 (14)	0.052 (6)	0.047 (2)	−0.001 (5)	−0.0026 (13)	0.012 (6)
Cu48	0.0189 (12)	0.0289 (14)	0.0380 (16)	−0.0011 (10)	0.0005 (10)	−0.0056 (12)
Cu49	0.0257 (13)	0.0228 (14)	0.0459 (17)	−0.0041 (10)	0.0010 (11)	0.0037 (12)
Cu50	0.0225 (12)	0.0217 (14)	0.0474 (17)	−0.0054 (10)	−0.0065 (11)	0.0078 (12)
Cu51A	0.0183 (15)	0.067 (6)	0.039 (4)	0.000 (3)	0.001 (2)	0.010 (3)
Cu51B	0.0183 (15)	0.067 (6)	0.039 (4)	0.000 (3)	0.001 (2)	0.010 (3)
Cu52	0.0261 (13)	0.0328 (15)	0.0285 (15)	0.0008 (10)	0.0046 (10)	0.0031 (12)
Cu53	0.0184 (12)	0.0289 (14)	0.0308 (15)	0.0022 (10)	−0.0019 (10)	−0.0042 (12)
Cu54A	0.0168 (17)	0.074 (4)	0.066 (3)	0.0043 (19)	−0.0020 (16)	0.019 (3)
Cu54B	0.0168 (17)	0.074 (4)	0.066 (3)	0.0043 (19)	−0.0020 (16)	0.019 (3)
Cu55	0.0190 (14)	0.068 (2)	0.086 (2)	0.0124 (13)	0.0022 (14)	0.0393 (19)
Cu56	0.0181 (12)	0.0362 (15)	0.0267 (14)	−0.0022 (10)	0.0018 (10)	−0.0042 (12)
Cu57	0.0207 (12)	0.0295 (14)	0.0319 (15)	−0.0015 (10)	−0.0047 (10)	0.0087 (12)
Cu58	0.0210 (12)	0.0254 (13)	0.0271 (14)	−0.0043 (10)	−0.0023 (10)	−0.0033 (11)
Cu59	0.0249 (13)	0.0423 (16)	0.0357 (16)	0.0023 (11)	0.0079 (11)	0.0120 (13)
Cu60A	0.0173 (15)	0.033 (2)	0.050 (4)	0.0003 (15)	−0.004 (2)	0.000 (3)
Cu60B	0.0173 (15)	0.033 (2)	0.050 (4)	0.0003 (15)	−0.004 (2)	0.000 (3)
Cu61	0.0277 (16)	0.101 (3)	0.077 (2)	0.0009 (16)	−0.0182 (15)	−0.052 (2)
Cu62A	0.0234 (16)	0.0261 (19)	0.051 (3)	−0.0025 (13)	−0.0185 (16)	0.0017 (18)
Cu62B	0.0234 (16)	0.0261 (19)	0.051 (3)	−0.0025 (13)	−0.0185 (16)	0.0017 (18)
S1	0.009 (2)	0.014 (2)	0.015 (2)	0.0002 (16)	0.0011 (16)	−0.0002 (19)
S2	0.013 (2)	0.008 (2)	0.020 (3)	−0.0007 (16)	−0.0007 (17)	0.0054 (19)
S3	0.012 (2)	0.014 (2)	0.014 (2)	−0.0026 (17)	−0.0036 (17)	−0.0003 (19)
S4	0.015 (2)	0.017 (2)	0.013 (2)	0.0006 (18)	−0.0006 (17)	0.0037 (19)
S5	0.018 (2)	0.014 (2)	0.015 (2)	−0.0027 (17)	−0.0028 (17)	0.0001 (19)
S6	0.014 (2)	0.015 (2)	0.016 (2)	−0.0014 (18)	−0.0007 (17)	0.004 (2)
S7	0.015 (2)	0.013 (2)	0.011 (2)	−0.0028 (17)	−0.0038 (16)	0.0035 (19)
S8	0.018 (2)	0.015 (2)	0.019 (3)	−0.0024 (18)	−0.0019 (18)	−0.006 (2)
S9	0.014 (2)	0.013 (2)	0.011 (2)	0.0000 (17)	0.0012 (17)	0.0030 (18)
S10	0.011 (2)	0.017 (2)	0.018 (3)	0.0006 (17)	0.0014 (17)	0.001 (2)
S11	0.016 (2)	0.015 (2)	0.019 (3)	−0.0028 (18)	0.0025 (18)	−0.002 (2)
S12	0.010 (2)	0.016 (2)	0.016 (3)	0.0017 (17)	0.0024 (16)	0.0014 (19)
S13	0.010 (2)	0.014 (2)	0.007 (2)	−0.0007 (17)	−0.0004 (15)	−0.0001 (19)
S14	0.012 (2)	0.014 (2)	0.014 (2)	0.0017 (17)	−0.0018 (16)	0.0031 (19)
S15	0.020 (2)	0.023 (3)	0.014 (2)	0.0034 (19)	−0.0006 (18)	0.002 (2)
S16	0.010 (2)	0.014 (2)	0.012 (2)	−0.0001 (16)	−0.0051 (16)	0.0028 (19)
S17	0.016 (2)	0.015 (2)	0.019 (3)	−0.0034 (18)	0.0020 (17)	0.000 (2)
S18	0.011 (2)	0.015 (2)	0.023 (3)	0.0034 (17)	−0.0021 (17)	−0.003 (2)
S19	0.018 (2)	0.014 (2)	0.014 (2)	−0.0005 (18)	0.0021 (17)	0.001 (2)
S20	0.018 (2)	0.014 (2)	0.014 (2)	−0.0006 (18)	−0.0016 (17)	0.000 (2)
S21	0.016 (2)	0.015 (2)	0.027 (3)	−0.0002 (18)	−0.0015 (19)	−0.004 (2)
S22	0.047 (3)	0.015 (2)	0.013 (3)	−0.006 (2)	0.006 (2)	−0.004 (2)
S23	0.015 (2)	0.014 (2)	0.020 (3)	−0.0012 (17)	0.0019 (18)	−0.001 (2)
S24	0.013 (2)	0.016 (2)	0.019 (3)	−0.0003 (17)	−0.0010 (17)	0.007 (2)
S25	0.012 (2)	0.015 (2)	0.018 (3)	−0.0005 (17)	−0.0005 (17)	0.005 (2)
S26	0.021 (2)	0.021 (3)	0.017 (3)	−0.0040 (19)	0.0009 (18)	0.000 (2)
S27	0.015 (2)	0.012 (2)	0.014 (2)	−0.0024 (17)	0.0008 (17)	0.0075 (19)
S28	0.019 (2)	0.021 (3)	0.019 (3)	−0.0060 (19)	−0.0024 (18)	0.004 (2)
S29	0.016 (2)	0.017 (2)	0.012 (2)	−0.0006 (18)	0.0036 (17)	−0.0014 (19)
S30	0.018 (2)	0.014 (2)	0.020 (3)	0.0010 (18)	0.0029 (18)	−0.001 (2)
S31	0.014 (2)	0.015 (2)	0.017 (3)	−0.0023 (17)	0.0004 (17)	−0.0054 (19)
S32	0.017 (2)	0.016 (2)	0.015 (3)	0.0004 (18)	−0.0012 (17)	−0.006 (2)

Geometric parameters (Å, º)

Cu1—S15i	2.285 (5)	Cu24—Cu34	2.644 (3)
Cu1—S14i	2.301 (5)	Cu24—Cu31xi	2.727 (3)
Cu1—S3	2.326 (5)	Cu25—S12iv	2.304 (4)
Cu1—Cu42i	2.697 (4)	Cu25—S2	2.335 (5)
Cu1—Cu22	2.734 (3)	Cu25—S6	2.338 (5)
Cu1—Cu44	2.745 (3)	Cu25—Cu30iv	2.612 (3)
Cu1—Cu33	2.858 (3)	Cu25—Cu26	2.788 (3)
Cu1—Cu51Bi	2.872 (11)	Cu26—S11iv	2.290 (5)
Cu1—Cu23	2.884 (3)	Cu26—S6	2.301 (5)
Cu2—S15i	2.272 (5)	Cu26—S3	2.403 (5)
Cu2—S4	2.315 (5)	Cu26—Cu35	2.729 (3)
Cu2—S16i	2.336 (5)	Cu26—Cu29Aiv	2.829 (5)
Cu2—Cu45A	2.705 (4)	Cu27—S10iv	2.265 (4)
Cu2—Cu21ii	2.720 (3)	Cu27—S7	2.411 (5)
Cu2—Cu45B	2.77 (3)	Cu27—S4	2.435 (5)
Cu2—Cu34	2.770 (3)	Cu27—Cu29Aiv	2.539 (4)
Cu2—Cu23	2.779 (3)	Cu27—S8	2.586 (5)
Cu2—Cu24	2.847 (3)	Cu27—Cu36A	2.603 (4)
Cu2—Cu43i	2.870 (3)	Cu27—Cu36B	2.652 (17)
Cu3—S5	2.291 (5)	Cu27—Cu29Biv	2.682 (18)
Cu3—S2	2.346 (5)	Cu27—Cu28iv	2.790 (4)
Cu3—S1iii	2.357 (5)	Cu28—S8iv	2.228 (5)
Cu3—Cu62A	2.670 (4)	Cu28—S9iii	2.310 (5)
Cu3—Cu62B	2.706 (14)	Cu28—S10	2.694 (5)
Cu3—Cu32	2.729 (3)	Cu28—S5	2.727 (5)
Cu3—Cu31iv	2.735 (3)	Cu29A—S7iv	2.248 (5)
Cu3—Cu30iv	2.781 (3)	Cu29A—S6	2.343 (6)
Cu3—Cu21	2.816 (3)	Cu29A—S11	2.567 (7)
Cu3—Cu25	2.992 (3)	Cu29B—S6	2.059 (17)
Cu3—Cu37iii	3.058 (3)	Cu29B—S7iv	2.118 (16)
Cu4—S5v	2.262 (5)	Cu30—S5iv	2.267 (5)
Cu4—S8	2.278 (5)	Cu30—S12	2.302 (5)
Cu4—S9	2.305 (5)	Cu30—S9	2.370 (5)
Cu4—Cu28v	2.638 (3)	Cu30—Cu39	2.665 (3)
Cu4—Cu37	2.715 (3)	Cu30—Cu31	2.976 (3)
Cu4—Cu28iv	2.815 (3)	Cu31—S1xi	2.266 (4)
Cu4—Cu39	2.824 (3)	Cu31—S16	2.335 (4)
Cu4—Cu30	3.055 (3)	Cu31—S9	2.360 (5)
Cu4—Cu48v	3.060 (3)	Cu31—Cu40v	2.709 (3)
Cu5—S5	2.271 (5)	Cu32—S1iii	2.271 (5)
Cu5—S6	2.290 (5)	Cu32—S17	2.278 (4)
Cu5—S10	2.297 (5)	Cu32—S13i	2.388 (4)
Cu5—Cu29B	2.556 (16)	Cu32—Cu34iii	2.703 (3)
Cu5—Cu28	2.733 (3)	Cu32—Cu40i	2.742 (3)
Cu5—Cu29A	2.737 (5)	Cu32—Cu62B	2.968 (16)
Cu5—Cu46	2.748 (3)	Cu33—S18	2.263 (4)
Cu5—Cu49	2.856 (3)	Cu33—S2	2.335 (5)
Cu5—Cu25	2.928 (3)	Cu33—S14i	2.368 (5)
Cu5—Cu27iv	2.993 (3)	Cu33—Cu62B	2.491 (14)
Cu5—Cu47B	3.024 (14)	Cu33—Cu44	2.759 (3)
Cu6—S7	2.283 (5)	Cu33—Cu62A	2.845 (4)
Cu6—S11	2.339 (5)	Cu33—Cu41i	2.906 (3)
Cu6—S6	2.366 (5)	Cu34—S16i	2.295 (4)
Cu6—Cu29A	2.535 (4)	Cu34—S20	2.305 (4)
Cu6—Cu29Biv	2.539 (16)	Cu34—S1	2.334 (5)
Cu6—Cu29Aiv	2.706 (4)	Cu34—Cu40xii	2.672 (3)
Cu6—Cu50	2.727 (3)	Cu34—Cu45A	2.985 (7)
Cu6—Cu29B	2.733 (18)	Cu35—S23	2.240 (5)
Cu6—Cu26	2.757 (3)	Cu35—S7	2.282 (5)
Cu6—Cu35	2.761 (3)	Cu35—S3	2.315 (5)
Cu6—Cu38	2.795 (3)	Cu35—Cu44	2.700 (3)
Cu6—Cu47A	2.875 (12)	Cu35—Cu47A	2.835 (12)
Cu7—S10	2.267 (5)	Cu36A—S24	2.236 (5)
Cu7—S9iii	2.307 (5)	Cu36A—S4	2.383 (8)
Cu7—S13	2.307 (4)	Cu36A—S8	2.384 (6)
Cu7—Cu40	2.612 (3)	Cu36A—Cu45A	2.562 (9)
Cu7—Cu28	2.690 (3)	Cu36A—S7	2.722 (7)
Cu7—Cu24iv	2.717 (3)	Cu36A—Cu37	2.989 (5)
Cu7—Cu31iii	2.793 (3)	Cu36B—S24	2.177 (17)
Cu7—Cu48	2.892 (3)	Cu36B—S8	2.21 (2)
Cu7—Cu41	2.907 (3)	Cu36B—S7	2.36 (2)
Cu8—S10	2.214 (5)	Cu36B—Cu39	2.93 (3)
Cu8—S11	2.273 (5)	Cu36B—Cu45B	2.99 (4)
Cu8—S14	2.342 (5)	Cu37—S8	2.267 (5)
Cu8—Cu42	2.566 (4)	Cu37—S21v	2.277 (5)
Cu8—Cu41	2.802 (3)	Cu37—S1	2.298 (5)
Cu8—Cu29A	2.815 (7)	Cu38—S27	2.285 (4)
Cu8—Cu23iv	2.838 (3)	Cu38—S7	2.285 (4)
Cu8—Cu27iv	2.892 (3)	Cu38—S12	2.296 (5)
Cu9—S11	2.297 (5)	Cu38—Cu50	2.765 (3)
Cu9—S15	2.299 (5)	Cu38—Cu39	2.771 (3)
Cu9—S12	2.327 (5)	Cu39—S8	2.268 (5)
Cu9—Cu22iv	2.715 (3)	Cu39—S28	2.274 (5)
Cu9—Cu26iv	2.774 (3)	Cu39—S12	2.328 (5)
Cu9—Cu42	2.778 (4)	Cu40—S13	2.295 (5)
Cu9—Cu25iv	2.781 (3)	Cu40—S29iii	2.317 (4)
Cu9—Cu43	2.850 (3)	Cu40—S16iii	2.352 (5)
Cu9—Cu51A	2.881 (7)	Cu41—S30	2.266 (5)
Cu9—Cu38	2.902 (3)	Cu41—S13	2.267 (5)
Cu10—S20vi	2.284 (5)	Cu41—S14	2.332 (5)
Cu10—S17vii	2.294 (5)	Cu42—S31	2.233 (5)
Cu10—S29	2.326 (5)	Cu42—S14	2.295 (5)
Cu10—Cu40v	2.687 (3)	Cu42—Cu51B	2.405 (13)
Cu10—Cu32vii	2.704 (3)	Cu42—S11	2.661 (5)
Cu10—Cu56viii	2.754 (3)	Cu42—Cu51A	2.759 (9)
Cu10—Cu34vi	2.760 (3)	Cu43—S32	2.246 (4)
Cu10—Cu61	2.895 (4)	Cu43—S12	2.274 (5)
Cu11—S17vi	2.233 (5)	Cu43—S16	2.281 (5)
Cu11—S30	2.273 (5)	Cu43—Cu51A	2.707 (9)
Cu11—S18vi	2.337 (5)	Cu44—S3	2.285 (4)
Cu11—Cu59	2.760 (3)	Cu44—S18	2.342 (5)
Cu11—Cu41	2.778 (3)	Cu44—S19	2.344 (5)
Cu11—Cu52vi	2.790 (3)	Cu44—Cu53	2.701 (3)
Cu11—Cu33vi	2.843 (3)	Cu44—Cu51Bi	2.971 (11)
Cu11—Cu62Bvi	2.936 (19)	Cu45A—S4	2.279 (6)
Cu11—Cu17ix	3.033 (3)	Cu45A—S19	2.312 (6)
Cu12—S32	2.185 (8)	Cu45A—S20	2.419 (10)
Cu12—Cu45Avi	2.210 (8)	Cu45B—S4	2.08 (2)
Cu12—S19vi	2.217 (7)	Cu45B—S19	2.17 (3)
Cu12—S20vi	2.229 (8)	Cu46—S5	2.236 (5)
Cu12—Cu61	2.235 (7)	Cu46—S22	2.279 (5)
Cu12—Cu51A	2.352 (10)	Cu46—S25	2.423 (5)
Cu12—Cu60B	2.591 (14)	Cu46—Cu54A	2.592 (4)
Cu12—Cu45Bvi	2.64 (4)	Cu46—Cu49	2.850 (4)
Cu12—Cu54Bviii	2.653 (15)	Cu46—Cu62A	2.901 (5)
Cu12—Cu51B	2.709 (14)	Cu46—Cu54B	2.910 (13)
Cu12—Cu60A	2.742 (8)	Cu46—Cu47B	2.926 (14)
Cu13—S17	2.231 (5)	Cu47A—S6	2.228 (11)
Cu13—S21	2.245 (5)	Cu47A—S26	2.360 (13)
Cu13—Cu62B	2.363 (13)	Cu47A—S23	2.399 (13)
Cu13—S22	2.470 (5)	Cu47A—Cu55	2.564 (11)
Cu13—Cu54A	2.714 (5)	Cu47A—S22	2.792 (13)
Cu13—Cu62A	2.722 (4)	Cu47A—Cu50	3.046 (13)
Cu13—Cu54B	2.728 (15)	Cu47B—S6	2.215 (15)
Cu13—Cu52	2.829 (4)	Cu47B—S26	2.348 (17)
Cu13—Cu46	2.958 (4)	Cu47B—S22	2.373 (16)
Cu14—S24	2.264 (5)	Cu47B—Cu55	2.621 (14)
Cu14—S19	2.319 (5)	Cu47B—Cu49	2.943 (16)
Cu14—S23	2.337 (5)	Cu48—S9iii	2.257 (4)
Cu14—Cu45B	2.54 (3)	Cu48—S25	2.447 (5)
Cu14—Cu54Bx	2.682 (15)	Cu48—S29iii	2.531 (5)
Cu14—Cu53	2.760 (3)	Cu48—S28iii	2.626 (5)
Cu14—Cu35	2.806 (3)	Cu49—S26	2.240 (5)
Cu14—Cu56	2.811 (3)	Cu49—S10	2.290 (5)
Cu14—Cu45A	2.852 (6)	Cu49—S25	2.344 (5)
Cu14—Cu44	2.876 (3)	Cu50—S11	2.280 (5)
Cu14—Cu54Ax	2.973 (5)	Cu50—S26	2.301 (5)
Cu15—S24	2.282 (5)	Cu50—S27	2.310 (5)
Cu15—S20	2.301 (5)	Cu50—Cu57	2.658 (3)
Cu15—S21v	2.310 (5)	Cu51A—S15	2.208 (7)
Cu15—Cu53x	2.702 (3)	Cu51A—S32	2.494 (9)
Cu15—Cu37	2.740 (3)	Cu51A—S19vi	2.539 (9)
Cu15—Cu55x	2.788 (4)	Cu51A—S31	2.593 (9)
Cu15—Cu52x	2.790 (3)	Cu51A—Cu60A	2.616 (8)
Cu15—Cu36A	2.794 (5)	Cu51B—S19vi	2.249 (12)
Cu15—Cu45A	2.846 (6)	Cu51B—S15	2.282 (10)
Cu16—S21v	2.225 (5)	Cu51B—S31	2.325 (12)
Cu16—S28	2.258 (5)	Cu51B—Cu60B	2.531 (14)
Cu16—S25v	2.327 (5)	Cu52—S18	2.290 (5)
Cu16—Cu48v	2.622 (4)	Cu52—S24xiii	2.292 (5)
Cu16—Cu54Av	2.752 (5)	Cu52—S22	2.303 (5)
Cu16—Cu59viii	2.920 (3)	Cu52—Cu62B	2.489 (13)
Cu16—Cu46v	2.973 (4)	Cu52—Cu53	2.748 (3)
Cu17—S24	2.243 (5)	Cu52—Cu62A	2.761 (4)
Cu17—S28	2.277 (5)	Cu53—S21x	2.267 (5)
Cu17—S27	2.297 (5)	Cu53—S23	2.286 (5)
Cu17—Cu58	2.768 (3)	Cu53—S18	2.344 (5)
Cu17—Cu39	2.785 (3)	Cu53—Cu55	2.899 (4)
Cu17—Cu56	2.818 (3)	Cu54A—S19xiii	2.224 (5)
Cu17—Cu36B	2.82 (2)	Cu54A—S22	2.467 (7)
Cu17—Cu38	2.863 (3)	Cu54A—S25	2.604 (6)
Cu18—S30	2.232 (5)	Cu54A—S21	2.771 (6)
Cu18—S29iii	2.303 (5)	Cu54A—Cu60Aix	2.833 (8)
Cu18—S25	2.384 (5)	Cu54B—S22	1.942 (14)
Cu18—Cu48	2.624 (3)	Cu54B—S19xiii	2.206 (13)
Cu18—Cu57ix	2.798 (3)	Cu54B—Cu60Bix	2.72 (2)
Cu18—Cu58ix	2.799 (3)	Cu55—S20xiii	2.241 (5)
Cu18—Cu60Aix	2.840 (6)	Cu55—S23	2.276 (5)
Cu18—Cu49	2.879 (3)	Cu55—S22	2.452 (6)
Cu19—S30	2.270 (5)	Cu55—Cu61ix	2.645 (4)
Cu19—S26	2.291 (5)	Cu55—S26	2.764 (5)
Cu19—S31	2.325 (5)	Cu56—S23	2.260 (5)
Cu19—Cu50	2.779 (3)	Cu56—S17x	2.268 (4)
Cu19—Cu57	2.798 (3)	Cu56—S27	2.282 (5)
Cu19—Cu42	2.805 (4)	Cu57—S29ix	2.274 (4)
Cu19—Cu59	2.903 (3)	Cu57—S31	2.292 (5)
Cu19—Cu49	2.933 (3)	Cu57—S27	2.327 (5)
Cu20—S28	2.250 (5)	Cu57—Cu58	2.754 (3)
Cu20—S29	2.258 (5)	Cu57—Cu60A	2.892 (7)
Cu20—S32	2.288 (5)	Cu58—S27	2.282 (5)
Cu20—Cu48v	2.722 (3)	Cu58—S30viii	2.289 (5)
Cu20—Cu61	2.735 (4)	Cu58—S32	2.297 (5)
Cu20—Cu58	2.818 (3)	Cu58—Cu60A	2.906 (8)
Cu20—Cu43	2.896 (3)	Cu59—S28ix	2.258 (5)
Cu21—S16iv	2.275 (4)	Cu59—S31	2.266 (5)
Cu21—S13i	2.327 (4)	Cu59—S18vi	2.277 (5)
Cu21—S2	2.341 (5)	Cu60A—S25viii	2.240 (6)
Cu21—Cu31iv	2.631 (3)	Cu60A—S32	2.272 (7)
Cu21—Cu32	2.724 (3)	Cu60A—S31	2.380 (6)
Cu21—Cu24ii	2.746 (3)	Cu60B—S25viii	2.222 (11)
Cu22—S3	2.264 (5)	Cu60B—S31	2.396 (13)
Cu22—S15iv	2.269 (5)	Cu60B—S19vi	2.452 (15)
Cu22—S2	2.346 (4)	Cu60B—S32	2.724 (14)
Cu22—Cu33	2.699 (3)	Cu61—S26viii	2.230 (5)
Cu22—Cu26	2.714 (3)	Cu61—S32	2.268 (5)
Cu22—Cu25	2.742 (3)	Cu61—S20vi	2.411 (5)
Cu23—S14iv	2.265 (4)	Cu62A—S22	2.141 (6)
Cu23—S4	2.267 (5)	Cu62A—S2	2.204 (5)
Cu23—S3	2.284 (5)	Cu62B—S2	2.199 (13)
Cu24—S13iv	2.272 (4)	Cu62B—S22	2.592 (16)
Cu24—S4	2.316 (5)	Cu62B—S17	2.607 (19)
Cu24—S1	2.364 (5)
S15i—Cu1—S14i	118.62 (18)	S16iii—Cu40—Cu34xv	53.90 (11)
S15i—Cu1—S3	113.59 (18)	Cu7—Cu40—Cu34xv	154.35 (11)
S14i—Cu1—S3	127.51 (18)	S13—Cu40—Cu10iii	107.31 (13)
S15i—Cu1—Cu42i	72.74 (14)	S29iii—Cu40—Cu10iii	54.80 (12)
S14i—Cu1—Cu42i	53.96 (13)	S16iii—Cu40—Cu10iii	106.23 (13)
S3—Cu1—Cu42i	146.74 (14)	Cu7—Cu40—Cu10iii	136.81 (11)
S15i—Cu1—Cu22	151.82 (15)	Cu34xv—Cu40—Cu10iii	61.99 (8)
S14i—Cu1—Cu22	81.69 (13)	S13—Cu40—Cu31iii	82.46 (12)
S3—Cu1—Cu22	52.39 (12)	S29iii—Cu40—Cu31iii	134.11 (15)
Cu42i—Cu1—Cu22	133.56 (12)	S16iii—Cu40—Cu31iii	54.39 (11)
S15i—Cu1—Cu44	105.19 (14)	Cu7—Cu40—Cu31iii	63.29 (8)
S14i—Cu1—Cu44	106.48 (13)	Cu34xv—Cu40—Cu31iii	98.60 (9)
S3—Cu1—Cu44	52.77 (11)	Cu10iii—Cu40—Cu31iii	159.83 (11)
Cu42i—Cu1—Cu44	94.00 (10)	S13—Cu40—Cu32vi	55.75 (12)
Cu22—Cu1—Cu44	85.29 (9)	S29iii—Cu40—Cu32vi	108.73 (14)
S15i—Cu1—Cu33	149.78 (15)	S16iii—Cu40—Cu32vi	107.80 (14)
S14i—Cu1—Cu33	53.31 (12)	Cu7—Cu40—Cu32vi	110.34 (10)
S3—Cu1—Cu33	78.71 (13)	Cu34xv—Cu40—Cu32vi	59.88 (8)
Cu42i—Cu1—Cu33	82.41 (10)	Cu10iii—Cu40—Cu32vi	59.73 (8)
Cu22—Cu1—Cu33	57.65 (8)	Cu31iii—Cu40—Cu32vi	117.08 (10)
Cu44—Cu1—Cu33	58.95 (8)	S30—Cu41—S13	128.41 (18)
S15i—Cu1—Cu51Bi	51.0 (2)	S30—Cu41—S14	119.03 (18)
S14i—Cu1—Cu51Bi	102.5 (3)	S13—Cu41—S14	111.51 (17)
S3—Cu1—Cu51Bi	105.8 (3)	S30—Cu41—Cu11	52.38 (13)
Cu42i—Cu1—Cu51Bi	51.0 (3)	S13—Cu41—Cu11	105.11 (14)
Cu22—Cu1—Cu51Bi	148.9 (2)	S14—Cu41—Cu11	105.95 (14)
Cu44—Cu1—Cu51Bi	63.8 (2)	S30—Cu41—Cu8	99.18 (15)
Cu33—Cu1—Cu51Bi	99.8 (2)	S13—Cu41—Cu8	119.45 (14)
S15i—Cu1—Cu23	68.99 (13)	S14—Cu41—Cu8	53.34 (12)
S14i—Cu1—Cu23	161.14 (14)	Cu11—Cu41—Cu8	134.99 (11)
S3—Cu1—Cu23	50.63 (12)	S30—Cu41—Cu33vi	102.98 (14)
Cu42i—Cu1—Cu23	140.42 (12)	S13—Cu41—Cu33vi	99.36 (14)
Cu22—Cu1—Cu23	85.98 (9)	S14—Cu41—Cu33vi	52.35 (12)
Cu44—Cu1—Cu23	86.57 (9)	Cu11—Cu41—Cu33vi	59.97 (8)
Cu33—Cu1—Cu23	129.33 (11)	Cu8—Cu41—Cu33vi	104.11 (10)
Cu51Bi—Cu1—Cu23	95.4 (3)	S30—Cu41—Cu7	104.11 (15)
S15i—Cu2—S4	118.77 (18)	S13—Cu41—Cu7	51.16 (12)
S15i—Cu2—S16i	116.36 (18)	S14—Cu41—Cu7	123.07 (13)
S4—Cu2—S16i	124.78 (18)	Cu11—Cu41—Cu7	130.17 (10)
S15i—Cu2—Cu45A	106.66 (18)	Cu8—Cu41—Cu7	86.37 (9)
S4—Cu2—Cu45A	53.31 (16)	Cu33vi—Cu41—Cu7	148.89 (11)
S16i—Cu2—Cu45A	112.4 (2)	S31—Cu42—S14	135.4 (2)
S15i—Cu2—Cu21ii	106.64 (14)	S31—Cu42—Cu51B	60.1 (3)
S4—Cu2—Cu21ii	106.83 (14)	S14—Cu42—Cu51B	119.0 (3)
S16i—Cu2—Cu21ii	52.81 (11)	S31—Cu42—Cu8	130.62 (18)
Cu45A—Cu2—Cu21ii	146.60 (16)	S14—Cu42—Cu8	57.29 (13)
S15i—Cu2—Cu45B	97.9 (7)	Cu51B—Cu42—Cu8	168.9 (3)
S4—Cu2—Cu45B	47.3 (6)	S31—Cu42—S11	115.95 (18)
S16i—Cu2—Cu45B	126.8 (9)	S14—Cu42—S11	100.75 (16)
Cu21ii—Cu2—Cu45B	151.7 (6)	Cu51B—Cu42—S11	123.8 (3)
S15i—Cu2—Cu34	154.81 (15)	Cu8—Cu42—S11	51.52 (12)
S4—Cu2—Cu34	77.46 (13)	S31—Cu42—Cu1vi	119.78 (17)
S16i—Cu2—Cu34	52.59 (12)	S14—Cu42—Cu1vi	54.16 (13)
Cu45A—Cu2—Cu34	66.07 (18)	Cu8—Cu42—Cu1vi	104.08 (11)
Cu21ii—Cu2—Cu34	84.50 (9)	S11—Cu42—Cu1vi	117.42 (13)
Cu45B—Cu2—Cu34	78.9 (9)	S31—Cu42—Cu51A	61.52 (18)
S15i—Cu2—Cu23	71.21 (14)	S14—Cu42—Cu51A	129.1 (2)
S4—Cu2—Cu23	51.88 (12)	Cu8—Cu42—Cu51A	159.7 (2)
S16i—Cu2—Cu23	156.06 (14)	S11—Cu42—Cu51A	110.0 (2)
Cu45A—Cu2—Cu23	84.7 (2)	Cu1vi—Cu42—Cu51A	75.67 (17)
Cu21ii—Cu2—Cu23	103.66 (9)	S31—Cu42—Cu9	103.80 (16)
Cu45B—Cu2—Cu23	70.9 (9)	S14—Cu42—Cu9	119.50 (14)
Cu34—Cu2—Cu23	129.09 (11)	Cu51B—Cu42—Cu9	75.4 (3)
S15i—Cu2—Cu24	148.85 (15)	Cu8—Cu42—Cu9	97.08 (11)
S4—Cu2—Cu24	52.09 (12)	S11—Cu42—Cu9	49.90 (12)
S16i—Cu2—Cu24	78.67 (13)	Cu1vi—Cu42—Cu9	90.34 (11)
Cu45A—Cu2—Cu24	90.27 (11)	Cu51A—Cu42—Cu9	62.69 (18)
Cu21ii—Cu2—Cu24	59.05 (8)	S31—Cu42—Cu19	53.52 (13)
Cu45B—Cu2—Cu24	92.6 (6)	S14—Cu42—Cu19	105.79 (15)
Cu34—Cu2—Cu24	56.15 (7)	Cu51B—Cu42—Cu19	113.5 (3)
Cu23—Cu2—Cu24	84.94 (9)	Cu8—Cu42—Cu19	77.38 (11)
S15i—Cu2—Cu43i	72.77 (14)	S11—Cu42—Cu19	89.11 (13)
S4—Cu2—Cu43i	155.55 (14)	Cu1vi—Cu42—Cu19	147.79 (14)
S16i—Cu2—Cu43i	50.72 (12)	Cu51A—Cu42—Cu19	113.96 (16)
Cu45A—Cu2—Cu43i	103.81 (16)	Cu9—Cu42—Cu19	121.68 (12)
Cu21ii—Cu2—Cu43i	88.39 (9)	S32—Cu43—S12	121.51 (18)
Cu34—Cu2—Cu43i	85.31 (9)	S32—Cu43—S16	125.13 (17)
Cu23—Cu2—Cu43i	143.93 (11)	S12—Cu43—S16	109.47 (16)
Cu24—Cu2—Cu43i	129.20 (10)	S32—Cu43—Cu51A	59.60 (19)
S5—Cu3—S2	122.84 (18)	S12—Cu43—Cu51A	112.9 (2)
S5—Cu3—S1iii	111.37 (18)	S16—Cu43—Cu51A	118.2 (2)
S2—Cu3—S1iii	125.14 (17)	S32—Cu43—Cu9	104.52 (14)
S5—Cu3—Cu62A	94.27 (16)	S12—Cu43—Cu9	52.56 (12)
S2—Cu3—Cu62A	51.63 (12)	S16—Cu43—Cu9	122.71 (14)
S1iii—Cu3—Cu62A	135.32 (16)	Cu51A—Cu43—Cu9	62.38 (17)
S5—Cu3—Cu62B	112.4 (4)	S32—Cu43—Cu2vi	108.65 (15)
S2—Cu3—Cu62B	51.0 (3)	S12—Cu43—Cu2vi	121.13 (14)
S1iii—Cu3—Cu62B	115.7 (4)	S16—Cu43—Cu2vi	52.44 (12)
S5—Cu3—Cu32	149.95 (15)	Cu51A—Cu43—Cu2vi	67.46 (17)
S2—Cu3—Cu32	80.96 (13)	Cu9—Cu43—Cu2vi	88.32 (9)
S1iii—Cu3—Cu32	52.43 (12)	S32—Cu43—Cu20	50.95 (13)
Cu62A—Cu3—Cu32	87.19 (12)	S12—Cu43—Cu20	102.26 (14)
Cu62B—Cu3—Cu32	66.2 (4)	S16—Cu43—Cu20	101.80 (14)
S5—Cu3—Cu31iv	103.45 (14)	Cu51A—Cu43—Cu20	110.55 (16)
S2—Cu3—Cu31iv	104.08 (13)	Cu9—Cu43—Cu20	133.25 (10)
S1iii—Cu3—Cu31iv	52.19 (11)	Cu2vi—Cu43—Cu20	134.15 (10)
Cu62A—Cu3—Cu31iv	155.56 (12)	S3—Cu44—S18	131.19 (18)
Cu32—Cu3—Cu31iv	85.77 (9)	S3—Cu44—S19	119.41 (17)
S5—Cu3—Cu30iv	52.01 (12)	S18—Cu44—S19	107.88 (17)
S2—Cu3—Cu30iv	98.65 (13)	S3—Cu44—Cu35	54.59 (12)
S1iii—Cu3—Cu30iv	108.50 (13)	S18—Cu44—Cu35	124.32 (15)
Cu62A—Cu3—Cu30iv	116.09 (13)	S19—Cu44—Cu35	105.48 (14)
Cu32—Cu3—Cu30iv	150.23 (11)	S3—Cu44—Cu53	140.57 (16)
Cu31iv—Cu3—Cu30iv	65.30 (8)	S18—Cu44—Cu53	54.83 (12)
S5—Cu3—Cu21	149.03 (14)	S19—Cu44—Cu53	81.10 (13)
S2—Cu3—Cu21	52.99 (12)	Cu35—Cu44—Cu53	88.85 (10)
S1iii—Cu3—Cu21	76.59 (13)	S3—Cu44—Cu1	54.16 (12)
Cu62A—Cu3—Cu21	100.06 (11)	S18—Cu44—Cu1	105.34 (14)
Cu62B—Cu3—Cu21	88.3 (3)	S19—Cu44—Cu1	103.49 (14)
Cu32—Cu3—Cu21	58.81 (7)	Cu35—Cu44—Cu1	108.54 (10)
Cu31iv—Cu3—Cu21	56.55 (7)	Cu53—Cu44—Cu1	159.63 (12)
Cu30iv—Cu3—Cu21	97.04 (9)	S3—Cu44—Cu33	81.54 (13)
S5—Cu3—Cu25	76.43 (13)	S18—Cu44—Cu33	51.88 (12)
S2—Cu3—Cu25	50.10 (12)	S19—Cu44—Cu33	143.21 (15)
S1iii—Cu3—Cu25	151.73 (13)	Cu35—Cu44—Cu33	111.21 (11)
Cu62A—Cu3—Cu25	67.77 (10)	Cu53—Cu44—Cu33	101.79 (10)
Cu62B—Cu3—Cu25	83.3 (4)	Cu1—Cu44—Cu33	62.58 (8)
Cu32—Cu3—Cu25	130.80 (10)	S3—Cu44—Cu14	105.33 (14)
Cu31iv—Cu3—Cu25	99.91 (9)	S18—Cu44—Cu14	113.33 (13)
Cu30iv—Cu3—Cu25	53.64 (7)	S19—Cu44—Cu14	51.51 (12)
Cu21—Cu3—Cu25	83.79 (8)	Cu35—Cu44—Cu14	60.34 (8)
S5—Cu3—Cu37iii	69.95 (13)	Cu53—Cu44—Cu14	59.22 (8)
S2—Cu3—Cu37iii	160.70 (14)	Cu1—Cu44—Cu14	138.67 (11)
S1iii—Cu3—Cu37iii	48.10 (12)	Cu33—Cu44—Cu14	157.56 (11)
Cu62A—Cu3—Cu37iii	117.38 (10)	S3—Cu44—Cu51Bi	103.9 (2)
Cu32—Cu3—Cu37iii	82.73 (9)	S18—Cu44—Cu51Bi	98.3 (3)
Cu31iv—Cu3—Cu37iii	84.87 (8)	S19—Cu44—Cu51Bi	48.3 (2)
Cu30iv—Cu3—Cu37iii	100.63 (9)	Cu35—Cu44—Cu51Bi	136.8 (3)
Cu21—Cu3—Cu37iii	124.68 (10)	Cu53—Cu44—Cu51Bi	114.0 (2)
Cu25—Cu3—Cu37iii	146.20 (10)	Cu1—Cu44—Cu51Bi	60.2 (2)
S5v—Cu4—S8	124.53 (19)	Cu33—Cu44—Cu51Bi	99.8 (3)
S5v—Cu4—S9	115.93 (18)	Cu14—Cu44—Cu51Bi	99.2 (2)
S8—Cu4—S9	119.18 (18)	Cu12i—Cu45A—S4	135.6 (3)
S5v—Cu4—Cu28v	67.13 (14)	Cu12i—Cu45A—S19	58.7 (2)
S8—Cu4—Cu28v	148.38 (16)	S4—Cu45A—S19	128.1 (4)
S9—Cu4—Cu28v	55.22 (13)	Cu12i—Cu45A—S20	57.3 (3)
S5v—Cu4—Cu37	77.34 (14)	S4—Cu45A—S20	120.5 (3)
S8—Cu4—Cu37	53.14 (13)	S19—Cu45A—S20	107.4 (3)
S9—Cu4—Cu37	157.98 (15)	Cu12i—Cu45A—Cu36A	163.2 (3)
Cu28v—Cu4—Cu37	143.61 (12)	S4—Cu45A—Cu36A	58.63 (19)
S5v—Cu4—Cu28iv	104.98 (14)	S19—Cu45A—Cu36A	123.2 (3)
S8—Cu4—Cu28iv	50.55 (12)	S20—Cu45A—Cu36A	109.7 (2)
S9—Cu4—Cu28iv	109.42 (14)	Cu12i—Cu45A—Cu2	81.2 (2)
Cu28v—Cu4—Cu28iv	99.50 (10)	S4—Cu45A—Cu2	54.54 (14)
Cu37—Cu4—Cu28iv	81.84 (10)	S19—Cu45A—Cu2	102.7 (2)
S5v—Cu4—Cu39	156.55 (16)	S20—Cu45A—Cu2	97.9 (3)
S8—Cu4—Cu39	51.45 (13)	Cu36A—Cu45A—Cu2	112.83 (19)
S9—Cu4—Cu39	75.67 (13)	Cu12i—Cu45A—Cu15	102.0 (3)
Cu28v—Cu4—Cu39	130.23 (12)	S4—Cu45A—Cu15	105.71 (18)
Cu37—Cu4—Cu39	86.04 (10)	S19—Cu45A—Cu15	119.97 (19)
Cu28iv—Cu4—Cu39	88.65 (9)	S20—Cu45A—Cu15	51.04 (17)
S5v—Cu4—Cu30	149.50 (15)	Cu36A—Cu45A—Cu15	61.95 (13)
S8—Cu4—Cu30	73.16 (14)	Cu2—Cu45A—Cu15	132.0 (2)
S9—Cu4—Cu30	50.12 (12)	Cu12i—Cu45A—Cu14	102.5 (2)
Cu28v—Cu4—Cu30	85.50 (10)	S4—Cu45A—Cu14	113.2 (3)
Cu37—Cu4—Cu30	126.15 (11)	S19—Cu45A—Cu14	52.09 (16)
Cu28iv—Cu4—Cu30	65.16 (9)	S20—Cu45A—Cu14	117.3 (2)
Cu39—Cu4—Cu30	53.73 (7)	Cu36A—Cu45A—Cu14	72.9 (2)
S5v—Cu4—Cu48v	107.41 (14)	Cu2—Cu45A—Cu14	140.6 (3)
S8—Cu4—Cu48v	113.77 (14)	Cu15—Cu45A—Cu14	86.13 (12)
S9—Cu4—Cu48v	47.22 (11)	Cu12i—Cu45A—Cu34	81.1 (3)
Cu28v—Cu4—Cu48v	85.30 (9)	S4—Cu45A—Cu34	73.52 (16)
Cu37—Cu4—Cu48v	113.56 (10)	S19—Cu45A—Cu34	138.6 (3)
Cu28iv—Cu4—Cu48v	146.45 (11)	S20—Cu45A—Cu34	49.13 (17)
Cu39—Cu4—Cu48v	64.26 (8)	Cu36A—Cu45A—Cu34	98.13 (18)
Cu30—Cu4—Cu48v	82.32 (9)	Cu2—Cu45A—Cu34	58.00 (12)
S5—Cu5—S6	121.35 (18)	Cu15—Cu45A—Cu34	75.02 (19)
S5—Cu5—S10	116.61 (18)	Cu14—Cu45A—Cu34	161.1 (2)
S6—Cu5—S10	120.26 (18)	S4—Cu45B—S19	153.1 (16)
S5—Cu5—Cu29B	143.1 (6)	S4—Cu45B—Cu14	136.7 (19)
S6—Cu5—Cu29B	49.9 (4)	S19—Cu45B—Cu14	58.4 (7)
S10—Cu5—Cu29B	89.9 (6)	S4—Cu45B—Cu12i	123.0 (17)
S5—Cu5—Cu28	65.30 (13)	S19—Cu45B—Cu12i	53.9 (8)
S6—Cu5—Cu28	157.37 (14)	Cu14—Cu45B—Cu12i	100.0 (9)
S10—Cu5—Cu28	64.07 (13)	S4—Cu45B—Cu2	54.9 (6)
Cu29B—Cu5—Cu28	110.6 (4)	S19—Cu45B—Cu2	104.8 (12)
S5—Cu5—Cu29A	157.31 (19)	Cu14—Cu45B—Cu2	160.9 (13)
S6—Cu5—Cu29A	54.69 (14)	Cu12i—Cu45B—Cu2	73.0 (10)
S10—Cu5—Cu29A	76.82 (17)	S4—Cu45B—Cu36B	69.2 (9)
Cu28—Cu5—Cu29A	109.95 (12)	S19—Cu45B—Cu36B	132.1 (14)
S5—Cu5—Cu46	51.85 (12)	Cu14—Cu45B—Cu36B	73.8 (9)
S6—Cu5—Cu46	100.82 (14)	Cu12i—Cu45B—Cu36B	141.9 (15)
S10—Cu5—Cu46	103.37 (14)	Cu2—Cu45B—Cu36B	122.7 (9)
Cu29B—Cu5—Cu46	150.1 (4)	S5—Cu46—S22	136.4 (2)
Cu28—Cu5—Cu46	99.34 (10)	S5—Cu46—S25	113.66 (18)
Cu29A—Cu5—Cu46	146.70 (13)	S22—Cu46—S25	109.83 (18)
S5—Cu5—Cu49	104.86 (13)	S5—Cu46—Cu54A	147.8 (2)
S6—Cu5—Cu49	99.29 (13)	S22—Cu46—Cu54A	60.44 (18)
S10—Cu5—Cu49	51.38 (12)	S25—Cu46—Cu54A	62.47 (15)
Cu29B—Cu5—Cu49	111.8 (6)	S5—Cu46—Cu5	53.00 (13)
Cu28—Cu5—Cu49	99.38 (10)	S22—Cu46—Cu5	114.57 (17)
Cu29A—Cu5—Cu49	97.79 (15)	S25—Cu46—Cu5	102.25 (15)
Cu46—Cu5—Cu49	61.10 (9)	Cu54A—Cu46—Cu5	156.44 (16)
S5—Cu5—Cu25	78.08 (13)	S5—Cu46—Cu49	106.02 (16)
S6—Cu5—Cu25	51.49 (12)	S22—Cu46—Cu49	97.91 (16)
S10—Cu5—Cu25	160.32 (15)	S25—Cu46—Cu49	52.01 (13)
Cu29B—Cu5—Cu25	71.4 (6)	Cu54A—Cu46—Cu49	95.69 (14)
Cu28—Cu5—Cu25	116.11 (10)	Cu5—Cu46—Cu49	61.31 (9)
Cu29A—Cu5—Cu25	85.24 (15)	S5—Cu46—Cu62A	89.44 (15)
Cu46—Cu5—Cu25	96.06 (10)	S22—Cu46—Cu62A	46.96 (15)
Cu49—Cu5—Cu25	141.06 (11)	S25—Cu46—Cu62A	156.65 (15)
S5—Cu5—Cu27iv	121.34 (15)	Cu54A—Cu46—Cu62A	99.96 (15)
S6—Cu5—Cu27iv	106.43 (14)	Cu5—Cu46—Cu62A	88.75 (12)
S10—Cu5—Cu27iv	48.55 (12)	Cu49—Cu46—Cu62A	120.35 (14)
Cu28—Cu5—Cu27iv	58.11 (9)	S5—Cu46—Cu54B	159.8 (4)
Cu29A—Cu5—Cu27iv	52.39 (10)	S22—Cu46—Cu54B	41.8 (4)
Cu46—Cu5—Cu27iv	148.36 (12)	S25—Cu46—Cu54B	74.6 (3)
Cu49—Cu5—Cu27iv	98.34 (10)	Cu5—Cu46—Cu54B	145.7 (4)
Cu25—Cu5—Cu27iv	113.37 (9)	Cu49—Cu46—Cu54B	93.5 (3)
S5—Cu5—Cu47B	105.6 (3)	S5—Cu46—Cu47B	109.8 (3)
S6—Cu5—Cu47B	46.8 (3)	S22—Cu46—Cu47B	52.5 (3)
S10—Cu5—Cu47B	105.1 (4)	S25—Cu46—Cu47B	106.9 (4)
Cu29B—Cu5—Cu47B	90.1 (5)	Cu5—Cu46—Cu47B	64.3 (3)
Cu28—Cu5—Cu47B	155.8 (3)	Cu49—Cu46—Cu47B	61.3 (4)
Cu46—Cu5—Cu47B	60.7 (3)	Cu54B—Cu46—Cu47B	83.6 (5)
Cu49—Cu5—Cu47B	60.0 (3)	S5—Cu46—Cu13	105.74 (16)
Cu25—Cu5—Cu47B	81.6 (3)	S22—Cu46—Cu13	54.43 (14)
Cu27iv—Cu5—Cu47B	132.4 (3)	S25—Cu46—Cu13	117.13 (15)
S7—Cu6—S11	125.84 (18)	Cu54A—Cu46—Cu13	58.11 (12)
S7—Cu6—S6	125.68 (18)	Cu5—Cu46—Cu13	140.60 (13)
S11—Cu6—S6	108.42 (17)	Cu49—Cu46—Cu13	147.87 (11)
S7—Cu6—Cu29A	150.24 (17)	Cu62A—Cu46—Cu13	55.35 (11)
S11—Cu6—Cu29A	63.41 (19)	Cu54B—Cu46—Cu13	55.4 (3)
S6—Cu6—Cu29A	56.99 (16)	Cu47B—Cu46—Cu13	103.0 (4)
S7—Cu6—Cu29Biv	51.8 (4)	S5—Cu46—Cu16iii	93.36 (15)
S11—Cu6—Cu29Biv	100.4 (5)	S22—Cu46—Cu16iii	117.57 (16)
S6—Cu6—Cu29Biv	125.3 (6)	S25—Cu46—Cu16iii	49.82 (12)
Cu29A—Cu6—Cu29Biv	100.6 (4)	Cu54A—Cu46—Cu16iii	58.78 (13)
S7—Cu6—Cu29Aiv	52.73 (13)	Cu5—Cu46—Cu16iii	126.70 (12)
S11—Cu6—Cu29Aiv	112.43 (18)	Cu49—Cu46—Cu16iii	100.73 (11)
S6—Cu6—Cu29Aiv	111.25 (18)	Cu62A—Cu46—Cu16iii	136.23 (14)
Cu29A—Cu6—Cu29Aiv	97.65 (12)	Cu13—Cu46—Cu16iii	82.06 (10)
S7—Cu6—Cu50	104.96 (13)	S6—Cu47A—S26	121.5 (6)
S11—Cu6—Cu50	52.84 (12)	S6—Cu47A—S23	128.3 (5)
S6—Cu6—Cu50	105.47 (13)	S26—Cu47A—S23	102.1 (4)
Cu29A—Cu6—Cu50	101.80 (16)	S6—Cu47A—Cu55	164.0 (6)
Cu29Biv—Cu6—Cu50	128.9 (6)	S26—Cu47A—Cu55	68.1 (3)
Cu29Aiv—Cu6—Cu50	143.27 (17)	S23—Cu47A—Cu55	54.5 (3)
S7—Cu6—Cu29B	141.3 (5)	S6—Cu47A—S22	110.8 (5)
S11—Cu6—Cu29B	78.2 (5)	S26—Cu47A—S22	90.4 (4)
S6—Cu6—Cu29B	46.9 (4)	S23—Cu47A—S22	94.0 (4)
Cu29Biv—Cu6—Cu29B	98.3 (5)	Cu55—Cu47A—S22	54.3 (3)
Cu50—Cu6—Cu29B	113.6 (5)	S6—Cu47A—Cu35	78.8 (3)
S7—Cu6—Cu26	80.21 (13)	S26—Cu47A—Cu35	134.8 (5)
S11—Cu6—Cu26	145.43 (14)	S23—Cu47A—Cu35	49.8 (3)
S6—Cu6—Cu26	52.70 (12)	Cu55—Cu47A—Cu35	103.6 (4)
Cu29A—Cu6—Cu26	82.89 (17)	S22—Cu47A—Cu35	121.7 (5)
Cu29Biv—Cu6—Cu26	77.4 (6)	S6—Cu47A—Cu6	53.4 (3)
Cu29Aiv—Cu6—Cu26	62.35 (15)	S26—Cu47A—Cu6	99.8 (5)
Cu50—Cu6—Cu26	150.62 (12)	S23—Cu47A—Cu6	95.7 (4)
Cu29B—Cu6—Cu26	68.2 (5)	Cu55—Cu47A—Cu6	141.1 (5)
S7—Cu6—Cu35	52.77 (13)	S22—Cu47A—Cu6	164.1 (5)
S11—Cu6—Cu35	153.06 (14)	Cu35—Cu47A—Cu6	57.8 (2)
S6—Cu6—Cu35	78.19 (13)	S6—Cu47A—Cu50	99.5 (4)
Cu29A—Cu6—Cu35	133.80 (17)	S26—Cu47A—Cu50	48.4 (3)
Cu29Biv—Cu6—Cu35	96.1 (5)	S23—Cu47A—Cu50	89.0 (4)
Cu29Aiv—Cu6—Cu35	87.85 (12)	Cu55—Cu47A—Cu50	96.3 (4)
Cu50—Cu6—Cu35	100.29 (10)	S22—Cu47A—Cu50	138.1 (4)
Cu29B—Cu6—Cu35	120.4 (5)	Cu35—Cu47A—Cu50	91.4 (4)
Cu26—Cu6—Cu35	59.29 (8)	Cu6—Cu47A—Cu50	54.7 (2)
S7—Cu6—Cu38	52.31 (12)	S6—Cu47B—S26	122.6 (8)
S11—Cu6—Cu38	76.78 (13)	S6—Cu47B—S22	129.1 (7)
S6—Cu6—Cu38	158.28 (14)	S26—Cu47B—S22	102.0 (6)
Cu29A—Cu6—Cu38	137.90 (18)	S6—Cu47B—Cu55	157.7 (7)
Cu29Biv—Cu6—Cu38	72.5 (5)	S26—Cu47B—Cu55	67.3 (4)
Cu29Aiv—Cu6—Cu38	84.73 (14)	S22—Cu47B—Cu55	58.5 (4)
Cu50—Cu6—Cu38	60.08 (8)	S6—Cu47B—Cu46	97.5 (5)
Cu29B—Cu6—Cu38	151.1 (5)	S26—Cu47B—Cu46	97.8 (5)
Cu26—Cu6—Cu38	132.51 (11)	S22—Cu47B—Cu46	49.6 (3)
Cu35—Cu6—Cu38	88.20 (9)	Cu55—Cu47B—Cu46	100.7 (5)
S7—Cu6—Cu47A	109.3 (3)	S6—Cu47B—Cu49	98.6 (5)
S11—Cu6—Cu47A	103.5 (3)	S26—Cu47B—Cu49	48.5 (3)
S6—Cu6—Cu47A	49.1 (3)	S22—Cu47B—Cu49	93.3 (5)
Cu29A—Cu6—Cu47A	93.4 (3)	Cu55—Cu47B—Cu49	101.9 (5)
Cu29Aiv—Cu6—Cu47A	143.7 (3)	Cu46—Cu47B—Cu49	58.1 (3)
Cu50—Cu6—Cu47A	65.8 (3)	S6—Cu47B—Cu5	48.9 (3)
Cu26—Cu6—Cu47A	85.1 (3)	S26—Cu47B—Cu5	101.8 (6)
Cu35—Cu6—Cu47A	60.4 (3)	S22—Cu47B—Cu5	102.8 (5)
Cu38—Cu6—Cu47A	109.3 (2)	Cu55—Cu47B—Cu5	153.1 (6)
S10—Cu7—S9iii	112.87 (17)	Cu46—Cu47B—Cu5	55.0 (2)
S10—Cu7—S13	114.61 (18)	Cu49—Cu47B—Cu5	57.2 (3)
S9iii—Cu7—S13	131.38 (18)	S9iii—Cu48—S25	121.44 (17)
S10—Cu7—Cu40	154.48 (15)	S9iii—Cu48—S29iii	118.93 (17)
S9iii—Cu7—Cu40	84.69 (13)	S25—Cu48—S29iii	101.40 (16)
S13—Cu7—Cu40	55.21 (12)	S9iii—Cu48—Cu16iii	114.57 (15)
S10—Cu7—Cu28	65.19 (13)	S25—Cu48—Cu16iii	54.53 (13)
S9iii—Cu7—Cu28	54.42 (12)	S29iii—Cu48—Cu16iii	125.78 (13)
S13—Cu7—Cu28	145.77 (14)	S9iii—Cu48—Cu18	118.99 (15)
Cu40—Cu7—Cu28	137.76 (11)	S25—Cu48—Cu18	55.95 (13)
S10—Cu7—Cu24iv	103.31 (14)	S29iii—Cu48—Cu18	53.03 (12)
S9iii—Cu7—Cu24iv	106.09 (13)	Cu16iii—Cu48—Cu18	106.60 (11)
S13—Cu7—Cu24iv	52.99 (11)	S9iii—Cu48—S28iii	115.36 (17)
Cu40—Cu7—Cu24iv	88.36 (9)	S25—Cu48—S28iii	98.47 (16)
Cu28—Cu7—Cu24iv	92.97 (10)	S29iii—Cu48—S28iii	96.73 (15)
S10—Cu7—Cu31iii	145.21 (14)	Cu16iii—Cu48—S28iii	50.97 (12)
S9iii—Cu7—Cu31iii	54.12 (12)	Cu18—Cu48—S28iii	125.48 (13)
S13—Cu7—Cu31iii	80.41 (13)	S9iii—Cu48—Cu20iii	117.60 (15)
Cu40—Cu7—Cu31iii	60.06 (8)	S25—Cu48—Cu20iii	120.74 (13)
Cu28—Cu7—Cu31iii	84.69 (9)	S29iii—Cu48—Cu20iii	50.76 (12)
Cu24iv—Cu7—Cu31iii	59.32 (8)	Cu16iii—Cu48—Cu20iii	96.75 (10)
S10—Cu7—Cu48	106.11 (14)	Cu18—Cu48—Cu20iii	99.09 (10)
S9iii—Cu7—Cu48	49.92 (11)	S28iii—Cu48—Cu20iii	49.73 (12)
S13—Cu7—Cu48	122.26 (14)	S9iii—Cu48—Cu7	51.45 (12)
Cu40—Cu7—Cu48	70.28 (9)	S25—Cu48—Cu7	94.02 (13)
Cu28—Cu7—Cu48	87.80 (9)	S29iii—Cu48—Cu7	87.38 (13)
Cu24iv—Cu7—Cu48	147.85 (11)	Cu16iii—Cu48—Cu7	135.45 (12)
Cu31iii—Cu7—Cu48	88.82 (9)	Cu18—Cu48—Cu7	67.56 (9)
S10—Cu7—Cu41	71.47 (13)	S28iii—Cu48—Cu7	165.79 (14)
S9iii—Cu7—Cu41	165.26 (14)	Cu20iii—Cu48—Cu7	127.69 (12)
S13—Cu7—Cu41	49.95 (12)	S9iii—Cu48—Cu4iii	48.56 (12)
Cu40—Cu7—Cu41	87.11 (9)	S25—Cu48—Cu4iii	90.91 (13)
Cu28—Cu7—Cu41	135.12 (11)	S29iii—Cu48—Cu4iii	166.55 (14)
Cu24iv—Cu7—Cu41	85.86 (9)	Cu16iii—Cu48—Cu4iii	66.08 (9)
Cu31iii—Cu7—Cu41	130.35 (10)	Cu18—Cu48—Cu4iii	133.96 (11)
Cu48—Cu7—Cu41	115.61 (9)	S28iii—Cu48—Cu4iii	86.67 (12)
S10—Cu8—S11	126.73 (19)	Cu20iii—Cu48—Cu4iii	126.50 (11)
S10—Cu8—S14	121.34 (19)	Cu7—Cu48—Cu4iii	86.37 (8)
S11—Cu8—S14	111.90 (18)	S26—Cu49—S10	130.46 (19)
S10—Cu8—Cu42	147.53 (16)	S26—Cu49—S25	119.09 (18)
S11—Cu8—Cu42	66.39 (14)	S10—Cu49—S25	110.08 (17)
S14—Cu8—Cu42	55.52 (13)	S26—Cu49—Cu46	102.71 (16)
S10—Cu8—Cu41	74.32 (14)	S10—Cu49—Cu46	100.52 (14)
S11—Cu8—Cu41	147.73 (15)	S25—Cu49—Cu46	54.56 (13)
S14—Cu8—Cu41	53.00 (12)	S26—Cu49—Cu5	110.12 (15)
Cu42—Cu8—Cu41	83.40 (11)	S10—Cu49—Cu5	51.62 (13)
S10—Cu8—Cu29A	76.42 (16)	S25—Cu49—Cu5	101.19 (14)
S11—Cu8—Cu29A	59.46 (15)	Cu46—Cu49—Cu5	57.58 (8)
S14—Cu8—Cu29A	146.07 (15)	S26—Cu49—Cu18	123.19 (15)
Cu42—Cu8—Cu29A	125.71 (14)	S10—Cu49—Cu18	90.51 (14)
Cu41—Cu8—Cu29A	150.14 (14)	S25—Cu49—Cu18	53.12 (13)
S10—Cu8—Cu23iv	108.35 (15)	Cu46—Cu49—Cu18	106.08 (11)
S11—Cu8—Cu23iv	105.92 (14)	Cu5—Cu49—Cu18	126.68 (10)
S14—Cu8—Cu23iv	50.75 (11)	S26—Cu49—Cu19	50.42 (13)
Cu42—Cu8—Cu23iv	92.98 (11)	S10—Cu49—Cu19	105.83 (15)
Cu41—Cu8—Cu23iv	85.89 (9)	S25—Cu49—Cu19	123.87 (14)
Cu29A—Cu8—Cu23iv	97.77 (11)	Cu46—Cu49—Cu19	151.08 (11)
S10—Cu8—Cu27iv	50.57 (12)	Cu5—Cu49—Cu19	134.94 (10)
S11—Cu8—Cu27iv	109.88 (14)	Cu18—Cu49—Cu19	85.61 (9)
S14—Cu8—Cu27iv	113.38 (14)	S26—Cu49—Cu47B	51.7 (3)
Cu42—Cu8—Cu27iv	160.70 (13)	S10—Cu49—Cu47B	107.9 (3)
Cu41—Cu8—Cu27iv	102.37 (10)	S25—Cu49—Cu47B	108.5 (3)
Cu29A—Cu8—Cu27iv	52.82 (10)	Cu46—Cu49—Cu47B	60.6 (3)
Cu23iv—Cu8—Cu27iv	69.37 (9)	Cu5—Cu49—Cu47B	62.8 (3)
S11—Cu9—S15	123.74 (19)	Cu18—Cu49—Cu47B	158.5 (3)
S11—Cu9—S12	120.40 (18)	Cu19—Cu49—Cu47B	99.4 (3)
S15—Cu9—S12	115.39 (18)	S11—Cu50—S26	116.56 (18)
S11—Cu9—Cu22iv	102.46 (13)	S11—Cu50—S27	127.28 (18)
S15—Cu9—Cu22iv	53.03 (12)	S26—Cu50—S27	115.94 (18)
S12—Cu9—Cu22iv	106.80 (13)	S11—Cu50—Cu57	135.92 (17)
S11—Cu9—Cu26iv	52.66 (12)	S26—Cu50—Cu57	83.56 (13)
S15—Cu9—Cu26iv	108.17 (14)	S27—Cu50—Cu57	55.31 (12)
S12—Cu9—Cu26iv	103.62 (13)	S11—Cu50—Cu6	54.82 (13)
Cu22iv—Cu9—Cu26iv	59.26 (8)	S26—Cu50—Cu6	105.77 (15)
S11—Cu9—Cu42	62.40 (14)	S27—Cu50—Cu6	105.83 (14)
S15—Cu9—Cu42	70.98 (14)	Cu57—Cu50—Cu6	161.03 (12)
S12—Cu9—Cu42	154.11 (14)	S11—Cu50—Cu38	78.32 (13)
Cu22iv—Cu9—Cu42	96.87 (10)	S26—Cu50—Cu38	151.34 (17)
Cu26iv—Cu9—Cu42	97.36 (9)	S27—Cu50—Cu38	52.59 (12)
S11—Cu9—Cu25iv	106.96 (14)	Cu57—Cu50—Cu38	102.80 (10)
S15—Cu9—Cu25iv	100.44 (14)	Cu6—Cu50—Cu38	61.18 (8)
S12—Cu9—Cu25iv	52.72 (11)	S11—Cu50—Cu19	98.13 (15)
Cu22iv—Cu9—Cu25iv	59.85 (8)	S26—Cu50—Cu19	52.59 (13)
Cu26iv—Cu9—Cu25iv	60.26 (8)	S27—Cu50—Cu19	117.20 (14)
Cu42—Cu9—Cu25iv	153.13 (11)	Cu57—Cu50—Cu19	61.90 (8)
S11—Cu9—Cu43	155.01 (14)	Cu6—Cu50—Cu19	136.82 (11)
S15—Cu9—Cu43	72.82 (14)	Cu38—Cu50—Cu19	154.13 (12)
S12—Cu9—Cu43	50.90 (12)	S11—Cu50—Cu47A	99.9 (2)
Cu22iv—Cu9—Cu43	102.52 (9)	S26—Cu50—Cu47A	50.0 (2)
Cu26iv—Cu9—Cu43	145.87 (10)	S27—Cu50—Cu47A	109.7 (3)
Cu42—Cu9—Cu43	114.27 (10)	Cu57—Cu50—Cu47A	121.3 (2)
Cu25iv—Cu9—Cu43	85.76 (8)	Cu6—Cu50—Cu47A	59.4 (2)
S11—Cu9—Cu51A	117.6 (2)	Cu38—Cu50—Cu47A	105.4 (2)
S15—Cu9—Cu51A	48.91 (18)	Cu19—Cu50—Cu47A	100.4 (2)
S12—Cu9—Cu51A	105.5 (2)	S15—Cu51A—Cu12	117.7 (4)
Cu22iv—Cu9—Cu51A	101.92 (16)	S15—Cu51A—S32	128.0 (4)
Cu26iv—Cu9—Cu51A	149.1 (2)	Cu12—Cu51A—S32	53.5 (3)
Cu42—Cu9—Cu51A	58.33 (19)	S15—Cu51A—S19vi	110.5 (3)
Cu25iv—Cu9—Cu51A	134.84 (19)	Cu12—Cu51A—S19vi	53.8 (2)
Cu43—Cu9—Cu51A	56.38 (19)	S32—Cu51A—S19vi	100.5 (3)
S11—Cu9—Cu38	75.19 (13)	S15—Cu51A—S31	121.8 (4)
S15—Cu9—Cu38	156.41 (15)	Cu12—Cu51A—S31	119.0 (3)
S12—Cu9—Cu38	50.65 (12)	S32—Cu51A—S31	96.5 (3)
Cu22iv—Cu9—Cu38	142.97 (10)	S19vi—Cu51A—S31	92.5 (3)
Cu26iv—Cu9—Cu38	94.54 (9)	S15—Cu51A—Cu60A	175.3 (4)
Cu42—Cu9—Cu38	113.23 (10)	Cu12—Cu51A—Cu60A	66.8 (3)
Cu25iv—Cu9—Cu38	85.05 (9)	S32—Cu51A—Cu60A	52.7 (2)
Cu43—Cu9—Cu38	84.86 (9)	S19vi—Cu51A—Cu60A	73.1 (3)
Cu51A—Cu9—Cu38	111.91 (17)	S31—Cu51A—Cu60A	54.38 (19)
S20vi—Cu10—S17vii	126.68 (18)	S15—Cu51A—Cu43	77.1 (3)
S20vi—Cu10—S29	116.99 (18)	Cu12—Cu51A—Cu43	75.9 (3)
S17vii—Cu10—S29	116.15 (18)	S32—Cu51A—Cu43	51.0 (2)
S20vi—Cu10—Cu40v	105.08 (13)	S19vi—Cu51A—Cu43	127.1 (4)
S17vii—Cu10—Cu40v	101.65 (13)	S31—Cu51A—Cu43	129.1 (3)
S29—Cu10—Cu40v	54.50 (12)	Cu60A—Cu51A—Cu43	103.3 (3)
S20vi—Cu10—Cu32vii	103.44 (14)	S15—Cu51A—Cu42	72.6 (3)
S17vii—Cu10—Cu32vii	53.46 (12)	Cu12—Cu51A—Cu42	163.9 (4)
S29—Cu10—Cu32vii	109.76 (14)	S32—Cu51A—Cu42	131.7 (3)
Cu40v—Cu10—Cu32vii	61.16 (8)	S19vi—Cu51A—Cu42	112.1 (3)
S20vi—Cu10—Cu56viii	111.56 (14)	S31—Cu51A—Cu42	49.19 (19)
S17vii—Cu10—Cu56viii	52.44 (12)	Cu60A—Cu51A—Cu42	103.5 (3)
S29—Cu10—Cu56viii	109.09 (14)	Cu43—Cu51A—Cu42	119.7 (3)
Cu40v—Cu10—Cu56viii	143.15 (11)	S15—Cu51A—Cu9	51.67 (18)
Cu32vii—Cu10—Cu56viii	105.24 (10)	Cu12—Cu51A—Cu9	137.0 (4)
S20vi—Cu10—Cu34vi	53.38 (12)	S32—Cu51A—Cu9	97.4 (3)
S17vii—Cu10—Cu34vi	109.44 (13)	S19vi—Cu51A—Cu9	160.7 (3)
S29—Cu10—Cu34vi	103.53 (13)	S31—Cu51A—Cu9	92.5 (3)
Cu40v—Cu10—Cu34vi	58.75 (8)	Cu60A—Cu51A—Cu9	124.3 (3)
Cu32vii—Cu10—Cu34vi	59.29 (7)	Cu43—Cu51A—Cu9	61.24 (17)
Cu56viii—Cu10—Cu34vi	147.21 (11)	Cu42—Cu51A—Cu9	58.98 (17)
S20vi—Cu10—Cu61	53.93 (14)	S19vi—Cu51B—S15	119.0 (5)
S17vii—Cu10—Cu61	154.86 (14)	S19vi—Cu51B—S31	108.3 (4)
S29—Cu10—Cu61	71.78 (14)	S15—Cu51B—S31	131.3 (5)
Cu40v—Cu10—Cu61	101.88 (10)	S19vi—Cu51B—Cu42	141.6 (6)
Cu32vii—Cu10—Cu61	149.48 (11)	S15—Cu51B—Cu42	78.7 (3)
Cu56viii—Cu10—Cu61	102.64 (10)	S31—Cu51B—Cu42	56.3 (3)
Cu34vi—Cu10—Cu61	90.37 (10)	S19vi—Cu51B—Cu60B	61.4 (4)
S17vi—Cu11—S30	120.37 (19)	S15—Cu51B—Cu60B	158.1 (6)
S17vi—Cu11—S18vi	122.06 (19)	S31—Cu51B—Cu60B	58.9 (4)
S30—Cu11—S18vi	116.73 (18)	Cu42—Cu51B—Cu60B	115.2 (5)
S17vi—Cu11—Cu59	158.95 (15)	S19vi—Cu51B—Cu12	52.1 (3)
S30—Cu11—Cu59	72.47 (14)	S15—Cu51B—Cu12	102.5 (5)
S18vi—Cu11—Cu59	52.26 (13)	S31—Cu51B—Cu12	115.5 (4)
S17vi—Cu11—Cu41	101.87 (14)	Cu42—Cu51B—Cu12	163.5 (5)
S30—Cu11—Cu41	52.15 (12)	Cu60B—Cu51B—Cu12	59.1 (4)
S18vi—Cu11—Cu41	104.95 (13)	S19vi—Cu51B—Cu1vi	102.2 (4)
Cu59—Cu11—Cu41	99.14 (10)	S15—Cu51B—Cu1vi	51.1 (2)
S17vi—Cu11—Cu52vi	75.77 (14)	S31—Cu51B—Cu1vi	110.1 (5)
S30—Cu11—Cu52vi	159.21 (15)	Cu42—Cu51B—Cu1vi	60.7 (3)
S18vi—Cu11—Cu52vi	52.15 (12)	Cu12—Cu51B—Cu1vi	132.7 (5)
Cu59—Cu11—Cu52vi	88.40 (10)	S19vi—Cu51B—Cu44vi	51.1 (3)
Cu41—Cu11—Cu52vi	142.32 (11)	S15—Cu51B—Cu44vi	98.5 (4)
S17vi—Cu11—Cu33vi	104.24 (14)	S31—Cu51B—Cu44vi	102.5 (4)
S30—Cu11—Cu33vi	104.74 (14)	Cu42—Cu51B—Cu44vi	95.0 (4)
S18vi—Cu11—Cu33vi	50.66 (11)	Cu12—Cu51B—Cu44vi	101.1 (4)
Cu59—Cu11—Cu33vi	86.72 (9)	Cu1vi—Cu51B—Cu44vi	56.0 (2)
Cu41—Cu11—Cu33vi	62.25 (8)	S18—Cu52—S24xiii	120.90 (19)
Cu52vi—Cu11—Cu33vi	81.60 (9)	S18—Cu52—S22	122.88 (19)
S17vi—Cu11—Cu62Bvi	58.7 (3)	S24xiii—Cu52—S22	114.8 (2)
S30—Cu11—Cu62Bvi	146.6 (3)	S18—Cu52—Cu62B	78.1 (3)
S18vi—Cu11—Cu62Bvi	68.7 (3)	S24xiii—Cu52—Cu62B	142.1 (4)
Cu59—Cu11—Cu62Bvi	121.0 (3)	S22—Cu52—Cu62B	65.4 (4)
Cu41—Cu11—Cu62Bvi	94.5 (3)	S18—Cu52—Cu53	54.54 (13)
Cu52vi—Cu11—Cu62Bvi	51.5 (3)	S24xiii—Cu52—Cu53	103.72 (14)
Cu33vi—Cu11—Cu62Bvi	51.0 (3)	S22—Cu52—Cu53	101.66 (15)
S17vi—Cu11—Cu17ix	91.94 (13)	Cu62B—Cu52—Cu53	113.5 (4)
S30—Cu11—Cu17ix	93.99 (13)	S18—Cu52—Cu62A	82.72 (14)
S18vi—Cu11—Cu17ix	93.28 (12)	S24xiii—Cu52—Cu62A	152.50 (17)
Cu59—Cu11—Cu17ix	69.53 (8)	S22—Cu52—Cu62A	49.01 (15)
Cu41—Cu11—Cu17ix	145.91 (11)	Cu53—Cu52—Cu62A	101.74 (12)
Cu52vi—Cu11—Cu17ix	71.16 (8)	S18—Cu52—Cu15xiii	105.50 (14)
Cu33vi—Cu11—Cu17ix	143.79 (10)	S24xiii—Cu52—Cu15xiii	52.24 (12)
S32—Cu12—Cu45Avi	155.4 (3)	S22—Cu52—Cu15xiii	98.02 (15)
S32—Cu12—S19vi	123.0 (3)	Cu53—Cu52—Cu15xiii	58.39 (8)
Cu45Avi—Cu12—S19vi	62.9 (3)	Cu62A—Cu52—Cu15xiii	140.14 (14)
S32—Cu12—S20vi	118.0 (3)	S18—Cu52—Cu11i	53.67 (13)
Cu45Avi—Cu12—S20vi	66.0 (3)	S24xiii—Cu52—Cu11i	96.58 (14)
S19vi—Cu12—S20vi	118.2 (3)	S22—Cu52—Cu11i	131.61 (16)
S32—Cu12—Cu61	61.7 (2)	Cu53—Cu52—Cu11i	105.62 (11)
Cu45Avi—Cu12—Cu61	131.0 (4)	Cu62A—Cu52—Cu11i	86.38 (11)
S19vi—Cu12—Cu61	141.5 (3)	Cu15xiii—Cu52—Cu11i	130.31 (11)
S20vi—Cu12—Cu61	65.4 (2)	S18—Cu52—Cu13	126.84 (15)
S32—Cu12—Cu51A	66.6 (3)	S24xiii—Cu52—Cu13	94.51 (15)
Cu45Avi—Cu12—Cu51A	99.2 (3)	S22—Cu52—Cu13	56.43 (14)
S19vi—Cu12—Cu51A	67.4 (3)	Cu62B—Cu52—Cu13	52.3 (3)
S20vi—Cu12—Cu51A	153.9 (4)	Cu53—Cu52—Cu13	156.41 (12)
Cu61—Cu12—Cu51A	128.0 (3)	Cu62A—Cu52—Cu13	58.26 (10)
S32—Cu12—Cu60B	69.0 (4)	Cu15xiii—Cu52—Cu13	127.65 (11)
S19vi—Cu12—Cu60B	60.7 (4)	Cu11i—Cu52—Cu13	86.70 (10)
S20vi—Cu12—Cu60B	144.0 (4)	S21x—Cu53—S23	122.59 (19)
Cu61—Cu12—Cu60B	93.5 (4)	S21x—Cu53—S18	120.59 (19)
S32—Cu12—Cu45Bvi	150.9 (7)	S23—Cu53—S18	116.79 (17)
Cu45Avi—Cu12—Cu45Bvi	12.7 (7)	S21x—Cu53—Cu44	138.96 (16)
S19vi—Cu12—Cu45Bvi	52.0 (8)	S23—Cu53—Cu44	78.56 (13)
S20vi—Cu12—Cu45Bvi	78.6 (8)	S18—Cu53—Cu44	54.78 (12)
Cu61—Cu12—Cu45Bvi	143.2 (8)	S21x—Cu53—Cu15xiii	54.56 (13)
Cu51A—Cu12—Cu45Bvi	88.1 (8)	S23—Cu53—Cu15xiii	107.06 (15)
S32—Cu12—Cu54Bviii	121.7 (4)	S18—Cu53—Cu15xiii	106.76 (14)
Cu45Avi—Cu12—Cu54Bviii	81.7 (4)	Cu44—Cu53—Cu15xiii	159.78 (12)
S19vi—Cu12—Cu54Bviii	53.0 (4)	S21x—Cu53—Cu52	107.74 (15)
S20vi—Cu12—Cu54Bviii	87.9 (4)	S23—Cu53—Cu52	104.57 (15)
Cu61—Cu12—Cu54Bviii	90.7 (4)	S18—Cu53—Cu52	52.74 (12)
Cu51A—Cu12—Cu54Bviii	112.1 (5)	Cu44—Cu53—Cu52	98.28 (10)
S32—Cu12—Cu51B	78.2 (3)	Cu15xiii—Cu53—Cu52	61.59 (8)
S19vi—Cu12—Cu51B	53.2 (3)	S21x—Cu53—Cu14	98.69 (14)
S20vi—Cu12—Cu51B	155.2 (4)	S23—Cu53—Cu14	54.19 (13)
Cu61—Cu12—Cu51B	137.5 (4)	S18—Cu53—Cu14	117.55 (14)
Cu60B—Cu12—Cu51B	57.0 (3)	Cu44—Cu53—Cu14	63.56 (8)
Cu45Bvi—Cu12—Cu51B	79.3 (8)	Cu15xiii—Cu53—Cu14	135.67 (11)
Cu54Bviii—Cu12—Cu51B	99.3 (5)	Cu52—Cu53—Cu14	152.91 (11)
S32—Cu12—Cu60A	53.5 (2)	S21x—Cu53—Cu55	102.09 (15)
Cu45Avi—Cu12—Cu60A	138.6 (4)	S23—Cu53—Cu55	50.39 (13)
S19vi—Cu12—Cu60A	75.7 (3)	S18—Cu53—Cu55	113.91 (15)
S20vi—Cu12—Cu60A	143.8 (3)	Cu44—Cu53—Cu55	117.02 (11)
Cu61—Cu12—Cu60A	83.2 (2)	Cu15xiii—Cu53—Cu55	59.57 (8)
Cu51A—Cu12—Cu60A	61.2 (2)	Cu52—Cu53—Cu55	68.25 (10)
S17—Cu13—S21	121.6 (2)	Cu14—Cu53—Cu55	100.91 (11)
S17—Cu13—Cu62B	69.1 (5)	S19xiii—Cu54A—S22	123.2 (3)
S21—Cu13—Cu62B	142.2 (4)	S19xiii—Cu54A—Cu46	172.1 (3)
S17—Cu13—S22	122.09 (19)	S22—Cu54A—Cu46	53.47 (15)
S21—Cu13—S22	116.29 (19)	S19xiii—Cu54A—S25	121.4 (2)
Cu62B—Cu13—S22	64.8 (4)	S22—Cu54A—S25	98.68 (19)
S17—Cu13—Cu54A	154.19 (18)	Cu46—Cu54A—S25	55.57 (13)
S21—Cu13—Cu54A	67.17 (17)	S19xiii—Cu54A—Cu13	117.5 (2)
S22—Cu13—Cu54A	56.59 (16)	S22—Cu54A—Cu13	56.70 (15)
S17—Cu13—Cu62A	89.77 (16)	Cu46—Cu54A—Cu13	67.70 (12)
S21—Cu13—Cu62A	130.95 (18)	S25—Cu54A—Cu13	119.68 (16)
S22—Cu13—Cu62A	48.42 (14)	S19xiii—Cu54A—Cu16iii	117.1 (2)
Cu54A—Cu13—Cu62A	101.56 (15)	S22—Cu54A—Cu16iii	119.34 (17)
S17—Cu13—Cu54B	138.4 (4)	Cu46—Cu54A—Cu16iii	67.54 (12)
S21—Cu13—Cu54B	87.2 (4)	S25—Cu54A—Cu16iii	51.41 (14)
Cu62B—Cu13—Cu54B	107.7 (5)	Cu13—Cu54A—Cu16iii	90.84 (15)
S22—Cu13—Cu54B	43.5 (3)	S19xiii—Cu54A—S21	113.5 (2)
S17—Cu13—Cu52	74.98 (14)	S22—Cu54A—S21	99.63 (19)
S21—Cu13—Cu52	156.28 (17)	Cu46—Cu54A—S21	74.38 (15)
Cu62B—Cu13—Cu52	56.4 (3)	S25—Cu54A—S21	95.07 (19)
S22—Cu13—Cu52	50.96 (13)	Cu13—Cu54A—S21	48.29 (13)
Cu54A—Cu13—Cu52	90.73 (14)	Cu16iii—Cu54A—S21	47.51 (14)
Cu62A—Cu13—Cu52	59.61 (10)	S19xiii—Cu54A—Cu60Aix	73.67 (18)
Cu54B—Cu13—Cu52	70.3 (4)	S22—Cu54A—Cu60Aix	122.7 (2)
S17—Cu13—Cu46	148.03 (16)	Cu46—Cu54A—Cu60Aix	101.81 (18)
S21—Cu13—Cu46	75.80 (15)	S25—Cu54A—Cu60Aix	48.43 (15)
Cu62B—Cu13—Cu46	81.2 (5)	Cu13—Cu54A—Cu60Aix	167.86 (19)
S22—Cu13—Cu46	48.63 (13)	Cu16iii—Cu54A—Cu60Aix	79.12 (16)
Cu54A—Cu13—Cu46	54.18 (10)	S21—Cu54A—Cu60Aix	124.4 (2)
Cu62A—Cu13—Cu46	61.26 (12)	S19xiii—Cu54A—Cu14xiii	50.51 (14)
Cu54B—Cu13—Cu46	61.4 (3)	S22—Cu54A—Cu14xiii	92.29 (19)
Cu52—Cu13—Cu46	98.73 (11)	Cu46—Cu54A—Cu14xiii	133.60 (17)
S24—Cu14—S19	119.67 (18)	S25—Cu54A—Cu14xiii	169.0 (2)
S24—Cu14—S23	116.30 (18)	Cu13—Cu54A—Cu14xiii	67.10 (12)
S19—Cu14—S23	123.10 (18)	Cu16iii—Cu54A—Cu14xiii	122.79 (18)
S24—Cu14—Cu45B	80.1 (7)	S21—Cu54A—Cu14xiii	83.48 (16)
S19—Cu14—Cu45B	52.7 (7)	Cu60Aix—Cu54A—Cu14xiii	124.18 (15)
S23—Cu14—Cu45B	132.9 (10)	S22—Cu54B—S19xiii	168.6 (9)
S24—Cu14—Cu54Bx	90.5 (4)	S22—Cu54B—Cu12ix	125.6 (8)
S19—Cu14—Cu54Bx	51.7 (3)	S19xiii—Cu54B—Cu12ix	53.3 (3)
S23—Cu14—Cu54Bx	137.5 (4)	S22—Cu54B—Cu14xiii	115.9 (7)
S24—Cu14—Cu53	152.39 (15)	S19xiii—Cu54B—Cu14xiii	55.6 (3)
S19—Cu14—Cu53	80.28 (14)	Cu12ix—Cu54B—Cu14xiii	96.1 (4)
S23—Cu14—Cu53	52.51 (13)	S22—Cu54B—Cu60Bix	131.9 (7)
Cu45B—Cu14—Cu53	126.9 (7)	S19xiii—Cu54B—Cu60Bix	58.6 (4)
Cu54Bx—Cu14—Cu53	88.2 (4)	Cu12ix—Cu54B—Cu60Bix	57.7 (4)
S24—Cu14—Cu35	106.15 (14)	Cu14xiii—Cu54B—Cu60Bix	110.7 (6)
S19—Cu14—Cu35	102.93 (14)	S22—Cu54B—Cu13	61.2 (4)
S23—Cu14—Cu35	50.65 (12)	S19xiii—Cu54B—Cu13	117.6 (7)
Cu45B—Cu14—Cu35	82.9 (10)	Cu12ix—Cu54B—Cu13	167.2 (6)
Cu54Bx—Cu14—Cu35	154.6 (3)	Cu14xiii—Cu54B—Cu13	71.2 (4)
Cu53—Cu14—Cu35	85.55 (9)	Cu60Bix—Cu54B—Cu13	128.1 (7)
S24—Cu14—Cu56	71.46 (13)	S22—Cu54B—Cu46	51.4 (3)
S19—Cu14—Cu56	162.78 (15)	S19xiii—Cu54B—Cu46	139.4 (8)
S23—Cu14—Cu56	51.06 (12)	Cu12ix—Cu54B—Cu46	129.6 (6)
Cu45B—Cu14—Cu56	144.4 (7)	Cu14xiii—Cu54B—Cu46	132.4 (6)
Cu54Bx—Cu14—Cu56	119.0 (3)	Cu60Bix—Cu54B—Cu46	88.2 (5)
Cu53—Cu14—Cu56	85.14 (10)	Cu13—Cu54B—Cu46	63.2 (3)
Cu35—Cu14—Cu56	84.91 (9)	S20xiii—Cu55—S23	133.3 (2)
S24—Cu14—Cu45A	73.51 (16)	S20xiii—Cu55—S22	114.4 (2)
S19—Cu14—Cu45A	51.88 (14)	S23—Cu55—S22	107.20 (19)
S23—Cu14—Cu45A	145.9 (2)	S20xiii—Cu55—Cu47A	158.8 (3)
Cu53—Cu14—Cu45A	131.25 (13)	S23—Cu55—Cu47A	59.1 (3)
Cu35—Cu14—Cu45A	95.56 (17)	S22—Cu55—Cu47A	67.6 (3)
Cu56—Cu14—Cu45A	143.59 (13)	S20xiii—Cu55—Cu47B	152.1 (4)
S24—Cu14—Cu44	149.67 (15)	S23—Cu55—Cu47B	71.3 (3)
S19—Cu14—Cu44	52.31 (12)	S22—Cu55—Cu47B	55.7 (4)
S23—Cu14—Cu44	74.20 (13)	S20xiii—Cu55—Cu61ix	58.42 (14)
Cu45B—Cu14—Cu44	73.4 (8)	S23—Cu55—Cu61ix	131.7 (2)
Cu54Bx—Cu14—Cu44	99.6 (3)	S22—Cu55—Cu61ix	102.19 (17)
Cu53—Cu14—Cu44	57.23 (8)	Cu47A—Cu55—Cu61ix	100.4 (3)
Cu35—Cu14—Cu44	56.71 (8)	S20xiii—Cu55—S26	106.56 (18)
Cu56—Cu14—Cu44	125.26 (11)	S23—Cu55—S26	94.01 (18)
Cu45A—Cu14—Cu44	82.98 (14)	S22—Cu55—S26	89.21 (17)
S24—Cu14—Cu54Ax	108.33 (16)	Cu47A—Cu55—S26	52.4 (3)
S19—Cu14—Cu54Ax	47.76 (13)	Cu47B—Cu55—S26	51.6 (4)
S23—Cu14—Cu54Ax	120.52 (17)	Cu61ix—Cu55—S26	48.63 (13)
Cu53—Cu14—Cu54Ax	69.58 (12)	S20xiii—Cu55—Cu15xiii	53.11 (13)
Cu35—Cu14—Cu54Ax	143.18 (13)	S23—Cu55—Cu15xiii	104.61 (16)
Cu56—Cu14—Cu54Ax	118.09 (11)	S22—Cu55—Cu15xiii	94.61 (17)
Cu45A—Cu14—Cu54Ax	82.27 (15)	Cu47A—Cu55—Cu15xiii	147.3 (3)
Cu44—Cu14—Cu54Ax	86.66 (11)	Cu61ix—Cu55—Cu15xiii	110.35 (12)
S24—Cu15—S20	120.64 (19)	S26—Cu55—Cu15xiii	158.88 (15)
S24—Cu15—S21v	120.39 (19)	S20xiii—Cu55—Cu53	104.77 (16)
S20—Cu15—S21v	118.97 (19)	S23—Cu55—Cu53	50.70 (13)
S24—Cu15—Cu53x	105.47 (14)	S22—Cu55—Cu53	94.01 (16)
S20—Cu15—Cu53x	109.50 (14)	Cu47A—Cu55—Cu53	95.9 (3)
S21v—Cu15—Cu53x	53.08 (12)	Cu47B—Cu55—Cu53	102.1 (4)
S24—Cu15—Cu37	106.01 (14)	Cu61ix—Cu55—Cu53	160.37 (14)
S20—Cu15—Cu37	108.57 (14)	S26—Cu55—Cu53	143.83 (14)
S21v—Cu15—Cu37	52.78 (12)	Cu15xiii—Cu55—Cu53	56.69 (9)
Cu53x—Cu15—Cu37	105.68 (10)	S23—Cu56—S17x	127.80 (18)
S24—Cu15—Cu55x	112.30 (15)	S23—Cu56—S27	113.04 (17)
S20—Cu15—Cu55x	51.18 (12)	S17x—Cu56—S27	117.59 (18)
S21v—Cu15—Cu55x	104.34 (15)	S23—Cu56—Cu10ix	103.98 (15)
Cu53x—Cu15—Cu55x	63.74 (9)	S17x—Cu56—Cu10ix	53.29 (12)
Cu37—Cu15—Cu55x	141.69 (12)	S27—Cu56—Cu10ix	103.14 (14)
S24—Cu15—Cu52x	52.58 (12)	S23—Cu56—Cu14	53.54 (13)
S20—Cu15—Cu52x	111.18 (14)	S17x—Cu56—Cu14	103.34 (15)
S21v—Cu15—Cu52x	105.12 (14)	S27—Cu56—Cu14	124.58 (14)
Cu53x—Cu15—Cu52x	60.02 (8)	Cu10ix—Cu56—Cu14	131.71 (11)
Cu37—Cu15—Cu52x	140.24 (11)	S23—Cu56—Cu17	124.31 (14)
Cu55x—Cu15—Cu52x	69.28 (10)	S17x—Cu56—Cu17	97.03 (14)
S24—Cu15—Cu36A	51.07 (16)	S27—Cu56—Cu17	52.25 (12)
S20—Cu15—Cu36A	105.7 (2)	Cu10ix—Cu56—Cu17	130.80 (11)
S21v—Cu15—Cu36A	111.22 (17)	Cu14—Cu56—Cu17	88.98 (10)
Cu53x—Cu15—Cu36A	144.58 (19)	S29ix—Cu57—S31	119.56 (18)
Cu37—Cu15—Cu36A	65.38 (10)	S29ix—Cu57—S27	122.84 (18)
Cu55x—Cu15—Cu36A	144.26 (15)	S31—Cu57—S27	117.39 (17)
Cu52x—Cu15—Cu36A	103.65 (14)	S29ix—Cu57—Cu50	136.20 (16)
S24—Cu15—Cu45A	73.40 (19)	S31—Cu57—Cu50	83.66 (13)
S20—Cu15—Cu45A	54.85 (19)	S27—Cu57—Cu50	54.73 (12)
S21v—Cu15—Cu45A	149.85 (15)	S29ix—Cu57—Cu58	106.99 (14)
Cu53x—Cu15—Cu45A	154.50 (13)	S31—Cu57—Cu58	104.71 (15)
Cu37—Cu15—Cu45A	98.92 (10)	S27—Cu57—Cu58	52.56 (12)
Cu55x—Cu15—Cu45A	92.64 (15)	Cu50—Cu57—Cu58	100.98 (10)
Cu52x—Cu15—Cu45A	104.14 (12)	S29ix—Cu57—Cu18viii	52.78 (13)
Cu36A—Cu15—Cu45A	54.0 (2)	S31—Cu57—Cu18viii	107.34 (14)
S21v—Cu16—S28	123.7 (2)	S27—Cu57—Cu18viii	105.38 (14)
S21v—Cu16—S25v	121.25 (19)	Cu50—Cu57—Cu18viii	160.03 (12)
S28—Cu16—S25v	113.94 (18)	Cu58—Cu57—Cu18viii	60.55 (8)
S21v—Cu16—Cu48v	159.87 (16)	S29ix—Cu57—Cu19	101.47 (14)
S28—Cu16—Cu48v	64.63 (14)	S31—Cu57—Cu19	53.22 (13)
S25v—Cu16—Cu48v	58.90 (13)	S27—Cu57—Cu19	115.88 (14)
S21v—Cu16—Cu54Av	66.70 (16)	Cu50—Cu57—Cu19	61.17 (8)
S28—Cu16—Cu54Av	142.30 (16)	Cu58—Cu57—Cu19	150.63 (12)
S25v—Cu16—Cu54Av	61.03 (15)	Cu18viii—Cu57—Cu19	138.74 (11)
Cu48v—Cu16—Cu54Av	119.61 (14)	S29ix—Cu57—Cu60A	102.51 (16)
S21v—Cu16—Cu59viii	105.71 (14)	S31—Cu57—Cu60A	53.13 (17)
S28—Cu16—Cu59viii	49.72 (12)	S27—Cu57—Cu60A	107.08 (18)
S25v—Cu16—Cu59viii	102.18 (14)	Cu50—Cu57—Cu60A	120.40 (13)
Cu48v—Cu16—Cu59viii	93.32 (10)	Cu58—Cu57—Cu60A	61.89 (15)
Cu54Av—Cu16—Cu59viii	93.24 (11)	Cu18viii—Cu57—Cu60A	59.86 (12)
S21v—Cu16—Cu46v	75.73 (14)	Cu19—Cu57—Cu60A	105.14 (16)
S28—Cu16—Cu46v	156.49 (16)	S27—Cu58—S30viii	126.18 (18)
S25v—Cu16—Cu46v	52.69 (13)	S27—Cu58—S32	116.77 (17)
Cu48v—Cu16—Cu46v	92.74 (10)	S30viii—Cu58—S32	116.33 (18)
Cu54Av—Cu16—Cu46v	53.68 (10)	S27—Cu58—Cu57	54.06 (12)
Cu59viii—Cu16—Cu46v	144.21 (11)	S30viii—Cu58—Cu57	106.79 (14)
S24—Cu17—S28	120.32 (19)	S32—Cu58—Cu57	101.52 (15)
S24—Cu17—S27	117.68 (18)	S27—Cu58—Cu17	53.04 (12)
S28—Cu17—S27	121.50 (18)	S30viii—Cu58—Cu17	101.04 (15)
S24—Cu17—Cu58	155.10 (15)	S32—Cu58—Cu17	124.80 (14)
S28—Cu17—Cu58	76.47 (14)	Cu57—Cu58—Cu17	104.84 (10)
S27—Cu17—Cu58	52.56 (12)	S27—Cu58—Cu18viii	106.62 (14)
S24—Cu17—Cu39	107.58 (14)	S30viii—Cu58—Cu18viii	50.84 (13)
S28—Cu17—Cu39	52.23 (12)	S32—Cu58—Cu18viii	104.68 (14)
S27—Cu17—Cu39	103.26 (14)	Cu57—Cu58—Cu18viii	60.51 (8)
Cu58—Cu17—Cu39	97.26 (10)	Cu17—Cu58—Cu18viii	130.51 (11)
S24—Cu17—Cu56	71.60 (14)	S27—Cu58—Cu20	124.44 (14)
S28—Cu17—Cu56	160.92 (15)	S30viii—Cu58—Cu20	95.21 (14)
S27—Cu17—Cu56	51.79 (12)	S32—Cu58—Cu20	51.94 (13)
Cu58—Cu17—Cu56	87.78 (9)	Cu57—Cu58—Cu20	151.86 (12)
Cu39—Cu17—Cu56	142.39 (11)	Cu17—Cu58—Cu20	87.44 (9)
S24—Cu17—Cu36B	49.3 (5)	Cu18viii—Cu58—Cu20	128.87 (10)
S28—Cu17—Cu36B	103.5 (5)	S27—Cu58—Cu60A	107.93 (16)
S27—Cu17—Cu36B	108.0 (5)	S30viii—Cu58—Cu60A	98.96 (16)
Cu58—Cu17—Cu36B	150.4 (5)	S32—Cu58—Cu60A	50.13 (15)
Cu39—Cu17—Cu36B	62.9 (5)	Cu57—Cu58—Cu60A	61.40 (12)
Cu56—Cu17—Cu36B	95.6 (4)	Cu17—Cu58—Cu60A	158.49 (13)
S24—Cu17—Cu38	106.41 (14)	Cu18viii—Cu58—Cu60A	59.69 (11)
S28—Cu17—Cu38	104.05 (14)	Cu20—Cu58—Cu60A	98.56 (13)
S27—Cu17—Cu38	51.14 (11)	S28ix—Cu59—S31	120.11 (19)
Cu58—Cu17—Cu38	84.81 (9)	S28ix—Cu59—S18vi	122.82 (19)
Cu39—Cu17—Cu38	58.76 (8)	S31—Cu59—S18vi	114.20 (18)
Cu56—Cu17—Cu38	84.86 (9)	S28ix—Cu59—Cu11	101.10 (15)
Cu36B—Cu17—Cu38	66.3 (5)	S31—Cu59—Cu11	127.31 (15)
S24—Cu17—Cu11viii	91.15 (13)	S18vi—Cu59—Cu11	54.25 (13)
S28—Cu17—Cu11viii	93.03 (13)	S28ix—Cu59—Cu19	103.81 (15)
S27—Cu17—Cu11viii	92.85 (12)	S31—Cu59—Cu19	51.68 (13)
Cu58—Cu17—Cu11viii	68.43 (8)	S18vi—Cu59—Cu19	123.64 (15)
Cu39—Cu17—Cu11viii	145.19 (11)	Cu11—Cu59—Cu19	89.69 (10)
Cu56—Cu17—Cu11viii	70.89 (8)	S28ix—Cu59—Cu16ix	49.72 (13)
Cu38—Cu17—Cu11viii	143.95 (10)	S31—Cu59—Cu16ix	103.59 (15)
S30—Cu18—S29iii	128.39 (18)	S18vi—Cu59—Cu16ix	102.20 (15)
S30—Cu18—S25	120.25 (18)	Cu11—Cu59—Cu16ix	128.64 (11)
S29iii—Cu18—S25	110.57 (18)	Cu19—Cu59—Cu16ix	133.17 (11)
S30—Cu18—Cu48	159.23 (15)	S25viii—Cu60A—S32	131.4 (3)
S29iii—Cu18—Cu48	61.43 (13)	S25viii—Cu60A—S31	117.6 (3)
S25—Cu18—Cu48	58.26 (13)	S32—Cu60A—S31	109.3 (2)
S30—Cu18—Cu57ix	107.01 (14)	S25viii—Cu60A—Cu51A	156.0 (4)
S29iii—Cu18—Cu57ix	51.86 (12)	S32—Cu60A—Cu51A	60.9 (2)
S25—Cu18—Cu57ix	101.12 (13)	S31—Cu60A—Cu51A	62.3 (2)
Cu48—Cu18—Cu57ix	93.18 (10)	S25viii—Cu60A—Cu12	115.8 (3)
S30—Cu18—Cu58ix	52.67 (12)	S32—Cu60A—Cu12	50.61 (19)
S29iii—Cu18—Cu58ix	104.74 (13)	S31—Cu60A—Cu12	112.5 (2)
S25—Cu18—Cu58ix	107.83 (14)	Cu51A—Cu60A—Cu12	52.0 (2)
Cu48—Cu18—Cu58ix	147.61 (11)	S25viii—Cu60A—Cu54Aviii	60.4 (2)
Cu57ix—Cu18—Cu58ix	58.95 (8)	S32—Cu60A—Cu54Aviii	114.5 (3)
S30—Cu18—Cu60Aix	102.32 (18)	S31—Cu60A—Cu54Aviii	110.0 (3)
S29iii—Cu18—Cu60Aix	103.34 (16)	Cu51A—Cu60A—Cu54Aviii	96.2 (3)
S25—Cu18—Cu60Aix	49.84 (16)	Cu12—Cu60A—Cu54Aviii	66.6 (2)
Cu48—Cu18—Cu60Aix	91.35 (15)	S25viii—Cu60A—Cu18viii	54.43 (16)
Cu57ix—Cu18—Cu60Aix	61.72 (12)	S32—Cu60A—Cu18viii	104.1 (3)
Cu58ix—Cu18—Cu60Aix	62.03 (14)	S31—Cu60A—Cu18viii	103.6 (2)
S30—Cu18—Cu49	74.64 (14)	Cu51A—Cu60A—Cu18viii	149.1 (3)
S29iii—Cu18—Cu49	153.74 (15)	Cu12—Cu60A—Cu18viii	141.0 (2)
S25—Cu18—Cu49	51.84 (12)	Cu54Aviii—Cu60A—Cu18viii	114.65 (17)
Cu48—Cu18—Cu49	92.69 (10)	S25viii—Cu60A—Cu57	102.0 (2)
Cu57ix—Cu18—Cu49	141.53 (11)	S32—Cu60A—Cu57	98.1 (3)
Cu58ix—Cu18—Cu49	99.86 (10)	S31—Cu60A—Cu57	50.41 (16)
Cu60Aix—Cu18—Cu49	80.16 (13)	Cu51A—Cu60A—Cu57	95.2 (2)
S30—Cu19—S26	116.86 (19)	Cu12—Cu60A—Cu57	141.3 (2)
S30—Cu19—S31	115.28 (18)	Cu54Aviii—Cu60A—Cu57	147.0 (2)
S26—Cu19—S31	127.84 (19)	Cu18viii—Cu60A—Cu57	58.42 (14)
S30—Cu19—Cu50	152.38 (15)	S25viii—Cu60A—Cu58	108.6 (3)
S26—Cu19—Cu50	52.93 (13)	S32—Cu60A—Cu58	50.89 (19)
S31—Cu19—Cu50	80.41 (14)	S31—Cu60A—Cu58	98.1 (2)
S30—Cu19—Cu57	150.67 (15)	Cu51A—Cu60A—Cu58	94.9 (2)
S26—Cu19—Cu57	80.62 (14)	Cu12—Cu60A—Cu58	101.1 (2)
S31—Cu19—Cu57	52.17 (13)	Cu54Aviii—Cu60A—Cu58	151.8 (2)
Cu50—Cu19—Cu57	56.93 (8)	Cu18viii—Cu60A—Cu58	58.29 (16)
S30—Cu19—Cu42	101.28 (15)	Cu57—Cu60A—Cu58	56.71 (15)
S26—Cu19—Cu42	117.94 (15)	S25viii—Cu60B—S31	117.7 (5)
S31—Cu19—Cu42	50.55 (12)	S25viii—Cu60B—S19vi	128.7 (6)
Cu50—Cu19—Cu42	70.28 (10)	S31—Cu60B—S19vi	99.8 (4)
Cu57—Cu19—Cu42	88.98 (10)	S25viii—Cu60B—Cu51B	173.3 (7)
S30—Cu19—Cu59	69.70 (14)	S31—Cu60B—Cu51B	56.2 (4)
S26—Cu19—Cu59	158.92 (15)	S19vi—Cu60B—Cu51B	53.6 (4)
S31—Cu19—Cu59	49.89 (13)	S25viii—Cu60B—Cu12	122.8 (5)
Cu50—Cu19—Cu59	130.27 (11)	S31—Cu60B—Cu12	117.4 (4)
Cu57—Cu19—Cu59	86.09 (9)	S19vi—Cu60B—Cu12	52.1 (3)
Cu42—Cu19—Cu59	77.83 (10)	Cu51B—Cu60B—Cu12	63.9 (4)
S30—Cu19—Cu49	73.02 (14)	S25viii—Cu60B—Cu54Bviii	81.7 (5)
S26—Cu19—Cu49	48.90 (13)	S31—Cu60B—Cu54Bviii	146.4 (7)
S31—Cu19—Cu49	158.54 (14)	S19vi—Cu60B—Cu54Bviii	50.2 (4)
Cu50—Cu19—Cu49	84.90 (9)	Cu12—Cu60B—Cu54Bviii	59.9 (5)
Cu57—Cu19—Cu49	129.39 (11)	S25viii—Cu60B—S32	112.1 (6)
Cu42—Cu19—Cu49	109.57 (10)	S31—Cu60B—S32	95.5 (4)
Cu59—Cu19—Cu49	142.72 (11)	S19vi—Cu60B—S32	96.6 (4)
S28—Cu20—S29	117.55 (19)	Cu51B—Cu60B—S32	72.5 (4)
S28—Cu20—S32	121.43 (19)	Cu12—Cu60B—S32	48.5 (3)
S29—Cu20—S32	120.02 (18)	Cu54Bviii—Cu60B—S32	102.1 (6)
S28—Cu20—Cu48v	62.94 (14)	S26viii—Cu61—Cu12	139.8 (3)
S29—Cu20—Cu48v	60.25 (13)	S26viii—Cu61—S32	128.8 (2)
S32—Cu20—Cu48v	146.74 (15)	Cu12—Cu61—S32	58.0 (2)
S28—Cu20—Cu61	157.88 (17)	S26viii—Cu61—S20vi	120.23 (19)
S29—Cu20—Cu61	75.95 (15)	Cu12—Cu61—S20vi	57.2 (2)
S32—Cu20—Cu61	52.77 (14)	S32—Cu61—S20vi	107.92 (19)
Cu48v—Cu20—Cu61	135.46 (13)	S26viii—Cu61—Cu55viii	68.48 (15)
S28—Cu20—Cu58	75.81 (14)	Cu12—Cu61—Cu55viii	91.6 (2)
S29—Cu20—Cu58	160.69 (16)	S32—Cu61—Cu55viii	148.6 (2)
S32—Cu20—Cu58	52.21 (13)	S20vi—Cu61—Cu55viii	52.38 (13)
Cu48v—Cu20—Cu58	137.26 (12)	S26viii—Cu61—Cu20	109.2 (2)
Cu61—Cu20—Cu58	87.28 (11)	Cu12—Cu61—Cu20	103.4 (2)
S28—Cu20—Cu43	106.60 (14)	S32—Cu61—Cu20	53.46 (14)
S29—Cu20—Cu43	103.94 (14)	S20vi—Cu61—Cu20	119.65 (15)
S32—Cu20—Cu43	49.67 (12)	Cu55viii—Cu61—Cu20	154.16 (18)
Cu48v—Cu20—Cu43	97.08 (9)	S26viii—Cu61—Cu10	102.81 (17)
Cu61—Cu20—Cu43	85.22 (11)	Cu12—Cu61—Cu10	100.8 (2)
Cu58—Cu20—Cu43	83.78 (9)	S32—Cu61—Cu10	121.80 (16)
S16iv—Cu21—S13i	132.65 (17)	S20vi—Cu61—Cu10	49.98 (13)
S16iv—Cu21—S2	118.96 (17)	Cu55viii—Cu61—Cu10	67.59 (11)
S13i—Cu21—S2	105.74 (16)	Cu20—Cu61—Cu10	88.73 (12)
S16iv—Cu21—Cu31iv	56.28 (12)	S22—Cu62A—S2	173.3 (3)
S13i—Cu21—Cu31iv	125.03 (14)	S22—Cu62A—Cu3	117.59 (18)
S2—Cu21—Cu31iv	107.50 (14)	S2—Cu62A—Cu3	56.57 (13)
S16iv—Cu21—Cu2ii	54.90 (12)	S22—Cu62A—Cu13	59.63 (15)
S13i—Cu21—Cu2ii	104.47 (13)	S2—Cu62A—Cu13	119.07 (19)
S2—Cu21—Cu2ii	100.34 (13)	Cu3—Cu62A—Cu13	76.41 (11)
Cu31iv—Cu21—Cu2ii	110.98 (9)	S22—Cu62A—Cu52	54.26 (15)
S16iv—Cu21—Cu32	141.99 (15)	S2—Cu62A—Cu52	131.8 (2)
S13i—Cu21—Cu32	55.78 (11)	Cu3—Cu62A—Cu52	135.45 (16)
S2—Cu21—Cu32	81.15 (12)	Cu13—Cu62A—Cu52	62.12 (10)
Cu31iv—Cu21—Cu32	87.95 (9)	S22—Cu62A—Cu33	133.45 (19)
Cu2ii—Cu21—Cu32	159.19 (11)	S2—Cu62A—Cu33	53.26 (13)
S16iv—Cu21—Cu24ii	81.87 (13)	Cu3—Cu62A—Cu33	104.34 (12)
S13i—Cu21—Cu24ii	52.42 (11)	Cu13—Cu62A—Cu33	116.79 (17)
S2—Cu21—Cu24ii	140.57 (14)	Cu52—Cu62A—Cu33	82.07 (12)
Cu31iv—Cu21—Cu24ii	111.81 (10)	S22—Cu62A—Cu46	51.06 (15)
Cu2ii—Cu21—Cu24ii	62.77 (8)	S2—Cu62A—Cu46	122.23 (17)
Cu32—Cu21—Cu24ii	102.94 (9)	Cu3—Cu62A—Cu46	71.03 (10)
S16iv—Cu21—Cu3	105.39 (13)	Cu13—Cu62A—Cu46	63.38 (10)
S13i—Cu21—Cu3	113.80 (13)	Cu52—Cu62A—Cu46	101.72 (11)
S2—Cu21—Cu3	53.14 (12)	Cu33—Cu62A—Cu46	175.31 (13)
Cu31iv—Cu21—Cu3	60.17 (8)	S2—Cu62B—Cu13	137.6 (6)
Cu2ii—Cu21—Cu3	137.70 (11)	S2—Cu62B—Cu52	150.9 (7)
Cu32—Cu21—Cu3	58.99 (8)	Cu13—Cu62B—Cu52	71.3 (3)
Cu24ii—Cu21—Cu3	158.77 (11)	S2—Cu62B—Cu33	59.3 (3)
S3—Cu22—S15iv	127.13 (18)	Cu13—Cu62B—Cu33	155.4 (9)
S3—Cu22—S2	121.72 (16)	Cu52—Cu62B—Cu33	95.3 (5)
S15iv—Cu22—S2	111.06 (17)	S2—Cu62B—S22	129.5 (9)
S3—Cu22—Cu33	83.28 (13)	Cu13—Cu62B—S22	59.6 (3)
S15iv—Cu22—Cu33	129.43 (15)	Cu52—Cu62B—S22	53.8 (3)
S2—Cu22—Cu33	54.60 (12)	Cu33—Cu62B—S22	129.1 (6)
S3—Cu22—Cu26	56.87 (13)	S2—Cu62B—S17	122.0 (7)
S15iv—Cu22—Cu26	111.13 (15)	Cu13—Cu62B—S17	53.1 (4)
S2—Cu22—Cu26	107.62 (14)	Cu52—Cu62B—S17	75.3 (4)
Cu33—Cu22—Cu26	119.44 (10)	Cu33—Cu62B—S17	104.2 (7)
S3—Cu22—Cu9iv	109.23 (14)	S22—Cu62B—S17	104.6 (5)
S15iv—Cu22—Cu9iv	54.04 (13)	S2—Cu62B—Cu3	56.0 (3)
S2—Cu22—Cu9iv	106.66 (14)	Cu13—Cu62B—Cu3	82.0 (4)
Cu33—Cu22—Cu9iv	161.22 (11)	Cu52—Cu62B—Cu3	150.7 (6)
Cu26—Cu22—Cu9iv	61.45 (8)	Cu33—Cu62B—Cu3	113.9 (4)
S3—Cu22—Cu1	54.49 (13)	S22—Cu62B—Cu3	102.2 (6)
S15iv—Cu22—Cu1	99.50 (15)	S17—Cu62B—Cu3	98.4 (5)
S2—Cu22—Cu1	117.27 (14)	S2—Cu62B—Cu11i	111.3 (6)
Cu33—Cu22—Cu1	63.49 (8)	Cu13—Cu62B—Cu11i	92.8 (6)
Cu26—Cu22—Cu1	110.13 (10)	Cu52—Cu62B—Cu11i	61.3 (4)
Cu9iv—Cu22—Cu1	135.14 (11)	Cu33—Cu62B—Cu11i	62.6 (4)
S3—Cu22—Cu25	110.28 (14)	S22—Cu62B—Cu11i	114.4 (5)
S15iv—Cu22—Cu25	102.36 (14)	S17—Cu62B—Cu11i	47.1 (3)
S2—Cu22—Cu25	53.95 (13)	Cu3—Cu62B—Cu11i	133.9 (6)
Cu33—Cu22—Cu25	101.72 (10)	S2—Cu62B—Cu32	78.0 (4)
Cu26—Cu22—Cu25	61.45 (8)	Cu13—Cu62B—Cu32	74.0 (4)
Cu9iv—Cu22—Cu25	61.25 (8)	Cu52—Cu62B—Cu32	123.0 (7)
Cu1—Cu22—Cu25	158.14 (11)	Cu33—Cu62B—Cu32	98.2 (5)
S14iv—Cu23—S4	124.53 (18)	S22—Cu62B—Cu32	132.0 (5)
S14iv—Cu23—S3	119.27 (17)	S17—Cu62B—Cu32	47.7 (3)
S4—Cu23—S3	112.70 (16)	Cu3—Cu62B—Cu32	57.3 (3)
S14iv—Cu23—Cu2	107.77 (14)	Cu11i—Cu62B—Cu32	77.2 (5)
S4—Cu23—Cu2	53.46 (13)	Cu31xi—S1—Cu32v	110.08 (19)
S3—Cu23—Cu2	122.23 (14)	Cu31xi—S1—Cu37	118.2 (2)
S14iv—Cu23—Cu8iv	53.22 (12)	Cu32v—S1—Cu37	114.01 (18)
S4—Cu23—Cu8iv	99.43 (14)	Cu31xi—S1—Cu34	129.0 (2)
S3—Cu23—Cu8iv	101.81 (14)	Cu32v—S1—Cu34	71.87 (14)
Cu2—Cu23—Cu8iv	133.87 (11)	Cu37—S1—Cu34	104.82 (17)
S14iv—Cu23—Cu1	100.67 (14)	Cu31xi—S1—Cu3v	72.52 (14)
S4—Cu23—Cu1	126.87 (14)	Cu32v—S1—Cu3v	72.21 (14)
S3—Cu23—Cu1	51.92 (13)	Cu37—S1—Cu3v	82.12 (16)
Cu2—Cu23—Cu1	89.69 (10)	Cu34—S1—Cu3v	143.0 (2)
Cu8iv—Cu23—Cu1	131.78 (11)	Cu31xi—S1—Cu24	72.16 (13)
S13iv—Cu24—S4	121.13 (17)	Cu32v—S1—Cu24	126.6 (2)
S13iv—Cu24—S1	132.55 (17)	Cu37—S1—Cu24	109.65 (19)
S4—Cu24—S1	105.23 (16)	Cu34—S1—Cu24	68.50 (13)
S13iv—Cu24—Cu34	138.01 (15)	Cu3v—S1—Cu24	144.15 (19)
S4—Cu24—Cu34	80.08 (13)	Cu62B—S2—Cu33	66.6 (4)
S1—Cu24—Cu34	55.21 (12)	Cu62A—S2—Cu33	77.59 (16)
S13iv—Cu24—Cu7iv	54.20 (12)	Cu62B—S2—Cu25	113.6 (5)
S4—Cu24—Cu7iv	107.17 (14)	Cu62A—S2—Cu25	88.5 (2)
S1—Cu24—Cu7iv	105.00 (13)	Cu33—S2—Cu25	129.3 (2)
Cu34—Cu24—Cu7iv	160.19 (11)	Cu62B—S2—Cu21	115.8 (5)
S13iv—Cu24—Cu31xi	82.47 (13)	Cu62A—S2—Cu21	135.4 (2)
S4—Cu24—Cu31xi	143.24 (15)	Cu33—S2—Cu21	111.61 (19)
S1—Cu24—Cu31xi	52.26 (11)	Cu25—S2—Cu21	112.19 (17)
Cu34—Cu24—Cu31xi	101.24 (9)	Cu62B—S2—Cu22	125.6 (4)
Cu7iv—Cu24—Cu31xi	61.72 (8)	Cu62A—S2—Cu22	114.1 (2)
S13iv—Cu24—Cu21ii	54.26 (12)	Cu33—S2—Cu22	70.43 (14)
S4—Cu24—Cu21ii	105.98 (14)	Cu25—S2—Cu22	71.74 (14)
S1—Cu24—Cu21ii	124.05 (14)	Cu21—S2—Cu22	109.91 (17)
Cu34—Cu24—Cu21ii	86.44 (9)	Cu62B—S2—Cu3	73.0 (4)
Cu7iv—Cu24—Cu21ii	108.42 (9)	Cu62A—S2—Cu3	71.80 (15)
Cu31xi—Cu24—Cu21ii	110.77 (10)	Cu33—S2—Cu3	137.20 (19)
S13iv—Cu24—Cu2	102.12 (13)	Cu25—S2—Cu3	79.48 (15)
S4—Cu24—Cu2	52.05 (12)	Cu21—S2—Cu3	73.87 (14)
S1—Cu24—Cu2	114.73 (13)	Cu22—S2—Cu3	150.2 (2)
Cu34—Cu24—Cu2	60.45 (8)	Cu22—S3—Cu23	114.86 (18)
Cu7iv—Cu24—Cu2	138.51 (10)	Cu22—S3—Cu44	109.39 (19)
Cu31xi—Cu24—Cu2	157.31 (11)	Cu23—S3—Cu44	115.35 (19)
Cu21ii—Cu24—Cu2	58.18 (8)	Cu22—S3—Cu35	124.6 (2)
S12iv—Cu25—S2	122.41 (17)	Cu23—S3—Cu35	113.01 (19)
S12iv—Cu25—S6	121.90 (18)	Cu44—S3—Cu35	71.87 (14)
S2—Cu25—S6	115.35 (16)	Cu22—S3—Cu1	73.12 (15)
S12iv—Cu25—Cu30iv	55.42 (12)	Cu23—S3—Cu1	77.46 (15)
S2—Cu25—Cu30iv	103.88 (14)	Cu44—S3—Cu1	73.07 (15)
S6—Cu25—Cu30iv	116.64 (15)	Cu35—S3—Cu1	144.5 (2)
S12iv—Cu25—Cu22	106.59 (14)	Cu22—S3—Cu26	71.06 (14)
S2—Cu25—Cu22	54.31 (12)	Cu23—S3—Cu26	105.73 (18)
S6—Cu25—Cu22	101.26 (14)	Cu44—S3—Cu26	132.4 (2)
Cu30iv—Cu25—Cu22	142.05 (11)	Cu35—S3—Cu26	70.65 (14)
S12iv—Cu25—Cu9iv	53.48 (12)	Cu1—S3—Cu26	141.63 (19)
S2—Cu25—Cu9iv	104.92 (13)	Cu45B—S4—Cu23	95.3 (11)
S6—Cu25—Cu9iv	107.08 (13)	Cu23—S4—Cu45A	108.8 (2)
Cu30iv—Cu25—Cu9iv	108.23 (10)	Cu45B—S4—Cu2	77.8 (10)
Cu22—Cu25—Cu9iv	58.89 (8)	Cu23—S4—Cu2	74.66 (16)
S12iv—Cu25—Cu26	103.82 (14)	Cu45A—S4—Cu2	72.15 (18)
S2—Cu25—Cu26	105.59 (14)	Cu45B—S4—Cu24	134.8 (13)
S6—Cu25—Cu26	52.44 (12)	Cu23—S4—Cu24	111.95 (18)
Cu30iv—Cu25—Cu26	150.23 (12)	Cu45A—S4—Cu24	117.9 (3)
Cu22—Cu25—Cu26	58.78 (8)	Cu2—S4—Cu24	75.85 (15)
Cu9iv—Cu25—Cu26	59.76 (8)	Cu23—S4—Cu36A	125.1 (2)
S12iv—Cu25—Cu5	100.60 (14)	Cu45A—S4—Cu36A	66.6 (2)
S2—Cu25—Cu5	121.04 (13)	Cu2—S4—Cu36A	138.2 (2)
S6—Cu25—Cu5	50.03 (12)	Cu24—S4—Cu36A	117.8 (2)
Cu30iv—Cu25—Cu5	67.54 (9)	Cu45B—S4—Cu27	120.5 (11)
Cu22—Cu25—Cu5	148.73 (10)	Cu23—S4—Cu27	87.74 (17)
Cu9iv—Cu25—Cu5	133.74 (10)	Cu45A—S4—Cu27	129.9 (2)
Cu26—Cu25—Cu5	100.12 (10)	Cu2—S4—Cu27	156.2 (2)
S12iv—Cu25—Cu3	106.21 (13)	Cu24—S4—Cu27	96.71 (17)
S2—Cu25—Cu3	50.42 (11)	Cu36A—S4—Cu27	65.39 (18)
S6—Cu25—Cu3	114.70 (13)	Cu46—S5—Cu4iii	103.85 (19)
Cu30iv—Cu25—Cu3	59.04 (8)	Cu46—S5—Cu30iv	148.9 (2)
Cu22—Cu25—Cu3	104.39 (9)	Cu4iii—S5—Cu30iv	107.14 (19)
Cu9iv—Cu25—Cu3	137.57 (10)	Cu46—S5—Cu5	75.15 (16)
Cu26—Cu25—Cu3	148.94 (10)	Cu4iii—S5—Cu5	122.3 (2)
Cu5—Cu25—Cu3	82.05 (8)	Cu30iv—S5—Cu5	85.86 (17)
S11iv—Cu26—S6	128.71 (18)	Cu46—S5—Cu3	91.47 (18)
S11iv—Cu26—S3	114.98 (17)	Cu4iii—S5—Cu3	120.9 (2)
S6—Cu26—S3	115.92 (17)	Cu30iv—S5—Cu3	75.20 (15)
S11iv—Cu26—Cu22	102.69 (14)	Cu5—S5—Cu3	116.9 (2)
S6—Cu26—Cu22	103.10 (14)	Cu46—S5—Cu28	114.32 (19)
S3—Cu26—Cu22	52.07 (12)	Cu4iii—S5—Cu28	63.04 (13)
S11iv—Cu26—Cu35	139.20 (15)	Cu30iv—S5—Cu28	78.13 (15)
S6—Cu26—Cu35	79.92 (13)	Cu5—S5—Cu28	65.56 (13)
S3—Cu26—Cu35	53.16 (11)	Cu3—S5—Cu28	152.86 (19)
Cu22—Cu26—Cu35	96.29 (10)	Cu29B—S6—Cu47B	136.1 (8)
S11iv—Cu26—Cu6	108.80 (15)	Cu29B—S6—Cu5	71.8 (5)
S6—Cu26—Cu6	54.87 (13)	Cu47B—S6—Cu5	84.3 (4)
S3—Cu26—Cu6	113.10 (13)	Cu47A—S6—Cu5	98.6 (4)
Cu22—Cu26—Cu6	148.46 (11)	Cu29B—S6—Cu26	89.7 (6)
Cu35—Cu26—Cu6	60.43 (8)	Cu47B—S6—Cu26	126.8 (4)
S11iv—Cu26—Cu9iv	52.90 (12)	Cu47A—S6—Cu26	114.5 (4)
S6—Cu26—Cu9iv	108.40 (14)	Cu5—S6—Cu26	145.5 (2)
S3—Cu26—Cu9iv	103.32 (13)	Cu29B—S6—Cu25	93.8 (7)
Cu22—Cu26—Cu9iv	59.29 (8)	Cu47B—S6—Cu25	117.3 (5)
Cu35—Cu26—Cu9iv	155.15 (12)	Cu47A—S6—Cu25	127.0 (4)
Cu6—Cu26—Cu9iv	143.58 (12)	Cu5—S6—Cu25	78.48 (15)
S11iv—Cu26—Cu25	106.92 (14)	Cu26—S6—Cu25	73.88 (14)
S6—Cu26—Cu25	53.68 (12)	Cu47A—S6—Cu29A	119.3 (4)
S3—Cu26—Cu25	104.69 (14)	Cu5—S6—Cu29A	72.40 (16)
Cu22—Cu26—Cu25	59.77 (8)	Cu26—S6—Cu29A	98.09 (19)
Cu35—Cu26—Cu25	113.84 (10)	Cu25—S6—Cu29A	110.2 (2)
Cu6—Cu26—Cu25	107.87 (10)	Cu29B—S6—Cu6	76.0 (6)
Cu9iv—Cu26—Cu25	59.98 (8)	Cu47B—S6—Cu6	91.5 (4)
S11iv—Cu26—Cu29Aiv	59.08 (15)	Cu47A—S6—Cu6	77.4 (4)
S6—Cu26—Cu29Aiv	109.14 (18)	Cu5—S6—Cu6	127.2 (2)
S3—Cu26—Cu29Aiv	108.20 (15)	Cu26—S6—Cu6	72.43 (15)
Cu22—Cu26—Cu29Aiv	147.56 (15)	Cu25—S6—Cu6	144.7 (2)
Cu35—Cu26—Cu29Aiv	86.05 (11)	Cu29A—S6—Cu6	65.15 (17)
Cu6—Cu26—Cu29Aiv	57.94 (13)	Cu29Biv—S7—Cu35	127.4 (6)
Cu9iv—Cu26—Cu29Aiv	111.81 (13)	Cu29Aiv—S7—Cu35	113.7 (2)
Cu25—Cu26—Cu29Aiv	147.10 (13)	Cu29Biv—S7—Cu6	70.4 (5)
S10iv—Cu27—S7	135.41 (18)	Cu29Aiv—S7—Cu6	73.36 (16)
S10iv—Cu27—S4	113.34 (18)	Cu35—S7—Cu6	74.43 (15)
S7—Cu27—S4	101.50 (16)	Cu29Biv—S7—Cu38	91.7 (7)
S10iv—Cu27—Cu29Aiv	81.60 (16)	Cu29Aiv—S7—Cu38	109.8 (2)
S7—Cu27—Cu29Aiv	53.93 (14)	Cu35—S7—Cu38	115.68 (18)
S4—Cu27—Cu29Aiv	133.8 (2)	Cu6—S7—Cu38	75.45 (15)
S10iv—Cu27—S8	112.16 (18)	Cu29Biv—S7—Cu36B	128.8 (7)
S7—Cu27—S8	91.42 (15)	Cu35—S7—Cu36B	99.5 (6)
S4—Cu27—S8	93.90 (16)	Cu6—S7—Cu36B	152.7 (6)
Cu29Aiv—Cu27—S8	121.7 (2)	Cu38—S7—Cu36B	83.9 (7)
S10iv—Cu27—Cu36A	158.4 (2)	Cu29Biv—S7—Cu27	72.3 (5)
S7—Cu27—Cu36A	65.63 (18)	Cu29Aiv—S7—Cu27	65.96 (15)
S4—Cu27—Cu36A	56.3 (2)	Cu35—S7—Cu27	118.08 (19)
Cu29Aiv—Cu27—Cu36A	119.56 (19)	Cu6—S7—Cu27	139.09 (19)
S8—Cu27—Cu36A	54.70 (15)	Cu38—S7—Cu27	122.0 (2)
S10iv—Cu27—Cu36B	161.9 (5)	Cu36B—S7—Cu27	67.5 (5)
S7—Cu27—Cu36B	55.4 (6)	Cu29Aiv—S7—Cu36A	126.5 (2)
S4—Cu27—Cu36B	71.4 (7)	Cu35—S7—Cu36A	92.47 (18)
S8—Cu27—Cu36B	49.8 (5)	Cu6—S7—Cu36A	159.9 (2)
S10iv—Cu27—Cu29Biv	87.4 (4)	Cu38—S7—Cu36A	97.5 (2)
S7—Cu27—Cu29Biv	48.8 (4)	Cu27—S7—Cu36A	60.59 (14)
S4—Cu27—Cu29Biv	143.0 (4)	Cu36B—S8—Cu37	91.2 (7)
Cu29Aiv—Cu27—Cu29Biv	15.2 (4)	Cu28iv—S8—Cu37	107.4 (2)
S8—Cu27—Cu29Biv	106.5 (5)	Cu36B—S8—Cu39	81.7 (8)
Cu36A—Cu27—Cu29Biv	112.0 (4)	Cu28iv—S8—Cu39	122.4 (2)
S10iv—Cu27—Cu28iv	63.40 (14)	Cu37—S8—Cu39	112.90 (19)
S7—Cu27—Cu28iv	128.21 (15)	Cu36B—S8—Cu4	145.7 (6)
S4—Cu27—Cu28iv	111.34 (15)	Cu28iv—S8—Cu4	77.33 (16)
Cu29Aiv—Cu27—Cu28iv	114.29 (15)	Cu37—S8—Cu4	73.37 (16)
S8—Cu27—Cu28iv	48.80 (12)	Cu39—S8—Cu4	76.82 (16)
Cu36A—Cu27—Cu28iv	100.95 (13)	Cu28iv—S8—Cu36A	128.9 (2)
S10iv—Cu27—Cu8iv	49.02 (13)	Cu37—S8—Cu36A	79.9 (2)
S7—Cu27—Cu8iv	103.63 (14)	Cu39—S8—Cu36A	97.8 (2)
S4—Cu27—Cu8iv	94.10 (14)	Cu4—S8—Cu36A	147.7 (2)
Cu29Aiv—Cu27—Cu8iv	62.04 (16)	Cu36B—S8—Cu27	66.7 (5)
S8—Cu27—Cu8iv	161.17 (15)	Cu28iv—S8—Cu27	70.39 (14)
Cu36A—Cu27—Cu8iv	142.32 (17)	Cu37—S8—Cu27	119.6 (2)
Cu28iv—Cu27—Cu8iv	112.37 (10)	Cu39—S8—Cu27	117.7 (2)
S10iv—Cu27—Cu5iv	49.47 (13)	Cu4—S8—Cu27	147.5 (2)
S7—Cu27—Cu5iv	97.46 (14)	Cu36A—S8—Cu27	63.02 (15)
S4—Cu27—Cu5iv	160.96 (15)	Cu48v—S9—Cu4	84.23 (16)
Cu29Aiv—Cu27—Cu5iv	58.61 (11)	Cu48v—S9—Cu7v	78.62 (15)
S8—Cu27—Cu5iv	87.28 (13)	Cu4—S9—Cu7v	124.1 (2)
Cu36A—Cu27—Cu5iv	135.8 (2)	Cu48v—S9—Cu28v	115.99 (19)
Cu28iv—Cu27—Cu5iv	56.27 (9)	Cu4—S9—Cu28v	69.73 (15)
Cu8iv—Cu27—Cu5iv	79.69 (9)	Cu7v—S9—Cu28v	71.26 (15)
S8iv—Cu28—S9iii	132.68 (19)	Cu48v—S9—Cu31	119.01 (19)
S8iv—Cu28—Cu4iii	131.44 (16)	Cu4—S9—Cu31	154.8 (2)
S9iii—Cu28—Cu4iii	55.05 (13)	Cu7v—S9—Cu31	73.50 (15)
S8iv—Cu28—Cu7	122.55 (17)	Cu28v—S9—Cu31	104.55 (17)
S9iii—Cu28—Cu7	54.32 (13)	Cu48v—S9—Cu30	120.86 (19)
Cu4iii—Cu28—Cu7	99.78 (10)	Cu4—S9—Cu30	81.60 (16)
S8iv—Cu28—S10	109.55 (17)	Cu7v—S9—Cu30	151.0 (2)
S9iii—Cu28—S10	98.95 (16)	Cu28v—S9—Cu30	111.87 (18)
Cu4iii—Cu28—S10	116.13 (13)	Cu31—S9—Cu30	78.00 (15)
Cu7—Cu28—S10	49.82 (11)	Cu8—S10—Cu27iv	80.41 (16)
S8iv—Cu28—S5	115.50 (18)	Cu8—S10—Cu7	121.4 (2)
S9iii—Cu28—S5	100.13 (16)	Cu27iv—S10—Cu7	101.00 (18)
Cu4iii—Cu28—S5	49.83 (11)	Cu8—S10—Cu49	92.03 (17)
Cu7—Cu28—S5	117.55 (13)	Cu27iv—S10—Cu49	152.7 (2)
S10—Cu28—S5	91.61 (15)	Cu7—S10—Cu49	105.31 (18)
S8iv—Cu28—Cu5	101.72 (15)	Cu8—S10—Cu5	113.4 (2)
S9iii—Cu28—Cu5	125.42 (14)	Cu27iv—S10—Cu5	81.98 (16)
Cu4iii—Cu28—Cu5	95.28 (11)	Cu7—S10—Cu5	124.9 (2)
Cu7—Cu28—Cu5	96.56 (10)	Cu49—S10—Cu5	77.00 (16)
S10—Cu28—Cu5	50.09 (11)	Cu8—S10—Cu28	148.14 (19)
S5—Cu28—Cu5	49.15 (11)	Cu27iv—S10—Cu28	67.84 (14)
S8iv—Cu28—Cu27iv	60.81 (13)	Cu7—S10—Cu28	65.00 (13)
S9iii—Cu28—Cu27iv	132.01 (16)	Cu49—S10—Cu28	117.36 (19)
Cu4iii—Cu28—Cu27iv	160.43 (13)	Cu5—S10—Cu28	65.84 (14)
Cu7—Cu28—Cu27iv	79.30 (10)	Cu8—S11—Cu50	102.93 (19)
S10—Cu28—Cu27iv	48.76 (11)	Cu8—S11—Cu26iv	102.45 (18)
S5—Cu28—Cu27iv	113.06 (14)	Cu50—S11—Cu26iv	154.4 (2)
Cu5—Cu28—Cu27iv	65.62 (9)	Cu8—S11—Cu9	122.5 (2)
S8iv—Cu28—Cu4iv	52.12 (13)	Cu50—S11—Cu9	94.58 (17)
S9iii—Cu28—Cu4iv	98.24 (14)	Cu26iv—S11—Cu9	74.44 (15)
Cu4iii—Cu28—Cu4iv	80.50 (10)	Cu8—S11—Cu6	123.2 (2)
Cu7—Cu28—Cu4iv	140.30 (12)	Cu50—S11—Cu6	72.35 (15)
S10—Cu28—Cu4iv	161.06 (13)	Cu26iv—S11—Cu6	90.85 (17)
S5—Cu28—Cu4iv	93.13 (13)	Cu9—S11—Cu6	114.2 (2)
Cu5—Cu28—Cu4iv	123.06 (12)	Cu8—S11—Cu29A	70.83 (16)
Cu27iv—Cu28—Cu4iv	112.84 (10)	Cu50—S11—Cu29A	114.7 (2)
S7iv—Cu29A—S6	128.5 (3)	Cu26iv—S11—Cu29A	70.99 (14)
S7iv—Cu29A—Cu6	136.2 (2)	Cu9—S11—Cu29A	145.1 (2)
S6—Cu29A—Cu6	57.86 (14)	Cu6—S11—Cu29A	62.03 (15)
S7iv—Cu29A—Cu27iv	60.11 (14)	Cu8—S11—Cu42	62.09 (14)
S6—Cu29A—Cu27iv	121.1 (2)	Cu50—S11—Cu42	80.75 (15)
Cu6—Cu29A—Cu27iv	162.3 (2)	Cu26iv—S11—Cu42	114.57 (19)
S7iv—Cu29A—S11	126.1 (3)	Cu9—S11—Cu42	67.70 (14)
S6—Cu29A—S11	101.92 (19)	Cu6—S11—Cu42	153.09 (19)
Cu6—Cu29A—S11	54.56 (15)	Cu29A—S11—Cu42	132.8 (2)
Cu27iv—Cu29A—S11	112.4 (3)	Cu43—S12—Cu38	116.24 (18)
S7iv—Cu29A—Cu6iv	53.92 (14)	Cu43—S12—Cu30	109.21 (19)
S6—Cu29A—Cu6iv	102.8 (2)	Cu38—S12—Cu30	126.5 (2)
Cu6—Cu29A—Cu6iv	82.35 (12)	Cu43—S12—Cu25iv	113.63 (19)
Cu27iv—Cu29A—Cu6iv	113.90 (14)	Cu38—S12—Cu25iv	113.27 (19)
S11—Cu29A—Cu6iv	102.48 (17)	Cu30—S12—Cu25iv	69.08 (13)
S7iv—Cu29A—Cu5	109.5 (2)	Cu43—S12—Cu9	76.53 (15)
S6—Cu29A—Cu5	52.91 (14)	Cu38—S12—Cu9	77.76 (15)
Cu6—Cu29A—Cu5	104.53 (13)	Cu30—S12—Cu9	141.5 (2)
Cu27iv—Cu29A—Cu5	69.00 (12)	Cu25iv—S12—Cu9	73.80 (14)
S11—Cu29A—Cu5	116.37 (18)	Cu43—S12—Cu39	102.51 (18)
Cu6iv—Cu29A—Cu5	136.8 (3)	Cu38—S12—Cu39	73.63 (15)
S7iv—Cu29A—Cu8	110.8 (2)	Cu30—S12—Cu39	70.27 (15)
S6—Cu29A—Cu8	114.47 (18)	Cu25iv—S12—Cu39	132.3 (2)
Cu6—Cu29A—Cu8	98.5 (2)	Cu9—S12—Cu39	147.4 (2)
Cu27iv—Cu29A—Cu8	65.14 (14)	Cu41—S13—Cu24iv	115.25 (19)
S11—Cu29A—Cu8	49.71 (16)	Cu41—S13—Cu40	113.18 (18)
Cu6iv—Cu29A—Cu8	136.4 (2)	Cu24iv—S13—Cu40	108.87 (18)
Cu5—Cu29A—Cu8	85.57 (13)	Cu41—S13—Cu7	78.89 (15)
S7iv—Cu29A—Cu26iv	79.21 (15)	Cu24iv—S13—Cu7	72.81 (14)
S6—Cu29A—Cu26iv	132.71 (18)	Cu40—S13—Cu7	69.15 (14)
Cu6—Cu29A—Cu26iv	75.64 (14)	Cu41—S13—Cu21vi	113.72 (19)
Cu27iv—Cu29A—Cu26iv	105.76 (18)	Cu24iv—S13—Cu21vi	73.32 (13)
S11—Cu29A—Cu26iv	49.93 (15)	Cu40—S13—Cu21vi	125.7 (2)
Cu6iv—Cu29A—Cu26iv	59.71 (10)	Cu7—S13—Cu21vi	146.02 (19)
Cu5—Cu29A—Cu26iv	163.5 (3)	Cu41—S13—Cu32vi	105.88 (16)
Cu8—Cu29A—Cu26iv	78.14 (18)	Cu24iv—S13—Cu32vi	133.32 (19)
S6—Cu29B—S7iv	163.8 (14)	Cu40—S13—Cu32vi	71.65 (14)
S6—Cu29B—Cu6iv	118.2 (8)	Cu7—S13—Cu32vi	138.81 (19)
S7iv—Cu29B—Cu6iv	57.9 (4)	Cu21vi—S13—Cu32vi	70.55 (13)
S6—Cu29B—Cu5	58.3 (4)	Cu23iv—S14—Cu42	118.75 (19)
S7iv—Cu29B—Cu5	121.3 (7)	Cu23iv—S14—Cu1vi	96.20 (17)
Cu6iv—Cu29B—Cu5	166.6 (12)	Cu42—S14—Cu1vi	71.88 (15)
S6—Cu29B—Cu27iv	127.0 (7)	Cu23iv—S14—Cu41	113.42 (19)
S7iv—Cu29B—Cu27iv	58.9 (4)	Cu42—S14—Cu41	101.19 (18)
Cu6iv—Cu29B—Cu27iv	114.7 (6)	Cu1vi—S14—Cu41	148.4 (2)
Cu5—Cu29B—Cu27iv	69.7 (4)	Cu23iv—S14—Cu8	76.02 (15)
S6—Cu29B—Cu6	57.1 (4)	Cu42—S14—Cu8	67.19 (15)
S7iv—Cu29B—Cu6	131.9 (8)	Cu1vi—S14—Cu8	126.8 (2)
Cu6iv—Cu29B—Cu6	81.7 (5)	Cu41—S14—Cu8	73.65 (15)
Cu5—Cu29B—Cu6	104.1 (5)	Cu23iv—S14—Cu33vi	132.1 (2)
Cu27iv—Cu29B—Cu6	135.6 (10)	Cu42—S14—Cu33vi	103.51 (17)
S5iv—Cu30—S12	138.15 (18)	Cu1vi—S14—Cu33vi	75.50 (15)
S5iv—Cu30—S9	109.47 (17)	Cu41—S14—Cu33vi	76.40 (14)
S12—Cu30—S9	112.08 (16)	Cu8—S14—Cu33vi	145.8 (2)
S5iv—Cu30—Cu25iv	85.27 (14)	Cu51A—S15—Cu22iv	152.3 (3)
S12—Cu30—Cu25iv	55.49 (12)	Cu51A—S15—Cu2vi	87.5 (3)
S9—Cu30—Cu25iv	150.43 (16)	Cu22iv—S15—Cu2vi	107.67 (19)
S5iv—Cu30—Cu39	141.59 (17)	Cu22iv—S15—Cu51B	154.3 (4)
S12—Cu30—Cu39	55.33 (12)	Cu2vi—S15—Cu51B	96.9 (4)
S9—Cu30—Cu39	77.89 (13)	Cu51A—S15—Cu1vi	96.3 (3)
Cu25iv—Cu30—Cu39	106.81 (11)	Cu22iv—S15—Cu1vi	94.68 (18)
S5iv—Cu30—Cu3iv	52.79 (13)	Cu2vi—S15—Cu1vi	122.4 (2)
S12—Cu30—Cu3iv	113.38 (15)	Cu51A—S15—Cu9	79.4 (3)
S9—Cu30—Cu3iv	100.65 (14)	Cu22iv—S15—Cu9	72.94 (15)
Cu25iv—Cu30—Cu3iv	67.32 (9)	Cu2vi—S15—Cu9	121.3 (2)
Cu39—Cu30—Cu3iv	165.38 (12)	Cu51B—S15—Cu9	88.0 (3)
S5iv—Cu30—Cu31	97.01 (14)	Cu1vi—S15—Cu9	115.8 (2)
S12—Cu30—Cu31	105.11 (15)	Cu21iv—S16—Cu43	117.66 (19)
S9—Cu30—Cu31	50.85 (12)	Cu21iv—S16—Cu34vi	107.75 (18)
Cu25iv—Cu30—Cu31	103.28 (10)	Cu43—S16—Cu34vi	113.25 (17)
Cu39—Cu30—Cu31	114.52 (10)	Cu21iv—S16—Cu31	69.59 (13)
Cu3iv—Cu30—Cu31	56.61 (8)	Cu43—S16—Cu31	116.90 (19)
S5iv—Cu30—Cu4	97.18 (14)	Cu34vi—S16—Cu31	123.6 (2)
S12—Cu30—Cu4	113.94 (14)	Cu21iv—S16—Cu2vi	72.30 (14)
S9—Cu30—Cu4	48.29 (12)	Cu43—S16—Cu2vi	76.84 (15)
Cu25iv—Cu30—Cu4	158.11 (12)	Cu34vi—S16—Cu2vi	73.45 (14)
Cu39—Cu30—Cu4	58.71 (8)	Cu31—S16—Cu2vi	141.52 (19)
Cu3iv—Cu30—Cu4	130.73 (10)	Cu21iv—S16—Cu40v	128.50 (19)
Cu31—Cu30—Cu4	98.02 (9)	Cu43—S16—Cu40v	108.87 (18)
S1xi—Cu31—S16	134.34 (18)	Cu34vi—S16—Cu40v	70.20 (14)
S1xi—Cu31—S9	118.24 (17)	Cu31—S16—Cu40v	70.62 (14)
S16—Cu31—S9	105.93 (16)	Cu2vi—S16—Cu40v	142.32 (19)
S1xi—Cu31—Cu21iv	82.06 (13)	Cu13—S17—Cu11i	119.6 (2)
S16—Cu31—Cu21iv	54.13 (12)	Cu13—S17—Cu56xiii	92.73 (18)
S9—Cu31—Cu21iv	143.89 (15)	Cu11i—S17—Cu56xiii	98.03 (17)
S1xi—Cu31—Cu40v	139.27 (15)	Cu13—S17—Cu32	92.01 (18)
S16—Cu31—Cu40v	54.98 (11)	Cu11i—S17—Cu32	109.41 (19)
S9—Cu31—Cu40v	81.55 (12)	Cu56xiii—S17—Cu32	145.1 (2)
Cu21iv—Cu31—Cu40v	102.58 (10)	Cu13—S17—Cu10xiv	115.3 (2)
S1xi—Cu31—Cu24xi	55.58 (12)	Cu11i—S17—Cu10xiv	124.9 (2)
S16—Cu31—Cu24xi	125.13 (14)	Cu56xiii—S17—Cu10xiv	74.27 (15)
S9—Cu31—Cu24xi	104.28 (13)	Cu32—S17—Cu10xiv	72.52 (14)
Cu21iv—Cu31—Cu24xi	111.76 (10)	Cu13—S17—Cu62B	57.8 (3)
Cu40v—Cu31—Cu24xi	86.20 (9)	Cu11i—S17—Cu62B	74.2 (4)
S1xi—Cu31—Cu3iv	55.29 (12)	Cu56xiii—S17—Cu62B	135.4 (3)
S16—Cu31—Cu3iv	106.25 (13)	Cu32—S17—Cu62B	74.5 (3)
S9—Cu31—Cu3iv	102.22 (13)	Cu10xiv—S17—Cu62B	146.0 (3)
Cu21iv—Cu31—Cu3iv	63.28 (8)	Cu33—S18—Cu59i	115.9 (2)
Cu40v—Cu31—Cu3iv	160.80 (11)	Cu33—S18—Cu52	107.9 (2)
Cu24xi—Cu31—Cu3iv	110.63 (9)	Cu59i—S18—Cu52	115.85 (19)
S1xi—Cu31—Cu7v	105.42 (14)	Cu33—S18—Cu11i	76.35 (15)
S16—Cu31—Cu7v	110.46 (13)	Cu59i—S18—Cu11i	73.49 (16)
S9—Cu31—Cu7v	52.38 (12)	Cu52—S18—Cu11i	74.17 (15)
Cu21iv—Cu31—Cu7v	155.80 (11)	Cu33—S18—Cu44	73.59 (14)
Cu40v—Cu31—Cu7v	56.65 (7)	Cu59i—S18—Cu44	110.6 (2)
Cu24xi—Cu31—Cu7v	58.97 (8)	Cu52—S18—Cu44	125.6 (2)
Cu3iv—Cu31—Cu7v	139.83 (10)	Cu11i—S18—Cu44	148.0 (2)
S1xi—Cu31—Cu30	104.86 (14)	Cu33—S18—Cu53	133.8 (2)
S16—Cu31—Cu30	93.47 (13)	Cu59i—S18—Cu53	103.40 (18)
S9—Cu31—Cu30	51.15 (12)	Cu52—S18—Cu53	72.73 (15)
Cu21iv—Cu31—Cu30	96.61 (9)	Cu11i—S18—Cu53	141.01 (19)
Cu40v—Cu31—Cu30	114.53 (9)	Cu44—S18—Cu53	70.39 (14)
Cu24xi—Cu31—Cu30	140.57 (10)	Cu12i—S19—Cu54Ax	87.1 (3)
Cu3iv—Cu31—Cu30	58.09 (7)	Cu12i—S19—Cu51Bi	74.7 (4)
Cu7v—Cu31—Cu30	103.38 (9)	Cu54Ax—S19—Cu51Bi	120.9 (3)
S1iii—Cu32—S17	131.38 (18)	Cu12i—S19—Cu45A	58.4 (3)
S1iii—Cu32—S13i	117.79 (16)	Cu54Ax—S19—Cu45A	115.3 (3)
S17—Cu32—S13i	110.74 (17)	Cu45B—S19—Cu14	68.9 (9)
S1iii—Cu32—Cu34iii	55.14 (12)	Cu54Bx—S19—Cu14	72.7 (4)
S17—Cu32—Cu34iii	111.93 (14)	Cu12i—S19—Cu14	122.1 (3)
S13i—Cu32—Cu34iii	102.88 (13)	Cu54Ax—S19—Cu14	81.73 (19)
S1iii—Cu32—Cu10xiv	108.77 (14)	Cu51Bi—S19—Cu14	154.2 (3)
S17—Cu32—Cu10xiv	54.02 (13)	Cu45A—S19—Cu14	76.0 (2)
S13i—Cu32—Cu10xiv	104.06 (13)	Cu45B—S19—Cu44	92.1 (12)
Cu34iii—Cu32—Cu10xiv	61.38 (8)	Cu54Bx—S19—Cu44	137.8 (5)
S1iii—Cu32—Cu21	79.91 (12)	Cu12i—S19—Cu44	148.3 (3)
S17—Cu32—Cu21	135.87 (15)	Cu54Ax—S19—Cu44	123.0 (2)
S13i—Cu32—Cu21	53.67 (11)	Cu51Bi—S19—Cu44	80.6 (3)
Cu34iii—Cu32—Cu21	111.89 (9)	Cu45A—S19—Cu44	109.2 (3)
Cu10xiv—Cu32—Cu21	156.37 (11)	Cu14—S19—Cu44	76.17 (15)
S1iii—Cu32—Cu3	55.35 (12)	Cu12i—S19—Cu60Bi	67.2 (4)
S17—Cu32—Cu3	106.52 (14)	Cu54Ax—S19—Cu60Bi	56.1 (3)
S13i—Cu32—Cu3	114.89 (13)	Cu45A—S19—Cu60Bi	125.5 (4)
Cu34iii—Cu32—Cu3	109.99 (10)	Cu14—S19—Cu60Bi	137.3 (3)
Cu10xiv—Cu32—Cu3	140.95 (11)	Cu44—S19—Cu60Bi	119.0 (3)
Cu21—Cu32—Cu3	62.21 (8)	Cu12i—S19—Cu51Ai	58.8 (3)
S1iii—Cu32—Cu40i	106.12 (14)	Cu54Ax—S19—Cu51Ai	116.7 (3)
S17—Cu32—Cu40i	100.42 (14)	Cu45A—S19—Cu51Ai	91.4 (3)
S13i—Cu32—Cu40i	52.59 (11)	Cu14—S19—Cu51Ai	161.1 (2)
Cu34iii—Cu32—Cu40i	58.77 (8)	Cu44—S19—Cu51Ai	95.3 (2)
Cu10xiv—Cu32—Cu40i	59.11 (8)	Cu12i—S20—Cu55x	103.5 (2)
Cu21—Cu32—Cu40i	97.59 (9)	Cu12i—S20—Cu10i	123.5 (3)
Cu3—Cu32—Cu40i	153.04 (10)	Cu55x—S20—Cu10i	86.07 (18)
S1iii—Cu32—Cu62B	109.3 (4)	Cu12i—S20—Cu15	121.4 (3)
S17—Cu32—Cu62B	57.8 (3)	Cu55x—S20—Cu15	75.71 (16)
S13i—Cu32—Cu62B	105.4 (3)	Cu10i—S20—Cu15	115.0 (2)
Cu34iii—Cu32—Cu62B	151.7 (3)	Cu12i—S20—Cu34	98.3 (2)
Cu10xiv—Cu32—Cu62B	111.4 (3)	Cu55x—S20—Cu34	156.2 (2)
Cu21—Cu32—Cu62B	84.9 (3)	Cu10i—S20—Cu34	73.94 (15)
Cu3—Cu32—Cu62B	56.5 (3)	Cu15—S20—Cu34	100.93 (18)
Cu40i—Cu32—Cu62B	144.4 (3)	Cu12i—S20—Cu61i	57.4 (2)
S18—Cu33—S2	130.36 (18)	Cu55x—S20—Cu61i	69.19 (15)
S18—Cu33—S14i	120.61 (18)	Cu10i—S20—Cu61i	76.08 (17)
S2—Cu33—S14i	108.33 (16)	Cu15—S20—Cu61i	142.4 (2)
S18—Cu33—Cu62B	78.6 (3)	Cu34—S20—Cu61i	116.6 (2)
S2—Cu33—Cu62B	54.1 (3)	Cu12i—S20—Cu45A	56.6 (2)
S14i—Cu33—Cu62B	147.8 (4)	Cu55x—S20—Cu45A	121.9 (2)
S18—Cu33—Cu22	136.94 (16)	Cu10i—S20—Cu45A	152.0 (2)
S2—Cu33—Cu22	54.97 (12)	Cu15—S20—Cu45A	74.11 (17)
S14i—Cu33—Cu22	81.27 (12)	Cu34—S20—Cu45A	78.34 (16)
Cu62B—Cu33—Cu22	102.3 (4)	Cu61i—S20—Cu45A	113.8 (2)
S18—Cu33—Cu44	54.53 (12)	Cu16iii—S21—Cu13	121.2 (2)
S2—Cu33—Cu44	122.45 (15)	Cu16iii—S21—Cu53xiii	103.03 (19)
S14i—Cu33—Cu44	104.15 (14)	Cu13—S21—Cu53xiii	97.83 (19)
Cu62B—Cu33—Cu44	108.0 (4)	Cu16iii—S21—Cu37iii	87.47 (18)
Cu22—Cu33—Cu44	85.70 (9)	Cu13—S21—Cu37iii	104.83 (19)
S18—Cu33—Cu11i	52.99 (12)	Cu53xiii—S21—Cu37iii	145.3 (2)
S2—Cu33—Cu11i	110.31 (14)	Cu16iii—S21—Cu15iii	116.7 (2)
S14i—Cu33—Cu11i	103.00 (14)	Cu13—S21—Cu15iii	122.0 (2)
Cu22—Cu33—Cu11i	165.01 (11)	Cu53xiii—S21—Cu15iii	72.35 (15)
Cu44—Cu33—Cu11i	106.80 (9)	Cu37iii—S21—Cu15iii	73.34 (15)
S18—Cu33—Cu62A	81.28 (14)	Cu16iii—S21—Cu54A	65.78 (16)
S2—Cu33—Cu62A	49.15 (12)	Cu13—S21—Cu54A	64.53 (16)
S14i—Cu33—Cu62A	156.87 (14)	Cu53xiii—S21—Cu54A	80.44 (15)
Cu22—Cu33—Cu62A	86.99 (11)	Cu37iii—S21—Cu54A	133.2 (2)
Cu44—Cu33—Cu62A	94.70 (11)	Cu15iii—S21—Cu54A	152.6 (2)
Cu11i—Cu33—Cu62A	83.81 (11)	Cu54B—S22—Cu46	86.8 (5)
S18—Cu33—Cu1	104.01 (14)	Cu62A—S22—Cu46	82.0 (2)
S2—Cu33—Cu1	113.08 (13)	Cu54B—S22—Cu52	97.5 (5)
S14i—Cu33—Cu1	51.19 (12)	Cu62A—S22—Cu52	76.72 (19)
Cu62B—Cu33—Cu1	155.5 (5)	Cu46—S22—Cu52	147.0 (2)
Cu22—Cu33—Cu1	58.86 (8)	Cu54B—S22—Cu47B	128.5 (6)
Cu44—Cu33—Cu1	58.47 (8)	Cu46—S22—Cu47B	77.9 (4)
Cu11i—Cu33—Cu1	134.75 (11)	Cu52—S22—Cu47B	121.5 (4)
Cu62A—Cu33—Cu1	135.73 (13)	Cu54B—S22—Cu55	89.3 (5)
S18—Cu33—Cu41i	102.99 (14)	Cu62A—S22—Cu55	121.6 (2)
S2—Cu33—Cu41i	100.88 (14)	Cu46—S22—Cu55	129.3 (2)
S14i—Cu33—Cu41i	51.25 (12)	Cu52—S22—Cu55	83.60 (18)
Cu22—Cu33—Cu41i	118.47 (10)	Cu47B—S22—Cu55	65.8 (4)
Cu44—Cu33—Cu41i	136.25 (11)	Cu62A—S22—Cu54A	132.0 (2)
Cu11i—Cu33—Cu41i	57.77 (8)	Cu46—S22—Cu54A	66.08 (17)
Cu62A—Cu33—Cu41i	120.62 (12)	Cu52—S22—Cu54A	111.6 (2)
Cu1—Cu33—Cu41i	101.28 (9)	Cu55—S22—Cu54A	106.4 (2)
S16i—Cu34—S20	117.94 (17)	Cu54B—S22—Cu13	75.3 (5)
S16i—Cu34—S1	124.42 (16)	Cu62A—S22—Cu13	71.95 (18)
S20—Cu34—S1	117.57 (17)	Cu46—S22—Cu13	76.94 (16)
S16i—Cu34—Cu24	83.81 (12)	Cu52—S22—Cu13	72.61 (16)
S20—Cu34—Cu24	137.80 (15)	Cu47B—S22—Cu13	143.8 (4)
S1—Cu34—Cu24	56.29 (12)	Cu55—S22—Cu13	149.3 (2)
S16i—Cu34—Cu40xii	55.90 (12)	Cu54A—S22—Cu13	66.71 (17)
S20—Cu34—Cu40xii	104.92 (14)	Cu54B—S22—Cu62B	129.8 (6)
S1—Cu34—Cu40xii	106.54 (14)	Cu46—S22—Cu62B	91.4 (4)
Cu24—Cu34—Cu40xii	116.95 (10)	Cu52—S22—Cu62B	60.8 (4)
S16i—Cu34—Cu32v	110.88 (14)	Cu47B—S22—Cu62B	99.8 (6)
S20—Cu34—Cu32v	102.88 (14)	Cu55—S22—Cu62B	127.5 (4)
S1—Cu34—Cu32v	52.99 (12)	Cu13—S22—Cu62B	55.6 (4)
Cu24—Cu34—Cu32v	101.53 (9)	Cu62A—S22—Cu47A	80.1 (3)
Cu40xii—Cu34—Cu32v	61.35 (8)	Cu46—S22—Cu47A	87.8 (3)
S16i—Cu34—Cu10i	105.56 (13)	Cu52—S22—Cu47A	112.6 (3)
S20—Cu34—Cu10i	52.68 (12)	Cu55—S22—Cu47A	58.1 (3)
S1—Cu34—Cu10i	105.12 (13)	Cu54A—S22—Cu47A	130.2 (3)
Cu24—Cu34—Cu10i	160.52 (11)	Cu13—S22—Cu47A	149.6 (3)
Cu40xii—Cu34—Cu10i	59.26 (8)	Cu35—S23—Cu56	114.8 (2)
Cu32v—Cu34—Cu10i	59.32 (8)	Cu35—S23—Cu55	140.2 (2)
S16i—Cu34—Cu2	53.96 (12)	Cu56—S23—Cu55	92.39 (18)
S20—Cu34—Cu2	98.98 (14)	Cu35—S23—Cu53	113.2 (2)
S1—Cu34—Cu2	118.67 (13)	Cu56—S23—Cu53	112.00 (18)
Cu24—Cu34—Cu2	63.40 (8)	Cu55—S23—Cu53	78.91 (17)
Cu40xii—Cu34—Cu2	109.23 (10)	Cu35—S23—Cu14	75.60 (16)
Cu32v—Cu34—Cu2	157.81 (10)	Cu56—S23—Cu14	75.39 (15)
Cu10i—Cu34—Cu2	135.89 (10)	Cu55—S23—Cu14	142.3 (2)
S16i—Cu34—Cu45A	104.47 (15)	Cu53—S23—Cu14	73.30 (16)
S20—Cu34—Cu45A	52.53 (17)	Cu35—S23—Cu47A	75.2 (3)
S1—Cu34—Cu45A	110.63 (16)	Cu56—S23—Cu47A	116.3 (4)
Cu24—Cu34—Cu45A	88.52 (14)	Cu55—S23—Cu47A	66.5 (3)
Cu40xii—Cu34—Cu45A	142.48 (13)	Cu53—S23—Cu47A	120.3 (4)
Cu32v—Cu34—Cu45A	144.02 (13)	Cu14—S23—Cu47A	150.8 (3)
Cu10i—Cu34—Cu45A	105.11 (14)	Cu36B—S24—Cu17	79.3 (8)
Cu2—Cu34—Cu45A	55.93 (12)	Cu36A—S24—Cu17	97.1 (3)
S23—Cu35—S7	119.66 (18)	Cu36B—S24—Cu14	97.5 (6)
S23—Cu35—S3	130.64 (19)	Cu36A—S24—Cu14	91.6 (2)
S7—Cu35—S3	108.13 (17)	Cu17—S24—Cu14	122.1 (2)
S23—Cu35—Cu44	79.35 (14)	Cu36B—S24—Cu15	88.9 (7)
S7—Cu35—Cu44	144.05 (16)	Cu36A—S24—Cu15	76.4 (2)
S3—Cu35—Cu44	53.54 (12)	Cu17—S24—Cu15	120.0 (2)
S23—Cu35—Cu26	139.88 (16)	Cu14—S24—Cu15	117.7 (2)
S7—Cu35—Cu26	80.83 (13)	Cu36A—S24—Cu52x	151.6 (3)
S3—Cu35—Cu26	56.18 (12)	Cu17—S24—Cu52x	96.89 (18)
Cu44—Cu35—Cu26	104.39 (10)	Cu14—S24—Cu52x	101.64 (19)
S23—Cu35—Cu6	102.82 (15)	Cu15—S24—Cu52x	75.18 (15)
S7—Cu35—Cu6	52.79 (12)	Cu60Aix—S25—Cu16iii	102.3 (2)
S3—Cu35—Cu6	115.95 (14)	Cu60Bix—S25—Cu49	118.1 (4)
Cu44—Cu35—Cu6	158.85 (12)	Cu60Aix—S25—Cu49	106.9 (2)
Cu26—Cu35—Cu6	60.29 (8)	Cu16iii—S25—Cu49	147.7 (2)
S23—Cu35—Cu14	53.75 (13)	Cu60Bix—S25—Cu18	94.0 (4)
S7—Cu35—Cu14	102.01 (14)	Cu60Aix—S25—Cu18	75.7 (2)
S3—Cu35—Cu14	106.68 (14)	Cu16iii—S25—Cu18	126.5 (2)
Cu44—Cu35—Cu14	62.95 (8)	Cu49—S25—Cu18	75.04 (16)
Cu26—Cu35—Cu14	162.08 (11)	Cu60Bix—S25—Cu46	114.9 (4)
Cu6—Cu35—Cu14	135.20 (11)	Cu60Aix—S25—Cu46	129.2 (3)
S23—Cu35—Cu47A	54.9 (2)	Cu16iii—S25—Cu46	77.49 (16)
S7—Cu35—Cu47A	110.7 (3)	Cu49—S25—Cu46	73.43 (15)
S3—Cu35—Cu47A	119.3 (3)	Cu18—S25—Cu46	144.5 (2)
Cu44—Cu35—Cu47A	105.2 (3)	Cu60Bix—S25—Cu48	117.3 (4)
Cu26—Cu35—Cu47A	86.4 (2)	Cu60Aix—S25—Cu48	113.1 (2)
Cu6—Cu35—Cu47A	61.8 (3)	Cu16iii—S25—Cu48	66.57 (14)
Cu14—Cu35—Cu47A	108.7 (2)	Cu49—S25—Cu48	112.60 (18)
S24—Cu36A—S4	134.5 (3)	Cu18—S25—Cu48	65.79 (14)
S24—Cu36A—S8	120.6 (3)	Cu46—S25—Cu48	112.85 (17)
S4—Cu36A—S8	100.7 (2)	Cu60Aix—S25—Cu54A	71.1 (2)
S24—Cu36A—Cu45A	80.1 (2)	Cu16iii—S25—Cu54A	67.56 (17)
S4—Cu36A—Cu45A	54.7 (2)	Cu49—S25—Cu54A	109.3 (2)
S8—Cu36A—Cu45A	141.4 (3)	Cu18—S25—Cu54A	146.4 (2)
S24—Cu36A—Cu27	157.7 (3)	Cu46—S25—Cu54A	61.96 (14)
S4—Cu36A—Cu27	58.27 (15)	Cu48—S25—Cu54A	133.7 (2)
S8—Cu36A—Cu27	62.29 (15)	Cu61ix—S26—Cu49	106.7 (2)
Cu45A—Cu36A—Cu27	111.6 (3)	Cu61ix—S26—Cu19	89.62 (19)
S24—Cu36A—S7	104.1 (3)	Cu49—S26—Cu19	80.68 (17)
S4—Cu36A—S7	94.41 (18)	Cu61ix—S26—Cu50	130.2 (2)
S8—Cu36A—S7	88.7 (2)	Cu49—S26—Cu50	116.3 (2)
Cu45A—Cu36A—S7	119.4 (3)	Cu19—S26—Cu50	74.48 (16)
Cu27—Cu36A—S7	53.78 (13)	Cu61ix—S26—Cu47B	117.8 (4)
S24—Cu36A—Cu15	52.55 (14)	Cu49—S26—Cu47B	79.8 (4)
S4—Cu36A—Cu15	104.4 (3)	Cu19—S26—Cu47B	149.9 (4)
S8—Cu36A—Cu15	101.14 (18)	Cu50—S26—Cu47B	94.1 (4)
Cu45A—Cu36A—Cu15	64.0 (2)	Cu61ix—S26—Cu47A	121.4 (3)
Cu27—Cu36A—Cu15	149.3 (2)	Cu49—S26—Cu47A	92.6 (3)
S7—Cu36A—Cu15	156.5 (2)	Cu19—S26—Cu47A	148.8 (4)
S24—Cu36A—Cu37	99.59 (18)	Cu50—S26—Cu47A	81.6 (3)
S4—Cu36A—Cu37	93.8 (2)	Cu61ix—S26—Cu55	62.90 (15)
S8—Cu36A—Cu37	48.33 (14)	Cu49—S26—Cu55	119.3 (2)
Cu45A—Cu36A—Cu37	99.5 (3)	Cu19—S26—Cu55	149.0 (2)
Cu27—Cu36A—Cu37	97.07 (13)	Cu50—S26—Cu55	111.34 (19)
S7—Cu36A—Cu37	137.1 (2)	Cu47B—S26—Cu55	61.1 (4)
Cu15—Cu36A—Cu37	56.44 (11)	Cu47A—S26—Cu55	59.4 (3)
S24—Cu36B—S8	132.6 (10)	Cu58—S27—Cu56	116.10 (18)
S24—Cu36B—S7	119.5 (10)	Cu58—S27—Cu38	112.53 (19)
S8—Cu36B—S7	103.1 (8)	Cu56—S27—Cu38	114.12 (19)
S24—Cu36B—Cu27	158.9 (13)	Cu58—S27—Cu17	74.40 (15)
S8—Cu36B—Cu27	63.5 (4)	Cu56—S27—Cu17	75.96 (15)
S7—Cu36B—Cu27	57.1 (4)	Cu38—S27—Cu17	77.34 (15)
S24—Cu36B—Cu17	51.4 (5)	Cu58—S27—Cu50	130.9 (2)
S8—Cu36B—Cu17	104.5 (10)	Cu56—S27—Cu50	102.52 (19)
S7—Cu36B—Cu17	99.7 (10)	Cu38—S27—Cu50	73.98 (14)
Cu27—Cu36B—Cu17	146.3 (12)	Cu17—S27—Cu50	147.7 (2)
S24—Cu36B—Cu39	104.8 (9)	Cu58—S27—Cu57	73.38 (15)
S8—Cu36B—Cu39	50.1 (5)	Cu56—S27—Cu57	101.52 (18)
S7—Cu36B—Cu39	92.9 (9)	Cu38—S27—Cu57	133.6 (2)
Cu27—Cu36B—Cu39	96.2 (7)	Cu17—S27—Cu57	142.4 (2)
Cu17—Cu36B—Cu39	57.9 (6)	Cu50—S27—Cu57	69.96 (14)
S24—Cu36B—Cu45B	71.6 (9)	Cu20—S28—Cu16	124.8 (2)
S8—Cu36B—Cu45B	124.9 (13)	Cu20—S28—Cu59viii	93.40 (18)
S7—Cu36B—Cu45B	97.4 (12)	Cu16—S28—Cu59viii	80.56 (17)
Cu27—Cu36B—Cu45B	87.8 (9)	Cu20—S28—Cu39	100.23 (19)
Cu17—Cu36B—Cu45B	121.6 (8)	Cu16—S28—Cu39	95.68 (18)
Cu39—Cu36B—Cu45B	169.5 (13)	Cu59viii—S28—Cu39	165.4 (2)
S8—Cu37—S21v	129.21 (19)	Cu20—S28—Cu17	117.0 (2)
S8—Cu37—S1	113.83 (17)	Cu16—S28—Cu17	118.1 (2)
S21v—Cu37—S1	115.94 (18)	Cu59viii—S28—Cu17	93.80 (18)
S8—Cu37—Cu4	53.49 (13)	Cu39—S28—Cu17	75.44 (16)
S21v—Cu37—Cu4	107.50 (16)	Cu20—S28—Cu48v	67.34 (15)
S1—Cu37—Cu4	118.77 (14)	Cu16—S28—Cu48v	64.40 (14)
S8—Cu37—Cu15	105.95 (15)	Cu59viii—S28—Cu48v	111.19 (19)
S21v—Cu37—Cu15	53.88 (13)	Cu39—S28—Cu48v	79.20 (15)
S1—Cu37—Cu15	102.42 (14)	Cu17—S28—Cu48v	154.6 (2)
Cu4—Cu37—Cu15	138.40 (11)	Cu20—S29—Cu57viii	95.27 (17)
S8—Cu37—Cu36A	51.75 (17)	Cu20—S29—Cu18v	126.2 (2)
S21v—Cu37—Cu36A	105.76 (15)	Cu57viii—S29—Cu18v	75.36 (15)
S1—Cu37—Cu36A	103.9 (2)	Cu20—S29—Cu40v	107.43 (18)
Cu4—Cu37—Cu36A	103.35 (17)	Cu57viii—S29—Cu40v	157.1 (2)
Cu15—Cu37—Cu36A	58.19 (10)	Cu18v—S29—Cu40v	93.02 (17)
S8—Cu37—Cu3v	124.60 (14)	Cu20—S29—Cu10	118.4 (2)
S21v—Cu37—Cu3v	95.61 (14)	Cu57viii—S29—Cu10	96.12 (17)
S1—Cu37—Cu3v	49.78 (12)	Cu18v—S29—Cu10	115.2 (2)
Cu4—Cu37—Cu3v	86.38 (9)	Cu40v—S29—Cu10	70.70 (14)
Cu15—Cu37—Cu3v	128.22 (10)	Cu20—S29—Cu48v	68.99 (14)
Cu36A—Cu37—Cu3v	152.25 (16)	Cu57viii—S29—Cu48v	110.05 (19)
S27—Cu38—S7	119.44 (17)	Cu18v—S29—Cu48v	65.55 (14)
S27—Cu38—S12	121.20 (17)	Cu40v—S29—Cu48v	81.71 (14)
S7—Cu38—S12	117.62 (17)	Cu10—S29—Cu48v	152.40 (19)
S27—Cu38—Cu50	53.43 (12)	Cu18—S30—Cu41	89.29 (17)
S7—Cu38—Cu50	103.71 (14)	Cu18—S30—Cu19	122.6 (2)
S12—Cu38—Cu50	122.91 (15)	Cu41—S30—Cu19	102.53 (18)
S27—Cu38—Cu39	104.01 (14)	Cu18—S30—Cu11	114.2 (2)
S7—Cu38—Cu39	98.81 (14)	Cu41—S30—Cu11	75.47 (16)
S12—Cu38—Cu39	53.72 (13)	Cu19—S30—Cu11	123.1 (2)
Cu50—Cu38—Cu39	154.11 (11)	Cu18—S30—Cu58ix	76.49 (16)
S27—Cu38—Cu6	104.41 (14)	Cu41—S30—Cu58ix	155.0 (2)
S7—Cu38—Cu6	52.24 (12)	Cu19—S30—Cu58ix	102.45 (18)
S12—Cu38—Cu6	120.94 (14)	Cu11—S30—Cu58ix	91.56 (17)
Cu50—Cu38—Cu6	58.74 (8)	Cu42—S31—Cu59	105.7 (2)
Cu39—Cu38—Cu6	147.11 (11)	Cu42—S31—Cu57	120.4 (2)
S27—Cu38—Cu17	51.52 (12)	Cu59—S31—Cu57	117.27 (19)
S7—Cu38—Cu17	100.46 (14)	Cu42—S31—Cu19	75.93 (16)
S12—Cu38—Cu17	105.39 (14)	Cu59—S31—Cu19	78.43 (16)
Cu50—Cu38—Cu17	103.67 (9)	Cu57—S31—Cu19	74.61 (15)
Cu39—Cu38—Cu17	59.22 (8)	Cu42—S31—Cu51B	63.7 (3)
Cu6—Cu38—Cu17	132.94 (10)	Cu59—S31—Cu51B	108.6 (3)
S27—Cu38—Cu9	101.61 (13)	Cu57—S31—Cu51B	128.4 (3)
S7—Cu38—Cu9	125.93 (14)	Cu19—S31—Cu51B	139.5 (3)
S12—Cu38—Cu9	51.59 (12)	Cu42—S31—Cu60A	132.4 (2)
Cu50—Cu38—Cu9	72.77 (9)	Cu59—S31—Cu60A	102.8 (2)
Cu39—Cu38—Cu9	103.91 (10)	Cu57—S31—Cu60A	76.5 (2)
Cu6—Cu38—Cu9	86.19 (9)	Cu19—S31—Cu60A	147.7 (2)
Cu17—Cu38—Cu9	133.33 (10)	Cu42—S31—Cu60B	128.5 (3)
S8—Cu39—S28	120.67 (19)	Cu59—S31—Cu60B	89.0 (4)
S8—Cu39—S12	116.84 (18)	Cu57—S31—Cu60B	92.9 (4)
S28—Cu39—S12	121.95 (18)	Cu19—S31—Cu60B	155.2 (3)
S8—Cu39—Cu30	81.64 (14)	Cu51B—S31—Cu60B	64.8 (4)
S28—Cu39—Cu30	140.79 (18)	Cu42—S31—Cu51A	69.3 (2)
S12—Cu39—Cu30	54.40 (12)	Cu59—S31—Cu51A	122.4 (3)
S8—Cu39—Cu38	101.58 (15)	Cu57—S31—Cu51A	112.8 (3)
S28—Cu39—Cu38	107.02 (15)	Cu19—S31—Cu51A	143.0 (2)
S12—Cu39—Cu38	52.65 (12)	Cu60A—S31—Cu51A	63.3 (2)
Cu30—Cu39—Cu38	98.09 (10)	Cu12—S32—Cu43	89.6 (2)
S8—Cu39—Cu17	104.00 (15)	Cu12—S32—Cu61	60.2 (2)
S28—Cu39—Cu17	52.32 (13)	Cu43—S32—Cu61	115.3 (2)
S12—Cu39—Cu17	106.93 (14)	Cu12—S32—Cu60A	75.9 (3)
Cu30—Cu39—Cu17	159.92 (12)	Cu43—S32—Cu60A	134.9 (2)
Cu38—Cu39—Cu17	62.02 (8)	Cu61—S32—Cu60A	94.2 (2)
S8—Cu39—Cu4	51.74 (13)	Cu12—S32—Cu20	121.9 (3)
S28—Cu39—Cu4	99.76 (15)	Cu43—S32—Cu20	79.38 (16)
S12—Cu39—Cu4	121.86 (14)	Cu61—S32—Cu20	73.76 (18)
Cu30—Cu39—Cu4	67.56 (9)	Cu60A—S32—Cu20	144.1 (3)
Cu38—Cu39—Cu4	149.96 (12)	Cu12—S32—Cu58	153.6 (3)
Cu17—Cu39—Cu4	131.04 (11)	Cu43—S32—Cu58	114.3 (2)
S8—Cu39—Cu36B	48.2 (5)	Cu61—S32—Cu58	114.2 (2)
S28—Cu39—Cu36B	100.4 (4)	Cu60A—S32—Cu58	79.0 (2)
S12—Cu39—Cu36B	111.8 (5)	Cu20—S32—Cu58	75.85 (16)
Cu30—Cu39—Cu36B	117.4 (3)	Cu12—S32—Cu51A	59.9 (3)
Cu38—Cu39—Cu36B	66.0 (5)	Cu43—S32—Cu51A	69.4 (2)
Cu17—Cu39—Cu36B	59.2 (4)	Cu61—S32—Cu51A	119.9 (3)
Cu4—Cu39—Cu36B	96.3 (5)	Cu60A—S32—Cu51A	66.4 (2)
S13—Cu40—S29iii	124.08 (17)	Cu20—S32—Cu51A	148.8 (3)
S13—Cu40—S16iii	121.74 (16)	Cu58—S32—Cu51A	116.3 (3)
S29iii—Cu40—S16iii	114.18 (17)	Cu12—S32—Cu60B	62.6 (4)
S13—Cu40—Cu7	55.65 (12)	Cu43—S32—Cu60B	127.7 (3)
S29iii—Cu40—Cu7	99.08 (14)	Cu61—S32—Cu60B	89.3 (3)
S16iii—Cu40—Cu7	116.37 (13)	Cu20—S32—Cu60B	152.7 (3)
S13—Cu40—Cu34xv	106.48 (14)	Cu58—S32—Cu60B	92.6 (3)
S29iii—Cu40—Cu34xv	106.51 (14)

Symmetry codes: (i) x, y, z−1; (ii) −x, −y+1, −z; (iii) x, y−1, z; (iv) −x, −y+1, −z+1; (v) x, y+1, z; (vi) x, y, z+1; (vii) x, y+1, z+1; (viii) −x+1/2, y+1/2, −z+3/2; (ix) −x+1/2, y−1/2, −z+3/2; (x) −x+1/2, y+1/2, −z+1/2; (xi) −x, −y+2, −z+1; (xii) x, y+1, z−1; (xiii) −x+1/2, y−1/2, −z+1/2; (xiv) x, y−1, z−1; (xv) x, y−1, z+1.

Funding Statement

Funding for this research was provided by: The National Natural Science Foundation of China (grant No. 52173231/51771165).