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. 2022 Nov 21;27(22):8074. doi: 10.3390/molecules27228074

Table 1.

NMR Data for 11 (500 MHz for 1H and 125 MHz for 13C, in CDCl3, δ in ppm, J in Hz).

Positions 1H 13C *
1 3.93 dt (10.5, 1.4) 74.8
2 2.18–2.04 m 31.34
3 2.36–2.21 m 37.94
4 - 153.51
5 5.13 dd (10.2, 1.6) 121.28
6 4.34 t (9.8) 80.05
7 2.36–2.21 m 41.56
8 1.97–1.80 m 36.81
9 4.76 dt (10.2, 1.5) 78.81
10 - 145.18
11 1.97–1.80 m 51.05
12 - 175.06
13 1.27 d (6.9) 12.55
14 5.42 d (1.2); 5.34 br s 114.37
15 1.58 d (1.3) 17.48
16 - 177.43
17 2.36–2.21 m 27.64
18 1.11 t (7.6) 8.53

* The assignments were based on HSQC and HMBC data.