Skip to main content
Proceedings of the National Academy of Sciences of the United States of America logoLink to Proceedings of the National Academy of Sciences of the United States of America
. 1995 Apr 25;92(9):3799–3803. doi: 10.1073/pnas.92.9.3799

Swapping structural determinants of ribonucleases: an energetic analysis of the hinge peptide 16-22.

L Mazzarella 1, L Vitagliano 1, A Zagari 1
PMCID: PMC42049  PMID: 7731986

Abstract

Bovine seminal ribonuclease (BS-RNase) is a homodimeric enzyme strictly homologous to the pancreatic ribonuclease (RNase A). Native BS-RNase is an equilibrium mixture of two distinct dimers differing in the interchange of the N-terminal segments and in their biological properties. The loop 16-22 plays a fundamental role on the relative stability of the two isomers. Both the primary and tertiary structures of the RNase A differ substantially from those of the seminal ribonuclease in the loop region 16-22. To analyze the possible stable conformations of this loop in both enzymes, structure predictions have been attempted, according to a procedure described by Palmer and Scheraga [Palmer, K. A. & Scheraga, H. A. (1992) J. Comput. Chem. 13, 329-350]. Results compare well with experimental x-ray structures and clarify the structural determinants that are responsible for the swapping of the N-terminal domains and for the peculiar properties of BS-RNase. Minimal modifications of RNase A sequence needed to form a stable swapped dimer are also predicted.

Selected References

These references are in PubMed. This may not be the complete list of references from this article.

  1. Bennett M. J., Choe S., Eisenberg D. Domain swapping: entangling alliances between proteins. Proc Natl Acad Sci U S A. 1994 Apr 12;91(8):3127–3131. doi: 10.1073/pnas.91.8.3127. [DOI] [PMC free article] [PubMed] [Google Scholar]
  2. Capasso S., Giordano F., Mattia C. A., Mazzarella L., Zagari A. Refinement of the structure of bovine seminal ribonuclease. Biopolymers. 1983 Jan;22(1):327–332. doi: 10.1002/bip.360220142. [DOI] [PubMed] [Google Scholar]
  3. D'Alessio G., Di Donato A., Parente A., Piccoli R. Seminal RNase: a unique member of the ribonuclease superfamily. Trends Biochem Sci. 1991 Mar;16(3):104–106. doi: 10.1016/0968-0004(91)90042-t. [DOI] [PubMed] [Google Scholar]
  4. D'Alessio G., Malorni M. C., Parente A. Dissociation of bovine seminal ribonuclease into catalytically active monomers by selective reduction and alkylation of the intersubunit disulfide bridges. Biochemistry. 1975 Mar 25;14(6):1116–1122. doi: 10.1021/bi00677a004. [DOI] [PubMed] [Google Scholar]
  5. D'Alessio G. Oligomer evolution in action? Nat Struct Biol. 1995 Jan;2(1):11–13. doi: 10.1038/nsb0195-11. [DOI] [PubMed] [Google Scholar]
  6. Di Donato A., Cafaro V., D'Alessio G. Ribonuclease A can be transformed into a dimeric ribonuclease with antitumor activity. J Biol Chem. 1994 Jul 1;269(26):17394–17396. [PubMed] [Google Scholar]
  7. Fruchter R. G., Crestfield A. M. On the structure of ribonuclease dimer. Isolation and identification of monomers derived from inactive carboxymethyl dimers. J Biol Chem. 1965 Oct;240(10):3875–3882. [PubMed] [Google Scholar]
  8. Mazzarella L., Capasso S., Demasi D., Di Lorenzo G., Mattia C. A., Zagari A. Bovine seminal ribonuclease: structure at 1.9 A resolution. Acta Crystallogr D Biol Crystallogr. 1993 Jul 1;49(Pt 4):389–402. doi: 10.1107/S0907444993003403. [DOI] [PubMed] [Google Scholar]
  9. Parente A., D'Alessio G. Reacquisition of quaternary structure by fully reduced and denatured seminal ribonuclease. Eur J Biochem. 1985 Jun 3;149(2):381–387. doi: 10.1111/j.1432-1033.1985.tb08936.x. [DOI] [PubMed] [Google Scholar]
  10. Piccoli R., Di Donato A., D'Alessio G. Co-operativity in seminal ribonuclease function. Kinetic studies. Biochem J. 1988 Jul 15;253(2):329–336. doi: 10.1042/bj2530329. [DOI] [PMC free article] [PubMed] [Google Scholar]
  11. Piccoli R., Tamburrini M., Piccialli G., Di Donato A., Parente A., D'Alessio G. The dual-mode quaternary structure of seminal RNase. Proc Natl Acad Sci U S A. 1992 Mar 1;89(5):1870–1874. doi: 10.1073/pnas.89.5.1870. [DOI] [PMC free article] [PubMed] [Google Scholar]
  12. Wlodawer A., Sjölin L. Structure of ribonuclease A: results of joint neutron and X-ray refinement at 2.0-A resolution. Biochemistry. 1983 May 24;22(11):2720–2728. doi: 10.1021/bi00280a021. [DOI] [PubMed] [Google Scholar]

Articles from Proceedings of the National Academy of Sciences of the United States of America are provided here courtesy of National Academy of Sciences

RESOURCES